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    Photoconductor materials based on new phase of titanyl phthalocyanine
    1.
    发明授权
    Photoconductor materials based on new phase of titanyl phthalocyanine 失效
    基于氧化钛酞菁新相的感光体材料

    公开(公告)号：US06815132B2

    公开(公告)日：2004-11-09

    申请号：US10328697

    申请日：2002-12-24

    申请人： Jiayi Zhu ,  Zbigniew Tokarski ,  James A. Baker ,  Ronald J. Moudry ,  David T. Ask ,  Nusrallah Jubran ,  Kam W. Law

    发明人： Jiayi Zhu ,  Zbigniew Tokarski ,  James A. Baker ,  Ronald J. Moudry ,  David T. Ask ,  Nusrallah Jubran ,  Kam W. Law

    IPC分类号： G03G506

    CPC分类号： C09B67/0026 ,  G03G5/047 ,  G03G5/0696 ,  G03G7/0033

    摘要： A crystalline phase of titanyl oxyphthalocyanine, referred to herein as the S-phase, has an internal blend of lattice arrangements is provided by treatment of the gamma-form of titanyl oxyphthalocyanine. The S-phase is a truly new phase, and not a mixture of particles of various phases (e.g., combinations of the beta-phase and the gamma-phase), with internal lattice distributions of atoms and molecules forming a new, non-continuous, non-uniform lattice structure. The x-ray spectrum shows a blend of diffraction peaks, having peaks that have previously been distinctly present only collectively among various crystalline forms of titanyl oxyphthalocyanine, but can now be provided in a single crystalline form. The visible spectra show significant absorption differences. The novel S-form titanyl oxyphthalocyanine is also used in a photoconductor displaying major peaks of Bragg's 2 theta angle to the CuK-alpha characteristic X-ray (wavelength 1.541 Angstrom) at least at 9.5±0.2 degrees, 9.7±0.2 degrees, 11.7±0.2 degrees, 13.5±0.2 degrees, (optionally at 21±0.2 degrees and/or 23.5±0.2 degrees,) 24.1±0.2 degrees, 26.4±0.2 degrees, and 27.3±0.2 degrees group. Additional peaks, approaching or equivalent to major peaks, may also be present as 15.0, 15.3 and 16.0±0.2 degrees.

    摘要翻译： 钛氧基氧酞菁的结晶相，本文称为S相，具有格子排列的内部共混物，通过处理γ型氧钛氧基酞菁得到。 S相是一个真正的新阶段，而不是各种相的粒子的混合物（例如，β相和γ相的组合），原子和分子的内部晶格分布形成新的非连续的 ，不均匀的晶格结构。 X射线光谱显示了衍射峰的混合物，其具有先前已经明确存在于各种结晶形式的氧钛氧酞菁中的峰，但现在可以单晶形式提供。 可见光谱显示出显着的吸收差异。 新型的S型氧基氧代酞菁也用于显示布拉格2θ角与CuK-α特征X射线（波长1.541埃）的主峰至少9.5±0.2度，9.7±0.2度，11.7± 24度±0.2度，26.4±0.2度和27.3±0.2度组（可选地为21±0.2度和/或23.5±0.2度）。 接近或等同于主峰的附加峰也可以以15.0,15.3和16.0±0.2度的形式存在。

    Photoconductor materials based on complex of charge generating material
    2.
    发明授权
    Photoconductor materials based on complex of charge generating material 失效
    基于电荷产生材料复合材料的感光体材料

    公开(公告)号：US07018757B2

    公开(公告)日：2006-03-28

    申请号：US10356683

    申请日：2003-01-31

    申请人： Jiayi Zhu ,  Zbigniew Tokarski ,  James A. Baker ,  Ronald J. Moudry ,  David T. Ask ,  Nusrallah Jubran ,  Kam W. Law

    发明人： Jiayi Zhu ,  Zbigniew Tokarski ,  James A. Baker ,  Ronald J. Moudry ,  David T. Ask ,  Nusrallah Jubran ,  Kam W. Law

    IPC分类号： G03G5/047

    CPC分类号： G03G5/047 ,  G03G5/06 ,  G03G5/0696 ,  G03G7/0033

    摘要： An electrophotographic article having a complex of charge generating material and at least one transfer material selected from the group consisting of electron transfer material and hole transfer material is formed by admixing the charge generating material, at least one transfer material, and an organic binder in a solvent to form a coatable dispersion comprising a complex of charge generating material and said at least one transfer material; and coating said coatable dispersion onto a conductive substrate to form a charge transfer layer on the electrophotoconductive article. A novel S-form titanyl oxyphthalocyanine is also preferred, the novel form displaying major peaks of Bragg's 2theta angle to the CuK-alpha characteristic X-ray (wavelength 1.541 Angstrom) at least at 9.5±0.2 degrees, 9.7±0.2 degrees, 11.7±0.2 degrees, 13.5±0.2 degrees, (optionally at 21±0.2 degrees and/or 23.5±0.2 degrees,) 24.1±0.2 degrees, 26.4±0.2 degrees, and 27.3±0.2 degrees group. Additional peaks, approaching or equivalent to major peaks, may also be present as 15.0, 15.3 and 16.0±0.2 degrees.

    摘要翻译： 通过将电荷产生材料，至少一种转印材料和有机粘合剂混合在一起形成具有电荷产生材料和选自电子转移材料和空穴转移材料的至少一种转移材料的复合物的电子照相制品， 溶剂以形成包含电荷产生材料和所述至少一种转移材料的复合物的可涂覆分散体; 并将所述可涂覆分散体涂覆到导电基材上以在电子导电制品上形成电荷转移层。 一种新型的S型氧基氧代酞菁也是优选的，这种形式显示了布拉格2θ角与CuKα特征X射线（波长1.541埃）至少9.5±0.2度，9.7±0.2度，11.7± 24度±0.2度，26.4±0.2度和27.3±0.2度组（可选地为21±0.2度和/或23.5±0.2度）。 接近或等同于主峰的附加峰也可以以15.0,15.3和16.0±0.2度的形式存在。

    Electrophotographic photoreceptors with novel overcoats
    3.
    发明授权
    Electrophotographic photoreceptors with novel overcoats 有权
    具有新颖大衣的电子照相感光体

    公开(公告)号：US06869741B2

    公开(公告)日：2005-03-22

    申请号：US10167932

    申请日：2002-06-10

    申请人： Jiayi Zhu ,  Zbigniew Tokarski ,  Ronald J. Moudry ,  Kristine A. Fordahl ,  David T. Ask ,  Jonas Sidaravicius ,  Edmundas Montrimas ,  Kam W. Law ,  Valentas Gaidelis

    发明人： Jiayi Zhu ,  Zbigniew Tokarski ,  Ronald J. Moudry ,  Kristine A. Fordahl ,  David T. Ask ,  Jonas Sidaravicius ,  Edmundas Montrimas ,  Kam W. Law ,  Valentas Gaidelis

    IPC分类号： G03G5/07 ,  G03G5/05 ,  G03G5/06 ,  G03G5/147

    CPC分类号： G03G5/0661 ,  G03G5/0532 ,  G03G5/0542 ,  G03G5/0546 ,  G03G5/0616 ,  G03G5/0648 ,  G03G5/1473 ,  G03G5/14734 ,  G03G5/14791 ,  G03G5/14795

    摘要： A photoreceptor with good mechanical and physical properties is provided with an overcoat layer comprising a copolymer of an α,β-ethylenically unsaturated carboxylic acid and an α,β-ethylenically unsaturated monomer wherein the weight percent of the α,β-ethylenically unsaturated carboxylic-acid is at least 25% up to 99% of the copolymer. The copolymer may comprise an α,β-ethylenically unsaturated carboxylic acid and an α,β-ethylenically unsaturated monomer wherein the copolymer has an acid value of at least 150 mg KOH/g the copolymer. The copolymer may be present in a blend with a second polymer or copolymer comprised of units derived from a second α,β-ethylenically unsaturated monomer that is different from the an α,β-ethylenically unsaturated carboxylic acid and/or the α,β-ethylenically unsaturated monomer. The copolymer or the copolymer blend may be present in a layer that is crosslinked or crosslinkable, the crosslinking being effected through a distinct crosslinking agent that reacts with group(s) on the an α,β-ethylenically unsaturated carboxylic acid or the α,β-ethylenically unsaturated monomer.

    摘要翻译： 提供具有良好机械和物理性质的感光体，其具有包含α，β-烯键式不饱和羧酸和α，β-烯属不饱和单体的共聚物的外涂层，其中α，β-烯键式不饱和羧酸 - 酸是至少25％至99％的共聚物。 共聚物可以包含α，β-烯属不饱和羧酸和α，β-烯属不饱和单体，其中共聚物的酸值至少为150mg KOH / g。 共聚物可以与第二聚合物或共聚物一起存在，所述第二聚合物或共聚物由衍生自不同于α，β-烯键式不饱和羧酸和/或α，β-烯属不饱和羧酸的第二α，β-烯属不饱和单体的单元组成， 烯属不饱和单体。 共聚物或共聚物共混物可以存在于交联或可交联的层中，交联通过与α，β-烯属不饱和羧酸或α，β上的基团反应的不同交联剂进行 烯属不饱和单体。

    Organophotoreceptor with an electron transport layer
    4.
    发明授权
    Organophotoreceptor with an electron transport layer 失效
    具有电子传递层的有机光感受器

    公开(公告)号：US06890693B2

    公开(公告)日：2005-05-10

    申请号：US10396536

    申请日：2003-03-25

    申请人： Jiayi Zhu ,  Nusrallah Jubran ,  Zbigniew Tokarski ,  James A. Baker ,  Ronald J. Moudry

    发明人： Jiayi Zhu ,  Nusrallah Jubran ,  Zbigniew Tokarski ,  James A. Baker ,  Ronald J. Moudry

    IPC分类号： G03G5/043 ,  G03G5/047 ,  G03G5/06 ,  G03G5/14 ,  G03G5/147

    CPC分类号： G03G5/047 ,  G03G5/0696 ,  G03G5/142 ,  G03G5/14708

    摘要： Improved organophotoreceptor have an electrically conductive substrate, a charge generation layer comprising a charge generation compound and optionally a charge transport compound, and an overcoat layer comprising an electron transport compound wherein the charge generation layer is between the overcoat layer and the electrically conductive substrate. The organophotoreceptor can optionally comprise a charge transport layer and/or other desired layers. The organophotoreceptors are useful in electrophotographic imaging apparatuses and corresponding processes.

    摘要翻译： 改进的有机光感受器具有导电基底，电荷产生层，其包含电荷产生化合物和任选的电荷输送化合物，以及包含电子传输化合物的外涂层，其中电荷产生层位于外涂层和导电基底之间。 有机光感受器可任选地包含电荷传输层和/或其它所需的层。 有机光感受器在电子照相成像设备和相应的工艺中是有用的。

    Dry toner blended with wax
    7.
    发明授权
    Dry toner blended with wax 失效
    干蜡与蜡混合

    公开(公告)号：US07354687B2

    公开(公告)日：2008-04-08

    申请号：US10978688

    申请日：2004-10-31

    申请人： Leonard Stulc ,  Ronald J. Moudry ,  Zbigniew Tokarski ,  Charles W. Simpson ,  Gay L. Herman ,  A. Kristine Fordahl ,  James A. Baker

    发明人： Leonard Stulc ,  Ronald J. Moudry ,  Zbigniew Tokarski ,  Charles W. Simpson ,  Gay L. Herman ,  A. Kristine Fordahl ,  James A. Baker

    IPC分类号： G03G9/00

    CPC分类号： G03G9/0825 ,  G03G9/08782 ,  G03G9/08788 ,  G03G9/08797

    摘要： Dry electrographic toner compositions are provided comprising a plurality of dry toner particles, wherein the toner particles comprise polymeric binder comprising at least one amphipathic copolymer comprising one or more S material portions and one or more D material portions. The dry electrographic toner composition comprises a wax associated with the dry toner particles, wherein substantially all of the wax is associated with the toner particle at the surface thereof. Methods of making electrographic toner compositions are also provided comprising preparing polymeric binder particles comprising at least one amphipathic copolymer comprising one or more S material portions and one or more D material portions, preparing toner particles, drying the toner particles, and milling the dry toner particles in the presence of a wax component to provide a dry toner particle composition having the wax associated with the toner particles. These toner compositions provide images having excellent durability and erasure resistance properties at low fusion temperatures and with little undesired offset.

    摘要翻译： 提供包含多个干调色剂颗粒的干燥电摄影调色剂组合物，其中调色剂颗粒包含包含至少一种包含一个或多个S材料部分和一个或多个D材料部分的两亲共聚物的聚合物粘合剂。 干电摄影调色剂组合物包含与干调色剂颗粒相关联的蜡，其中基本上所有的蜡在其表面与调色剂颗粒相关联。 还提供了制备电子照相色调剂组合物的方法，包括制备包含至少一种包含一种或多种S材料部分和一种或多种D材料部分的两亲共聚物的聚合物粘合剂颗粒，制备调色剂颗粒，干燥调色剂颗粒和研磨干调色剂颗粒 在蜡组分的存在下，提供具有与调色剂颗粒相关的蜡的干调色剂颗粒组合物。 这些调色剂组合物在低熔融温度下提供具有优异的耐久性和耐擦性能的图像，并且几乎没有不希望的偏移。

    Dry toner comprising wax
    9.
    发明授权
    Dry toner comprising wax 失效
    含蜡的干燥调色剂

    公开(公告)号：US07306886B2

    公开(公告)日：2007-12-11

    申请号：US10978836

    申请日：2004-10-31

    申请人： Gay L. Herman ,  Ronald J. Moudry ,  Zbigniew Tokarski ,  Charles W. Simpson ,  Leonard Stulc ,  A. Kristine Fordahl ,  James A. Baker

    发明人： Gay L. Herman ,  Ronald J. Moudry ,  Zbigniew Tokarski ,  Charles W. Simpson ,  Leonard Stulc ,  A. Kristine Fordahl ,  James A. Baker

    IPC分类号： G03G9/00

    CPC分类号： G03G9/08711 ,  G03G9/0804 ,  G03G9/08782 ,  G03G9/08786 ,  G03G9/08795 ,  G03G9/08797

    摘要： Dry electrographic toner compositions are provided comprising a plurality of dry toner particles, wherein the toner particles comprise polymeric binder comprising at least one amphipathic copolymer comprising one or more S material portions and one or more D material portions. The dry electrographic toner composition comprises a wax associated with the dry toner particles, wherein a substantial portion of the wax is entrained in the toner particle and a substantial portion of the wax is associated with the toner particle at the surface thereof. Methods of making electrographic toner compositions are also provided comprising preparing polymeric binder particles comprising at least one amphipathic copolymer comprising one or more S material portions and one or more D material portions, and milling the particles before or after formulation as toner particles with wax in the liquid carrier prior to drying to form the dry toner composition. These toner compositions provide images having excellent durability and erasure resistance properties at low fusion temperatures and with little undesired offset.

    摘要翻译： 提供包含多个干调色剂颗粒的干燥电摄影调色剂组合物，其中调色剂颗粒包含包含至少一种包含一个或多个S材料部分和一个或多个D材料部分的两亲共聚物的聚合物粘合剂。 干电摄影调色剂组合物包含与干调色剂颗粒相关联的蜡，其中大部分蜡被夹带在调色剂颗粒中，并且蜡的大部分与其表面处的调色剂颗粒相关联。 还提供了制备电子照相色调剂组合物的方法，包括制备包含至少一种包含一种或多种S材料部分和一种或多种D材料部分的两亲共聚物的聚合物粘合剂颗粒，并且在配制之前或之后将颗粒研磨成具有蜡的调色剂颗粒 在干燥之前形成干燥的调色剂组合物。 这些调色剂组合物在低熔融温度下提供具有优异的耐久性和耐擦性能的图像，并且几乎没有不希望的偏移。

    Positively charged coated electrographic toner particles
    10.
    发明授权
    Positively charged coated electrographic toner particles 有权
    带正电荷的涂布电子照相调色剂颗粒

    公开(公告)号：US07183031B2

    公开(公告)日：2007-02-27

    申请号：US10840897

    申请日：2004-05-07

    申请人： Zbigniew Tokarski ,  Ronald J. Moudry

    发明人： Zbigniew Tokarski ,  Ronald J. Moudry

    IPC分类号： G03G9/00

    CPC分类号： G03G9/1355 ,  G03G9/08786 ,  G03G9/08788 ,  G03G9/08791 ,  G03G9/08793 ,  G03G9/08795 ,  G03G9/08797 ,  G03G9/09 ,  G03G9/09307 ,  G03G9/09321 ,  G03G9/09335 ,  G03G9/09342 ,  G03G9/1138 ,  G03G9/122 ,  G03G9/131 ,  G03G9/133 ,  G03G9/135

    摘要： Positively charged coated toner particles are provided that comprise a plurality of polymeric binder particles that are substantially free of positively charged pigment and a coating material comprising at least one positively charged pigment coated on the outside surface of the polymeric binder particles. In one embodiment, a majority of the specific charge of the toner particles is contributed from the positively charged pigment. In another embodiment, the toner particles are substantially free of additional charge director or charge control additive. Electrographic toner compositions comprising these particles are also provided.

    摘要翻译： 提供了带电荷的涂覆的调色剂颗粒，其包含基本上不带正电的颜料的多个聚合物粘合剂颗粒和包含涂覆在聚合物粘合剂颗粒的外表面上的至少一种带正电的颜料的涂料。 在一个实施方案中，调色剂颗粒的大部分特定电荷由带正电的颜料贡献。 在另一个实施方案中，调色剂颗粒基本上不含附加的电荷导向剂或电荷控制添加剂。 还提供了包含这些颗粒的电子调色剂组合物。