Manufacture of conjugated linoleic salts and acids
    3.
    发明授权
    Manufacture of conjugated linoleic salts and acids 有权
    共轭亚油酸盐和酸的制备

    公开(公告)号:US06897327B2

    公开(公告)日:2005-05-24

    申请号:US10434011

    申请日:2003-05-08

    IPC分类号: C07C51/09 C07C51/347

    CPC分类号: C07C51/09 C07C57/12

    摘要: A process to manufacture conjugated linoleic acid (CLA)-containing materials such as conjugated linoleic salts and acids that are enriched in desirable cis-9, trans-11- and trans-10, cis-12-CLA isomers and are low in certain undesirable isomers. The process generally entails isomerization of an alkyl ester of a linoleic acid-containing material at a temperature typically between about 90 to 140° C. to effectuate conjugation of the double bonds, followed by saponification of the resultant CLA-containing fatty acid ester to produce a CLA-containing fatty acid salt, optionally followed by neutralization of the CLA-containing fatty acid salt with an acid source to produce a CLA-containing fatty acid.

    摘要翻译: 一种制备共轭亚油酸(CLA)的物质,例如共轭亚油酸盐和酸的方法,其富含所需的顺式-9,反式-11-和反式-10,顺式-12-CLA异构体,并且在某些不期望的情况下是低的 异构体。 该方法通常需要含有亚油酸的材料的烷基酯在典型地在约90至140℃之间的温度下进行异构化,以实现双键的共轭化,然后将所得的含CLA脂肪酸酯皂化以产生 含CLA的脂肪酸盐,任选地随后用酸源中和含CLA的脂肪酸盐以产生含CLA的脂肪酸。

    Process for Enzymatic Production of Triglycerides
    4.
    发明申请
    Process for Enzymatic Production of Triglycerides 有权
    甘油三酯的酶促生产工艺

    公开(公告)号:US20090131701A1

    公开(公告)日:2009-05-21

    申请号:US10585427

    申请日:2004-01-29

    IPC分类号: C07C59/00 C12P7/64

    CPC分类号: C12P7/6472 C12P7/6454

    摘要: A process for enzymatic production of glyceride compositions, specifically industrially practicable production of triglycerides, including conjugated linoleic and linolenic acid triglycerides, and the compositions produced by such process. An enzymatic reaction zone is first utilized, in which a mixture of glycerol and fatty acids or fatty acid derivatives is reacted in the presence of an enzymatic catalyst to form 1,3 diglycerides. The mixture is then circulated through a second thermal rearrangement zone, maintained at a higher temperature, to promote rearrangement of the 1,3 diglycerides to 1,2 diglycerides. Triglycerides are produced by re-circulating the mixture through the enzymatic production zone.

    摘要翻译: 用于酶促生产甘油酯组合物的方法,特别是在工业上可行地生产甘油三酯,包括共轭亚油酸和亚麻酸甘油三酸酯,以及通过该方法制备的组合物。 首先使用酶反应区,其中甘油和脂肪酸或脂肪酸衍生物的混合物在酶催化剂的存在下反应以形成1,3-甘油二酯。 然后将混合物循环通过保持在较高温度的第二热重排区域,以促进1,3-甘油二酯重新配置为1,2-甘油二酯。 通过将混合物再循环通过酶促生产区产生甘油三酸酯。

    Process for enzymatic production of triglycerides
    6.
    发明授权
    Process for enzymatic production of triglycerides 有权
    酶促生产甘油三酯的方法

    公开(公告)号:US07759096B2

    公开(公告)日:2010-07-20

    申请号:US10585427

    申请日:2004-01-29

    IPC分类号: C12P7/64

    CPC分类号: C12P7/6472 C12P7/6454

    摘要: A process for enzymatic production of glyceride compositions, specifically industrially practicable production of triglycerides, including conjugated linoleic and linolenic acid triglycerides, and the compositions produced by such process. An enzymatic reaction zone is first utilized, in which a mixture of glycerol and fatty acids or fatty acid derivatives is reacted in the presence of an enzymatic catalyst to form 1,3 diglycerides. The mixture is then circulated through a second thermal rearrangement zone, maintained at a higher temperature, to promote rearrangement of the 1,3 diglycerides to 1,2 diglycerides. Triglycerides are produced by re-circulating the mixture through the enzymatic production zone.

    摘要翻译: 用于酶促生产甘油酯组合物的方法,特别是在工业上可行地生产甘油三酯,包括共轭亚油酸和亚麻酸甘油三酸酯,以及通过该方法制备的组合物。 首先使用酶反应区,其中甘油和脂肪酸或脂肪酸衍生物的混合物在酶催化剂的存在下反应以形成1,3-甘油二酯。 然后将混合物循环通过保持在较高温度的第二热重排区域,以促进1,3-甘油二酯重新配置为1,2-甘油二酯。 通过将混合物再循环通过酶促生产区产生甘油三酸酯。