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公开(公告)号：US4400408A
公开(公告)日：1983-08-23
申请号：US263542
申请日：1981-05-14
IPC分类号： C25B11/06 , B22F7/04 , C23C18/14 , C23C24/08 , C23C24/10 , C23C26/00 , C25B11/10 , B05D3/02 , B05D3/12
CPC分类号： C23C24/106 , B22F7/04 , C23C18/14 , C23C24/08
摘要： A method for forming an anticorrosive coating on the surface of a metal substrate, which comprises, in one embodiment, (1) coating the surface of the metal substrate with an anticorrosive metal capable of forming an alloy with the substrate metal and/or a hydride of the anticorrosive metal; (2) heating the coated surface, and then; (3) heating the coated surface in a vacuum or in an atmosphere substantially inert to the metal coating and the metal substrate by irradiating the coated surface with electron beams, laser beams or a plasma arc to sinter the coated metal and form an alloy layer in the interface between the metal substrate and the metal coating and, in another embodiment, subsequent to Step (2) and prior Step (3) above, coating the coated surface with a solution of a thermally decomposable platinum-group metal compound and then heating the resulting coated surface at about 40.degree. C. to about 600.degree. C.
摘要翻译： 一种在金属基材的表面上形成防腐涂层的方法，在一个实施方案中包括（1）用能够与基底金属和/或氢化物形成合金的防腐金属涂覆金属基材的表面 的防腐金属; （2）加热涂层表面，然后; （3）通过用电子束，激光束或等离子体电弧照射涂覆的表面，在真空中或在基本上对金属涂层和金属基板惰性的气氛中加热涂覆的表面，以烧结涂覆的金属并形成合金层 金属基材和金属涂层之间的界面，在另一个实施方案中，在上述步骤（2）和先前步骤（3）之后，用可热分解的铂族金属化合物的溶液涂覆涂布表面，然后加热 得到的涂覆表面在约40℃至约600℃
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2.发明授权
公开(公告)号：US4568568A
公开(公告)日：1986-02-04
申请号：US688204
申请日：1985-01-03
CPC分类号： C25B11/0478 , C25B11/0489
摘要： A cathode for electrolyzing acid solutions which comprises an electrically conductive metal substrate, a spray coated layer of a cathode active material containing tungsten, tungsten carbide or a mixture thereof in an amount of 10% by weight or more on the substrate, and an impregnation coated layer of 1 g/m.sup.2 or more of an acid-resistant fluorine containing resin on the outside surface of the coated layer of cathode active material, and a process for producing such.
摘要翻译： 一种用于电解酸性溶液的阴极，其包含导电金属基底，在基底上含有10重量％以上的含有钨，碳化钨或其混合物的阴极活性材料的喷涂层，以及浸渍涂层 在阴极活性物质的被覆层的外表面上为1g / m 2以上的耐酸性含氟树脂层，以及其制造方法。
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公开(公告)号：US4349581A
公开(公告)日：1982-09-14
申请号：US233704
申请日：1981-02-12
摘要： A method for forming an anticorrosive coating on the surface of a metal substrate, which comprises, in one embodiment, (1) coating the surface of the metal substrate with an anticorrosive metal capable of forming an alloy with the substrate metal using a spraying procedure, and (2) then heating the coated surface in a vacuum or in an atmosphere substantially inert to the metal coating and metal substrate by irradiating electron beams or a plasma arc thereonto to form an alloy layer in the interface between the metal substrate and the metal coating and, in a second embodiment, subsequent to step (1) and prior to step (2) above coating a solution of a thermally decomposable platinum-group metal compound on the surface of the resulting coating, and heat-treating the coated product at about 50.degree. to about 300.degree. C.
摘要翻译： 一种在金属基材表面上形成防腐蚀涂层的方法，其特征在于，在一个实施方案中，（1）使用喷涂方法用能够与基材金属形成合金的防腐蚀金属涂覆金属基材的表面， 和（2）然后在真空中或在基本上对金属涂层和金属基底呈惰性的气氛中通过在其上照射电子束或等离子弧来加热涂覆表面，以在金属基底和金属涂层之间的界面中形成合金层 在第二实施方案中，在步骤（1）之后并且在上述步骤（2）之前，在所得涂层的表面上涂覆可热分解的铂族金属化合物溶液，并将涂覆产物在约 50〜300℃
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4.发明授权Electrolysis apparatus using a diaphragm of a solid polymer electrolyte, and method for production thereof 失效使用固体高分子电解质膜片的电解装置及其制造方法
公开(公告)号：US4498942A
公开(公告)日：1985-02-12
申请号：US503452
申请日：1983-06-13
申请人： Hiroshi Asano , Takayuki Shimamune , Toshiki Goto
发明人： Hiroshi Asano , Takayuki Shimamune , Toshiki Goto
IPC分类号： C25B9/00 , C25B1/46 , C25B9/06 , C25B9/08 , C25B9/10 , C25B11/04 , C25B11/06 , H01M8/10 , B32B31/12
CPC分类号： C25B9/10 , C25B11/0484 , H01M8/1004 , H01M8/1023 , H01M8/1039 , Y02P70/56
摘要： An electrolysis apparatus comprising a diaphragm of a solid polymer electrolyte, and an anode electrode structure and a cathode electrode structure located on both sides of the diaphragm, at least one of the electrode structures intimately contacting the surface of said diaphragm, the intimately contacting electrode structure comprising a gas-permeable electrically conductive substrate and a film-like porous electrode catalyst layer bonded integrally thereto and a method for producing such.
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5.发明授权
公开(公告)号：US4473454A
公开(公告)日：1984-09-25
申请号：US508752
申请日：1983-06-28
CPC分类号： C25B11/0489
摘要： A cathode for use in the electrolysis of acid solutions, comprisingan electrically conductive substrate,a sprayed coating layer containing at least 10% by weight of W, WC or a mixture thereof on the substrate andan impregnated coating layer comprising a mixture of a cathode active substance and an acid-resistant fluorine-based resin on the external surface of the sprayed coating layer, and a process for the production of such a cathode. The cathode has very superior hydrogen overvoltage characteristics and durability, and is very suitable for use in the electrolysis of acid solutions.
摘要翻译： 一种用于电解酸性溶液的阴极，包括导电基材，在基材上含有至少10重量％的W，WC或其混合物的喷涂层，以及包含阴极的混合物的浸渍涂层 活性物质和喷涂层的外表面上的耐酸氟系树脂，以及这种阴极的制造方法。 阴极具有非常优异的氢过电压特性和耐久性，非常适用于电解酸溶液。
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公开(公告)号：US4457822A
公开(公告)日：1984-07-03
申请号：US217608
申请日：1980-12-18
申请人： Hiroshi Asano , Takayuki Shimamune , Toshiki Goto
发明人： Hiroshi Asano , Takayuki Shimamune , Toshiki Goto
IPC分类号： C25B9/00 , C25B1/46 , C25B9/06 , C25B9/08 , C25B9/10 , C25B11/04 , C25B11/06 , H01M8/10 , C25B11/03 , C25B11/10
CPC分类号： C25B9/10 , C25B11/0484 , H01M8/1004 , H01M8/1023 , H01M8/1039 , Y02P70/56
摘要： An electrolysis apparatus comprising a diaphragm of a solid polymer electrolyte, and an anode electrode structure and a cathode electrode structure located on both sides of the diaphragm, at least one of the electrode structures intimately contacting the surface of said diaphragm, the intimately contacting electrode structure comprising a gas-permeable electrically conductive substrate and a film-like porous electrode catalyst layer bonded integrally thereto and a method for producing such.
摘要翻译： 一种电解装置，包括固体聚合物电解质的隔膜和位于隔膜两侧的阳极电极结构和阴极电极结构，至少一个电极结构与所述隔膜的表面紧密接触，紧密接触的电极结构 包括透气性导电性基材和与其一体结合的膜状多孔电极催化剂层及其制造方法。
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公开(公告)号：US4500405A
公开(公告)日：1985-02-19
申请号：US568515
申请日：1984-01-09
CPC分类号： C25B11/0478 , C25B11/0489
摘要： A cathode for electrolyzing acid solutions which comprises an electrically conductive metal substrate, a spray coated layer of a cathode active material containing tungsten, tungsten carbide or a mixture thereof in an amount of 10% by weight or more on the substrate, and an impregnation coated layer of 1 g/m.sup.2 or more of an acid-resistant fluorine containing resin on the outside surface of the coated layer of cathode active material, and a process for producing such.
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公开(公告)号：US4253933A
公开(公告)日：1981-03-03
申请号：US074946
申请日：1979-09-13
申请人： Hideo Sato , Takayuki Shimamune , Toshiki Goto , Hideo Nitta
发明人： Hideo Sato , Takayuki Shimamune , Toshiki Goto , Hideo Nitta
CPC分类号： C22C14/00 , C25B11/0431
摘要： An alloy for use as a substrate of an electrode for use in electrolysis, the alloy comprising(1) titanium and(2) 0.05 to 10% by weight of (a) tantalum and (b) niobium, zirconium or mixtures thereof, where the tantalum is present in an amount of 0.01 to 9.99% by weight, with each % by weight being based on the weight of the alloy. The alloy can additionally contain(3) 0.001 to 1.5% by weight of at least one platinum-group metal selected from the group consisting of platinum, iridium, rhodium, ruthenium, palladium and osmium, with the % by weight being based on the weight of the alloy. The alloy of this invention is an excellent material to prepare a corrosion-resistant electrode substrate.
摘要翻译： 一种用作电解用电极基板的合金，所述合金包括（1）钛和（2）0.05-10重量％的（a）钽和（b）铌，锆或其混合物，其中 钽以0.01〜9.99重量％的量存在，其中每重量％以合金的重量计。 该合金还可以含有（3）0.001-1.5重量％的至少一种选自铂，铱，铑，钌，钯和锇的铂族金属，其中重量百分数以重量为基准 的合金。 本发明的合金是制备耐腐蚀电极基材的优良材料。
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9.发明申请Combustion-Assisted Substrate Deposition Method For Producing Carbon Nanosubstances 审中-公开用于生产碳纳米管的燃烧辅助底物沉积方法公开(公告)号：US20090191352A1
公开(公告)日：2009-07-30
申请号：US12019352
申请日：2008-01-24
申请人： Douglas P. DuFaux , Randy Vander Wal , Masato Tani , Toshiki Goto
发明人： Douglas P. DuFaux , Randy Vander Wal , Masato Tani , Toshiki Goto
CPC分类号： B01J37/0242 , B01J23/28 , B01J23/745 , B01J23/755 , B01J23/78 , B01J23/881 , B01J23/882 , B01J23/8892 , B01J37/0225 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/162 , C01B32/17
摘要： The present invention provides a combustion-based method and apparatus for producing and isolating carbon nanotubes. The nanotubes are formed when hot combustion gases are contacted with a catalytic surface, which is readily separated from the catalyst support and subsequently dissolved. The process is suitable for large-scale manufacture of carbon nanotubes.
摘要翻译： 本发明提供一种用于制造和分离碳纳米管的基于燃烧的方法和装置。 当热燃烧气体与催化剂表面接触时形成纳米管，催化表面容易与催化剂载体分离并随后溶解。 该方法适用于大规模制造碳纳米管。
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10.发明申请Production Method for Carbon Nano Structure of Catalyst Particle Diameter Control Mode, Production Device, and Carbon Nano Structure 审中-公开催化剂粒径控制模式，生产装置和碳纳米结构碳纳米结构的生产方法公开(公告)号：US20080063589A1
公开(公告)日：2008-03-13
申请号：US11632466
申请日：2005-07-13
申请人： Yoshikazu Nakayama , Takeshi Nagasaka , Toru Sakai , Toshiki Goto , Hiroyuki Tsuchiya , Keisuke Shiono , Nobuharu Okazaki
发明人： Yoshikazu Nakayama , Takeshi Nagasaka , Toru Sakai , Toshiki Goto , Hiroyuki Tsuchiya , Keisuke Shiono , Nobuharu Okazaki
CPC分类号： D01F9/127 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/36 , D01F9/133
摘要： The subject invention provides a stable mass production method of carbon nano structure at low cost immune to variation of particle diameter of the catalyst microparticle in the catalyst material. The subject invention also provides a production device used for the method, and a new carbon nano structure having a conformation suitable for the mass production. The production method of carbon nano structure comprising fluidizing a material gas and catalyst microparticles in the reactor so that the material gas and the catalyst microparticles are brought into contact with each other, wherein said catalyst microparticles are suspended by the instantaneous spraying of the high-pressure gas, and then the suspension effect of the catalyst microparticles is stopped so that the catalyst microparticles naturally fall. The particle diameter of the catalyst microparticles is thus selected. With this arrangement, only the selected catalyst microparticles with the desired diameter are supplied to the reactor. Since this arrangement is immune to influence of variation in particle diameter of catalyst microparticles contained in the catalyst material, it achieves stable mass production of carbon nano structure at low cost.
摘要翻译： 本发明提供一种低成本的碳纳米结构的稳定的大规模生产方法，其不受催化剂材料中催化剂微粒的粒径变化的影响。 本发明还提供了一种用于该方法的生产装置和具有适于批量生产的构象的新型碳纳米结构。 碳纳米结构体的制造方法，其特征在于，在所述反应器中使原料气体和催化剂微粒流化，使得原料气体和催化剂微粒相互接触，其中，所述催化剂微粒通过瞬时喷射高压 气体，然后停止催化剂微粒的悬浮效果，使得催化剂微粒自然落下。 因此选择催化剂微粒的粒径。 利用这种布置，只有所选择的具有所需直径的催化剂微粒被提供给反应器。 由于这种布置不受催化剂材料中所含的催化剂微粒的粒径变化的影响，因此以低成本实现了碳纳米结构的稳定的批量生产。
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