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1.发明授权Catalysts having enhanced stability, efficiency and/or activity for alkylene oxide production 有权具有提高环氧烷生产的稳定性，效率和/或活性的催化剂公开(公告)号：US08765630B2
公开(公告)日：2014-07-01
申请号：US12713020
申请日：2010-02-25
CPC分类号： C07D301/10 , B01J21/066 , B01J23/50 , B01J23/66 , B01J23/686 , B01J23/688 , B01J35/1009 , B01J35/1042 , B01J35/1076 , B01J37/0018 , B01J37/0201 , B01J37/0203
摘要： A catalyst for the manufacture of alkylene oxide, for example ethylene oxide, by the vapor-phase epoxidation of alkene containing impregnated silver and at least one efficiency-enhancing promoter on an inert, refractory solid support, said support incorporating a sufficient amount of zirconium component (present and remaining substantially as zirconium silicate) as to enhance at least one of catalyst activity, efficiency and stability as compared to a similar catalyst which does not contain the zirconium component.
摘要翻译： 用于通过气相环氧化含烯烃的浸渍的银和至少一种在惰性耐火固体载体上的效率增强促进剂来制备环氧烷烃例如环氧乙烷的催化剂，所述载体包含足量的锆组分 （存在并基本上保持为硅酸锆），与不含锆组分的类似催化剂相比，可提高催化剂活性，效率和稳定性中的至少一种。
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2.发明授权Catalysts having enhanced stability, efficiency and/or activity for alkylene oxide production 有权具有提高环氧烷生产的稳定性，效率和/或活性的催化剂公开(公告)号：US08513156B2
公开(公告)日：2013-08-20
申请号：US12846984
申请日：2010-07-30
CPC分类号： C07D301/10 , B01J21/066 , B01J23/50 , B01J23/66 , B01J23/686 , B01J23/688 , B01J35/1009 , B01J35/1042 , B01J35/1076 , B01J37/0018 , B01J37/0201 , B01J37/0203
摘要： A catalyst for the manufacture of alkylene oxide, for example ethylene oxide, by the vapor-phase epoxidation of alkene containing impregnated silver and at least one efficiency-enhancing promoter on an inert, refractory solid support, said support incorporating a sufficient amount of zirconium component (present and remaining substantially as zirconium silicate) as to enhance at least one of catalyst activity, efficiency and stability as compared to a similar catalyst which does not contain the zirconium component.
摘要翻译： 用于通过气相环氧化含烯烃的浸渍的银和至少一种在惰性耐火固体载体上的效率增强促进剂来制备环氧烷烃例如环氧乙烷的催化剂，所述载体包含足量的锆组分 （存在并基本上保持为硅酸锆），与不含锆组分的类似催化剂相比，可提高催化剂活性，效率和稳定性中的至少一种。
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3.发明申请Catalysts Having Enhanced Stability, Efficiency and/or Activity For Alkylene Oxide Production 审中-公开具有增强的氧化亚烷基生产稳定性，效率和/或活性的催化剂公开(公告)号：US20090291847A1
公开(公告)日：2009-11-26
申请号：US12533322
申请日：2009-07-31
IPC分类号： B01J21/06
CPC分类号： C07D301/10 , B01J21/066 , B01J23/50 , B01J23/66 , B01J23/686 , B01J23/688 , B01J35/1009 , B01J35/1042 , B01J35/1076 , B01J37/0018 , B01J37/0201 , B01J37/0203
摘要： A catalyst for the manufacture of alkylene oxide, for example ethylene oxide, by the vapor-phase epoxidation of alkene containing impregnated silver and at least one efficiency-enhancing promoter on an inert, refractory solid support, said support incorporating a sufficient amount of zirconium component (present and remaining substantially as zirconium silicate) as to enhance at least one of catalyst activity, efficiency and stability as compared to a similar catalyst which does not contain the zirconium component.
摘要翻译： 用于通过气相环氧化含烯烃的浸渍的银和至少一种在惰性耐火固体载体上的效率增强促进剂来制备环氧烷烃例如环氧乙烷的催化剂，所述载体包含足量的锆组分 （存在并基本上保持为硅酸锆），与不含锆组分的类似催化剂相比，可提高催化剂活性，效率和稳定性中的至少一种。
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4.发明申请CATALYSTS HAVING ENHANCED STABILITY, EFFICIENCY AND/OR ACTIVITY FOR ALKYLENE OXIDE PRODUCTION 审中-公开具有增强的稳定性，有效和/或活性的烷基氧化铝生产的催化剂公开(公告)号：US20090275763A1
公开(公告)日：2009-11-05
申请号：US12476908
申请日：2009-06-02
IPC分类号： C07D301/03 , B01J23/02 , B01J23/58 , B01J21/06 , C07C29/17 , C07C41/00 , C07C291/00
CPC分类号： C07D301/10 , B01J21/066 , B01J23/50 , B01J23/66 , B01J23/686 , B01J23/688 , B01J35/1009 , B01J35/1042 , B01J35/1076 , B01J37/0018 , B01J37/0201 , B01J37/0203
摘要： A catalyst for the manufacture of alkylene oxide, for example ethylene oxide, by the vapor-phase epoxidation of alkene containing impregnated silver and at least one efficiency-enhancing promoter on an inert, refractory solid support, said support incorporating a sufficient amount of zirconium component (present and remaining substantially as zirconium silicate) as to enhance at least one of catalyst activity, efficiency and stability as compared to a similar catalyst which does not contain the zirconium component.
摘要翻译： 用于通过气相环氧化含烯烃的浸渍的银和至少一种在惰性耐火固体载体上的效率增强促进剂来制备环氧烷烃例如环氧乙烷的催化剂，所述载体包含足量的锆组分 （存在并基本上保持为硅酸锆），与不含锆组分的类似催化剂相比，可提高催化剂活性，效率和稳定性中的至少一种。
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5.发明申请CATALYSTS HAVING ENHANCED STABILITY, EFFICIENCY AND/OR ACTIVITY FOR ALKYLENE OXIDE PRODUCTION 有权具有增强的稳定性，有效和/或活性的烷基氧化铝生产的催化剂公开(公告)号：US20100173771A1
公开(公告)日：2010-07-08
申请号：US12713020
申请日：2010-02-25
CPC分类号： C07D301/10 , B01J21/066 , B01J23/50 , B01J23/66 , B01J23/686 , B01J23/688 , B01J35/1009 , B01J35/1042 , B01J35/1076 , B01J37/0018 , B01J37/0201 , B01J37/0203
摘要： A catalyst for the manufacture of alkylene oxide, for example ethylene oxide, by the vapor-phase epoxidation of alkene containing impregnated silver and at least one efficiency-enhancing promoter on an inert, refractory solid support, said support incorporating a sufficient amount of zirconium component (present and remaining substantially as zirconium silicate) as to enhance at least one of catalyst activity, efficiency and stability as compared to a similar catalyst which does not contain the zirconium component.
摘要翻译： 用于通过气相环氧化含烯烃的浸渍的银和至少一种在惰性耐火固体载体上的效率增强促进剂来制备环氧烷烃例如环氧乙烷的催化剂，所述载体包含足量的锆组分 （存在并基本上保持为硅酸锆），与不含锆组分的类似催化剂相比，可提高催化剂活性，效率和稳定性中的至少一种。
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6.发明授权公开(公告)号：US08845975B2
公开(公告)日：2014-09-30
申请号：US12974439
申请日：2010-12-21
申请人： William H. Henstock , Juliana G. Serafin , Albert C. Liu , Hwaili Soo , Yujun Liu , Manuk Colakyan , Sagar Petkar
发明人： William H. Henstock , Juliana G. Serafin , Albert C. Liu , Hwaili Soo , Yujun Liu , Manuk Colakyan , Sagar Petkar
IPC分类号： B01J8/00 , C07D301/03 , C07D301/10 , C07D301/36 , C07D301/32
CPC分类号： C07D301/10 , C07D301/32 , C07D301/36 , Y02P20/582
摘要： A plant and process for producing alkylene oxides to control the production of silver chloride on a high efficiency silver catalyst is disclosed and described. The process involves reacting an alkylene and an organic chloride gas phase promoter with oxygen over the high efficiency silver catalyst. The sulfur concentration in the alkylene oxide reactor feed is controlled to reduce the production of silver chloride which acts as a catalyst poison.
摘要翻译： 公开和描述了一种用于生产烯化氧以控制高效率银催化剂上的氯化银生产的设备和方法。 该方法包括在高效率银催化剂上使亚烷基和有机氯化物气相促进剂与氧反应。 控制环氧烷反应器进料中的硫浓度以减少作为催化剂毒物的氯化银的产生。
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7.发明申请公开(公告)号：US20110160470A1
公开(公告)日：2011-06-30
申请号：US12974439
申请日：2010-12-21
申请人： William H. Henstock , Juliana G. Serafin , Albert C. Liu , Hwaili Soo , Yujun Liu , Manuk Colakyan , Sagar Petkar
发明人： William H. Henstock , Juliana G. Serafin , Albert C. Liu , Hwaili Soo , Yujun Liu , Manuk Colakyan , Sagar Petkar
IPC分类号： C07D301/10 , B01D53/48 , B01J8/00 , B01D53/02
CPC分类号： C07D301/10 , C07D301/32 , C07D301/36 , Y02P20/582
摘要： A plant and process for producing alkylene oxides to control the production of silver chloride on a high efficiency silver catalyst is disclosed and described. The process involves reacting an alkylene and an organic chloride gas phase promoter with oxygen over the high efficiency silver catalyst. The sulfur concentration in the alkylene oxide reactor feed is controlled to reduce the production of silver chloride which acts as a catalyst poison.
摘要翻译： 公开和描述了一种用于生产烯化氧以控制高效率银催化剂上的氯化银生产的设备和方法。 该方法包括在高效率银催化剂上使亚烷基和有机氯化物气相促进剂与氧反应。 控制环氧烷反应器进料中的硫浓度以减少作为催化剂毒物的氯化银的产生。
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8.发明申请公开(公告)号：US20100267969A1
公开(公告)日：2010-10-21
申请号：US12760044
申请日：2010-04-14
申请人： Albert C. Liu , Hwaili Soo
发明人： Albert C. Liu , Hwaili Soo
IPC分类号： C07D317/36 , B01J27/055 , C07D301/10 , C07C29/00 , C07C213/04 , C07C41/03
CPC分类号： C07D301/10 , B01J21/04 , B01J23/6567 , B01J35/1009 , B01J35/1042 , B01J35/1076 , B01J37/0201 , B01J37/0203 , B01J37/0207 , B01J37/0213 , B01J37/26 , C07C29/00 , C07C41/03 , C07C213/04 , C07D317/36
摘要： The present invention provides rhenium-promoted epoxidation catalysts based upon shaped porous bodies comprising a minimized percentage of their total pore volume being present in pores having diameters of less than one micron, and a surface area of at least about 1.0 m2/g. Processes of making the catalysts and using them in epoxidation processes are also provided.
摘要翻译： 本发明提供了基于成形多孔体的铼促进的环氧化催化剂，其包含直径小于1微米，表面积至少约1.0m 2 / g的孔体积的最小百分比。 还提供了制备催化剂并将其用于环氧化方法中的方法。
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公开(公告)号：US20190118167A1
公开(公告)日：2019-04-25
申请号：US16176786
申请日：2018-10-31
申请人： Manuel A.W. Natal , Madan M. Bhasin , Hwaili Soo , Albert C. Liu
发明人： Manuel A.W. Natal , Madan M. Bhasin , Hwaili Soo , Albert C. Liu
IPC分类号： B01J27/055 , B01J23/58 , C07C209/60 , B01J37/02 , B01J35/02 , B01J23/68 , C07D301/10 , B01J23/50 , B01J21/04 , B01J37/16
摘要： A supported silver catalyst and use thereof in a process for producing an alkylene oxide, such as ethylene oxide, by the direct oxidation of an alkylene with oxygen or an oxygen-containing gas, wherein the catalyst provides improved stability and improved resilience to reactor upsets and timely recovery to substantially pre-upset levels of catalyst activity and/or efficiency. In some embodiments, the catalyst also exhibits improved activity. A catalyst capable of producing ethylene oxide at a selectivity of at least 87 percent while achieving a work rate of at least 184 kg/h/m3 at a temperature of no greater than 235° C. when operated in a process where the inlet feed to a reactor containing the catalyst comprises ethylene, oxygen, and carbon dioxide, wherein the concentration of carbon dioxide in the inlet feed is greater than or equal to 2 mole percent.
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公开(公告)号：US20160082423A9
公开(公告)日：2016-03-24
申请号：US13624131
申请日：2012-09-21
申请人： Manuel A. W. Natal , Madan M. Bhasin , Hwaili Soo , Albert C. Liu
发明人： Manuel A. W. Natal , Madan M. Bhasin , Hwaili Soo , Albert C. Liu
IPC分类号： B01J27/055 , B01J23/68 , C07D301/10 , C07C29/10 , B01J35/02 , C07C41/02 , B01J37/02 , B01J23/66 , C07C209/16
CPC分类号： B01J27/055 , B01J21/04 , B01J23/50 , B01J23/58 , B01J23/688 , B01J35/0013 , B01J35/006 , B01J35/023 , B01J37/0203 , B01J37/0205 , B01J37/0244 , B01J37/16 , C07C209/60 , C07D301/10 , Y02P20/52
摘要： A supported silver catalyst and use thereof in a process for producing an alkylene oxide, such as ethylene oxide, by the direct oxidation of an alkylene with oxygen or an oxygen-containing gas, wherein the catalyst provides improved stability and improved resilience to reactor upsets and timely recovery to substantially pre-upset levels of catalyst activity and/or efficiency. In some embodiments, the catalyst also exhibits improved activity. A catalyst capable of producing ethylene oxide at a selectivity of at least 87 percent while achieving a work rate of at least 184 kg/h/m3 at a temperature of no greater than 235° C. when operated in a process where the inlet feed to a reactor containing the catalyst comprises ethylene, oxygen, and carbon dioxide, wherein the concentration of carbon dioxide in the inlet feed is greater than or equal to 2 mole percent.
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