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公开(公告)号：US20110184105A1
公开(公告)日：2011-07-28
申请号：US12892680
申请日：2010-09-28
申请人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Francisco Manuel Benitez , Catherine Anne Faler , Allen David Godwin , Jörg Friedrich Wilhelm Weber , Diana S. Smirnova
发明人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Francisco Manuel Benitez , Catherine Anne Faler , Allen David Godwin , Jörg Friedrich Wilhelm Weber , Diana S. Smirnova
CPC分类号： C07C69/612 , C07C69/76
摘要： A process for making non-phthalate, 1,2-phenylene oxo-diester plasticizers for polymer compositions, by selectively hydrogenating naphthalene to form a partially hydrogenated naphthalene, oxygenating said partially hydrogenated naphthalene to form phenylene diacids, and esterifying said phenylene diacids with oxo-alcohols to form 1,2-phenylene oxo-diesters. Also a process for making phenylene oxo-diester plasticizers by selectively brominating xylenes to form bisbromomethylbenzene, catalytic carboalkoxylation of the bromo-compound to form phenylene diacetate, followed by transesterification to form the phenylene oxo-diester.
摘要翻译： 通过选择性氢化萘以形成部分氢化的萘来制备用于聚合物组合物的非邻苯二甲酸酯，1,2-亚苯基氧代二酯增塑剂的方法，将所述部分氢化的萘氧化以形成亚苯基二酸，并用所述亚苯基二酸酯化所述亚苯基二酸， 醇形成1,2-亚苯基氧代二酯。 也是通过选择性溴化二甲苯以形成双溴甲苯制备亚苯基二氧代二酯增塑剂的方法，溴化合物的催化羰基烷氧基化形成亚苯基二乙酸酯，然后酯交换以形成亚苯基氧代二酯。
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公开(公告)号：US08604114B2
公开(公告)日：2013-12-10
申请号：US12840715
申请日：2010-07-21
申请人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Karla Schall Colle , Allen David Godwin , Diana S. Smirnova , Jörg Friedrich Wilhelm Weber , Stephen Zushma
发明人： Jihad Mohammed Dakka , Edmund John Mozeleski , Lisa Saunders Baugh , Karla Schall Colle , Allen David Godwin , Diana S. Smirnova , Jörg Friedrich Wilhelm Weber , Stephen Zushma
CPC分类号： C08K5/12 , C07C51/31 , C07C67/08 , C07C67/31 , C07C69/73 , C07C69/732 , C07C69/738 , C07C2602/10 , C08K5/10 , C07C59/84 , C07C59/86
摘要： Provided is a process for making non-phthalate plasticizers, by acylating an aromatic compound with a succinic anhydride to form a keto-acid, and then esterifying the keto-acid with C4-C13 OXO-alcohols to form a plasticizer compound. The aromatic rings of the aromatic compound may also be optionally hydrogenated.
摘要翻译： 提供了制备非邻苯二甲酸酯增塑剂的方法，通过用琥珀酸酐酰化芳族化合物以形成酮酸，然后用C4-C13OXO-醇酯化酮酸以形成增塑剂化合物。 芳族化合物的芳环也可以任选氢化。
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公开(公告)号：US20130035431A1
公开(公告)日：2013-02-07
申请号：US13198851
申请日：2011-08-05
申请人： Jihad Mohammed Dakka , Stephen Zushma , Christine A. Costello , Edmund John Mozeleski , Diana S. Smirnova , Allen David Godwin , Pierre J. Osterrieth , Jörg Friedrich Wilhelm Weber , Paul Hamden Daniels , Thomas M. Larson , Catherine A. Faler
发明人： Jihad Mohammed Dakka , Stephen Zushma , Christine A. Costello , Edmund John Mozeleski , Diana S. Smirnova , Allen David Godwin , Pierre J. Osterrieth , Jörg Friedrich Wilhelm Weber , Paul Hamden Daniels , Thomas M. Larson , Catherine A. Faler
IPC分类号： C08K5/12 , C07C69/736 , C07C67/08 , C07C67/343 , C08L33/00 , C08L67/00 , C08L75/04 , C08L31/04 , C08L21/00 , C07C69/612 , C08L27/06
CPC分类号： C07C67/08 , C07C67/343 , C07C69/612 , C07C69/734 , C08K5/0016 , C08K5/11
摘要： Provided are compounds of the formula: wherein m=0-3 and n=0-3, and R1 represents CxH2x wherein x=0 to 4 or cyclohexane; R2 represents H, a C1-C6 alkyl group at any of the ortho-, meta- or para-positions, a residue including heteroatoms chosen from O, N, and S, or mixtures thereof; and R3 and R4 represent hydrocarbon residues of OXO-C5-C9 alcohols which are different isomers of equal carbon number or different in carbon number. Also provided are processes for making the compounds and plasticized polymer compositions containing said compounds.
摘要翻译： 提供下式的化合物：其中m = 0-3且n = 0-3，并且R1表示CxH2x，其中x = 0至4或环己烷; R 2表示H，任何邻位，间位或对位的C 1 -C 6烷基，包括选自O，N和S的杂原子的残基或其混合物; 并且R 3和R 4代表相同碳数或碳数不同的不同异构体的OXO-C5-C9醇的烃残基。 还提供了制备含有所述化合物的化合物和增塑聚合物组合物的方法。
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公开(公告)号：US08604110B2
公开(公告)日：2013-12-10
申请号：US13198851
申请日：2011-08-05
申请人： Jihad Mohammed Dakka , Stephen Zushma , Christine A. Costello , Edmund John Mozeleski , Diana S. Smirnova , Allen David Godwin , Pierre J. Osterrieth , Jörg Friedrich Wilhelm Weber , Paul Hamden Daniels , Thomas M. Larson , Catherine A. Faler
发明人： Jihad Mohammed Dakka , Stephen Zushma , Christine A. Costello , Edmund John Mozeleski , Diana S. Smirnova , Allen David Godwin , Pierre J. Osterrieth , Jörg Friedrich Wilhelm Weber , Paul Hamden Daniels , Thomas M. Larson , Catherine A. Faler
CPC分类号： C07C67/08 , C07C67/343 , C07C69/612 , C07C69/734 , C08K5/0016 , C08K5/11
摘要： Provided are compounds of the formula: wherein m=0-3 and n=0-3, and R1 represents CxH2x wherein x=0 to 4 or cyclohexane; R2 represents H, a C1-C6 alkyl group at any of the ortho-, meta- or para-positions, a residue including heteroatoms chosen from O, N, and S, or mixtures thereof; and R3 and R4 represent hydrocarbon residues of OXO-C5-C9 alcohols which are different isomers of equal carbon number or different in carbon number. Also provided are processes for making the compounds and plasticized polymer compositions containing said compounds.
摘要翻译： 提供下式的化合物：其中m = 0-3且n = 0-3，并且R1表示CxH2x，其中x = 0至4或环己烷; R 2表示H，任何邻位，间位或对位的C 1 -C 6烷基，包括选自O，N和S的杂原子的残基或其混合物; 并且R 3和R 4代表相同碳数或碳数不同的不同异构体的OXO-C5-C9醇的烃残基。 还提供了制备含有所述化合物的化合物和增塑聚合物组合物的方法。
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