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1.发明授权Liquid crystal phase of an azo reactive dyestuff and its use for dyeing and printing natural and synthetic substrates 失效偶氮活性染料的液晶相及其用于染色和印刷天然和合成基材的用途
公开(公告)号：US4309182A
公开(公告)日：1982-01-05
申请号：US208595
申请日：1980-11-19
申请人： Jochen Koll , Volker Paulat , Reinhold Hornle , Hans-Heinz Molls , Konrad Nonn
发明人： Jochen Koll , Volker Paulat , Reinhold Hornle , Hans-Heinz Molls , Konrad Nonn
IPC分类号： C09K19/24 , C09B62/28 , C09B62/405 , C09B67/24 , C09B67/26 , C09B67/00 , C09B62/24 , C09B62/32
CPC分类号： C09B62/405 , C09B67/0072 , C09K19/601 , Y10S8/917 , Y10S8/918 , Y10S8/919
摘要： Liquid finished formulations which are stable to storage and hydrolysis and are based on the lyotropic liquid crystal aqueous phase of the dyestuff of the formula ##STR1## which is present in water in a concentration of 23-35% at room temperature, are outstandingly suitable for the preparation of dyebaths and printing pastes for dyeing cotton, wool, regenerated cellulose, paper and leather.
摘要翻译： 对储存和水解稳定的基于在室温下以23-35％的浓度存在于水中的式“IMAGE”的染料的溶致液晶水相的液体成品制剂非常适合于 染色棉，羊毛，再生纤维素，纸和皮革染色浴和印花浆的制备。
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2.发明授权Liquid crystal phase of an azo reactive dyestuff and its use for dyeing and printing natural and synthetic substrates 失效偶氮活性染料的液晶相及其用于染色和印刷天然和合成基材的用途
公开(公告)号：US4309183A
公开(公告)日：1982-01-05
申请号：US208592
申请日：1980-11-19
申请人： Jochen Koll , Volker Paulat , Reinhold Hornle , Hans-Heinz Molls , Konrad Nonn
发明人： Jochen Koll , Volker Paulat , Reinhold Hornle , Hans-Heinz Molls , Konrad Nonn
CPC分类号： C09B67/0073 , C09B62/405 , C09K19/601 , Y10S8/917 , Y10S8/918 , Y10S8/919
摘要： Liquid finished formulations which are stable to storage and hydrolysis and are based on the lyotropic liquid crystal aqueous phase of the dyestuff of the formula ##STR1## in water in a concentration of 12-35% at room temperature are outstandingly suitable for the preparation of dyebaths and printing pastes for dyeing cotton, wool, regenerated cellulose, paper and leather.
摘要翻译： 对于储存和水解稳定并且基于式（IMAGE）的染料的溶致液晶水相，在室温下浓度为12-35％的水中的液体成品配方显着地适用于染浴的制备 并印染棉，羊毛，再生纤维素，纸和皮革的浆料。
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3.发明授权Liquid-crystalline phase of an azo reactive dyestuff, and its use for the dyeing and printing of natural and synthetic substrates 失效偶氮活性染料的液晶相，以及其用于染色和印刷天然和合成基材的用途
公开(公告)号：US4443225A
公开(公告)日：1984-04-17
申请号：US444024
申请日：1982-11-23
申请人： Joachim Wolff , Karlheinz Wolf , Jochen Koll , Reinhold Hornle , Hans-Heinz Molls , Volker Paulat
发明人： Joachim Wolff , Karlheinz Wolf , Jochen Koll , Reinhold Hornle , Hans-Heinz Molls , Volker Paulat
IPC分类号： C09B62/028 , C09B67/00 , D21H21/28 , C09B62/00 , D06P1/38
CPC分类号： C09B62/028 , C09B67/0029 , D21H21/28 , Y10S8/917 , Y10S8/918 , Y10S8/919
摘要： The lyotropic, liquid-crystalline, aqueous phase of a reactive dyestuff of the formula ##STR1## wherein M.sym. represents H.sym. or an alkali metal cation (preferably Na.sym., K.sym. or Li.sym.) andR is a fibre-reactive groupingpresent in water at room temperature in a concentration of 10-25%, if appropriate in the presence of concentration-increasing additives and/or buffer substances, is highly suitable for preparing dyebaths and print pastes for application to natural and synthetic substrates, in particular cotton, wool, regenerated cellulose, paper and leather.
摘要翻译： 式（I）其中M（+）表示H（+）或碱金属阳离子（优选Na（+），K（+）或Li（Ⅴ））的活性染料的溶致液晶， （+）），R是在室温下以10-25％的浓度存在于水中的纤维反应性分解剂，如果在浓度增加的添加剂和/或缓冲物质的存在下适当，则非常适用于制备染浴和 印刷适用于天然和合成基材的浆料，特别是棉，羊毛，再生纤维素，纸和皮革。
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公开(公告)号：US4013481A
公开(公告)日：1977-03-22
申请号：US311779
申请日：1972-12-04
申请人： Hans-Heinz Molls , Karlheinz Wolf , Reinhold Hornle , Gottfried Popp , Konrad Nonn , Jurgen Spille
发明人： Hans-Heinz Molls , Karlheinz Wolf , Reinhold Hornle , Gottfried Popp , Konrad Nonn , Jurgen Spille
IPC分类号： C09D7/00 , C08J3/20 , C09B67/08 , C09B67/40 , C09C3/00 , C09C3/04 , C09C3/08 , C09D11/00 , C09D11/02
CPC分类号： C09C3/041 , C09B67/0004 , C09B67/0009 , C01P2004/61
摘要： Process for the manufacture of pigment preparations by comminution in the presence of surface-active agents which can be saponified under acid or alkaline conditions and which contain at least one group which confers solubility in a radical which is to be split off during the saponification.
摘要翻译： 通过在酸性或碱性条件下皂化的表面活性剂的存在下粉碎制造颜料制剂的方法，其含有至少一个赋予在皂化期间被分离的基团中溶解度的基团。
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5.发明授权Leather dyeing agents and their preparation: membrame separation of dye mother liquor 失效皮革染色剂及其制备方法：将母液分离成母液
公开(公告)号：US4402701A
公开(公告)日：1983-09-06
申请号：US304239
申请日：1981-09-21
申请人： Harald Gleinig , Hans-Heinz Molls , Jochen Koll , Gottfried Dick , Reinhold Hornle , Friedrich Kunert
发明人： Harald Gleinig , Hans-Heinz Molls , Jochen Koll , Gottfried Dick , Reinhold Hornle , Friedrich Kunert
CPC分类号： C09B67/0096 , C09B67/0072
摘要： Leather dyeing agents, which can be obtained by concentrating, by means of a membrane separation process, the mother liquors, which are produced in the salting-out process in the preparation of organic dyestuffs which are water-soluble or which contain groups imparting water-solubility, the mother liquors having an extinction in the absorption maximum which is .gtoreq.500, with a layer thickness of 10 cm, and by drying the concentrate, if appropriate.
摘要翻译： 皮革染色剂，其可以通过膜分离方法浓缩而获得，在盐析过程中制备的母液是制备有机染料的水溶性或含有赋予水溶性的组分， 溶解度，吸收最大值为> = 500的消光母液，层厚度为10厘米，如果合适，干燥浓缩物。
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公开(公告)号：US4329145A
公开(公告)日：1982-05-11
申请号：US176388
申请日：1980-08-08
申请人： Jochen Koll , Hans-Heinz Molls , Reinhold Hornle , Erhard Schuffenhauer , Horst Brandt , Fritz Bremer , Karlheinz Wolf , Willy Schiwy
发明人： Jochen Koll , Hans-Heinz Molls , Reinhold Hornle , Erhard Schuffenhauer , Horst Brandt , Fritz Bremer , Karlheinz Wolf , Willy Schiwy
CPC分类号： C09B67/0082 , C09B67/0091 , C09B67/0096
摘要： Highly concentrated liquid preparations of disperse dyestuffs are obtained with a low consumption of energy by first adding a dispersing agent to the water-moist dyestuff press-cake to convert it into a form in which it is capable of flow, subjecting this product to wet grinding and increasing the dyestuff content of the resulting, insufficiently concentrated dispersion in a second step by means of a membrane separation process, for example pressure permeation.
摘要翻译： 通过首先向水润染料压饼中加入分散剂将其分解成能够流动的形式，使该产品进行湿磨，得到分散染料的高浓度液体制剂，其能量消耗低 并且通过膜分离方法，例如压力渗透，在第二步骤中增加所得到的，不充分浓缩的分散体的染料含量。
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公开(公告)号：US4318848A
公开(公告)日：1982-03-09
申请号：US866523
申请日：1978-01-03
IPC分类号： B01F17/00 , B01F17/12 , B01J19/00 , C09B1/00 , C09B1/22 , C09B7/02 , C09B11/02 , C09B29/20 , C09B41/00 , C09B45/01 , C09B45/16 , C09B67/46 , C07C105/00 , C07C107/04 , C07C107/06 , C07C107/08
CPC分类号： C09B67/0091 , B01F17/0057 , B01J19/0086 , C09B1/005 , C09B1/22 , C09B11/02 , C09B29/20 , C09B41/001 , C09B45/01 , C09B45/16 , C09B7/02
摘要： Chemical reaction products, obtained in an alkaline medium and which require the addition of a dispersing agent, are neutralized by addition of a free surface-active acid to which, after its preparation, basic agents have not been added or have only been added up to a pH value of 3.
摘要翻译： 在碱性介质中获得并且需要加入分散剂的化学反应产物通过添加游离的表面活性酸中和，在其制备之后，碱性试剂未被加入或仅添加到 pH值为3。
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公开(公告)号：US3958929A
公开(公告)日：1976-05-25
申请号：US440662
申请日：1974-02-08
申请人： Reinhold Hornle , Hans-Heinz Molls , Roland Rupp , Robert Kuth
发明人： Reinhold Hornle , Hans-Heinz Molls , Roland Rupp , Robert Kuth
CPC分类号： C09B67/0092 , D06L3/1264 , Y10S8/912
摘要： Pressing of uniform shape and uniform weight of disperse dyestuffs and optical brightening agents with a solubility in water less than 0.5% at 20.degree.C which are suitable for an automate metering step and which disintegrate in aqueous dye baths to give dispersions are manufactured by compressing the dyestuff or brightening agent, an anionic dispersing agent and a solid water-soluble mould release agent which gives a neutral to weakly alkaline reaction in water.
摘要翻译： 压制均匀的形状和均匀重量的分散染料和荧光增白剂，其在20℃下的溶解度小于0.5％，适用于自动计量步骤，并在水性染料浴中分解以得到分散体，通过压缩 染料或增亮剂，阴离子分散剂和在水中产生中性至弱碱性反应的固体水溶性脱模剂。
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公开(公告)号：US4198264A
公开(公告)日：1980-04-15
申请号：US844348
申请日：1977-10-21
摘要： Sifting is improved by the installation of one or more nozzles in the longitudinal axis of a drier. A spray-dried granulate is thereby substantially freed from dust. The effect of heat on low melting products is reduced by cooling the gas.
摘要翻译： 通过在干燥器的纵向轴线上安装一个或多个喷嘴来改善筛分。 因此，喷雾干燥的颗粒基本上没有灰尘。 通过冷却气体来降低热量对低熔点产品的影响。
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公开(公告)号：US4089700A
公开(公告)日：1978-05-16
申请号：US684649
申请日：1976-05-10
CPC分类号： C09B67/0004 , C09B67/0003
摘要： Organic pigments which provide an opaque color impression in binders and exhibit adequate flow properties in binders are obtained from pigments which provide a transparent color impression in binders in a simple way in that an azeotrope-forming agent which is appropriate for the liquid adhering to the pigment is added to the moist pigment obtained after the preparation, and the azeotropic mixture and any excess solvent which may be present are then distilled off.
摘要翻译： 在粘合剂中提供不透明色印象并且在粘合剂中表现出足够的流动性的有机颜料由颜料获得，所述颜料以简单的方式在粘合剂中提供透明的颜色印象，因为适合于粘附于颜料的液体的共沸形成剂 加入到制备后获得的湿润颜料中，然后蒸馏出共沸混合物和任何可能存在的过量溶剂。
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