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    Method for producing a glass ceramic having a garnet phase
    4.
    发明授权
    Method for producing a glass ceramic having a garnet phase 有权
    具有石榴石相的玻璃陶瓷的制造方法

    公开(公告)号：US07958746B2

    公开(公告)日：2011-06-14

    申请号：US11757609

    申请日：2007-06-04

    申请人： Karine Seneschal-Merz ,  Bernd Hoppe ,  Dirk Sprenger ,  Friedrich Siebers ,  Martin Letz ,  Thilo Zachau

    发明人： Karine Seneschal-Merz ,  Bernd Hoppe ,  Dirk Sprenger ,  Friedrich Siebers ,  Martin Letz ,  Thilo Zachau

    IPC分类号： C03C10/00

    CPC分类号： C09K11/7774 ,  C03B32/02 ,  C03C10/0009 ,  C03C10/0054 ,  H01L33/501 ,  H01L33/502 ,  H01L2924/0002 ,  H01L2924/00

    摘要： The invention proposes a method for producing glass ceramics which is particularly well suited as light conversion material, especially for down conversion. One initially produces a starting glass, containing (on an oxide basis) 5-50% by weight of SiO2, 5-50% by weight of Al2O3 and 10-80% by weight of at least one oxide selected from the from the group formed by Y2O3, Lu2O3, Sc2O3, Gd2O3, Yb2O3, Ce2O3, as well as 0.1-30% by weight of at least one oxide selected from the group formed by B2O3, Th2O3, and oxides of the lanthanoids, except Lu2O3, Gd2O3, Yb2O3, Ce2O3. Thereafter, the material is heated up for ceramization at a heating rate of at least 100 K/min to a temperature in the range of between 1000° C. to 1400° C. until crystallites are formed that contain a garnet phase. Thereafter, the material is cooled down to room temperature. Alternatively, controlled cooling-down from the molten state is possible.

    摘要翻译： 本发明提出一种特别适合作为光转换材料的玻璃陶瓷的制造方法，特别是用于下转换。 最初产生起始玻璃，其含有5-50重量％的SiO 2，5-50重量％的Al 2 O 3和10-80重量％的至少一种氧化物的起始玻璃，所述氧化物选自由Y 2 O 3 ，Lu 2 O 3，Sc 2 O 3，Gd 2 O 3，Yb 2 O 3，Ce 2 O 3，以及选自B 2 O 3，Th 2 O 3的至少一种氧化物和除了Lu 2 O 3，Gd 2 O 3，Yb 2 O 3，Ce 2 O 3以外的镧系元素的氧化物的至少一种氧化物。 此后，将材料以至少100K /分钟的加热速率加热至陶瓷化，至1000℃至1400℃的温度，直至形成含有石榴石相的微晶。 此后，将材料冷却至室温。 或者，可以从熔融状态控制冷却。

    METHOD FOR PRODUCING A GLASS CERAMIC HAVING A GARNET PHASE
    5.
    发明申请
    METHOD FOR PRODUCING A GLASS CERAMIC HAVING A GARNET PHASE 有权
    用于生产具有GARNET相的玻璃陶瓷的方法

    公开(公告)号：US20080041106A1

    公开(公告)日：2008-02-21

    申请号：US11757609

    申请日：2007-06-04

    申请人： Karine Seneschal-Merz ,  Bernd Hoppe ,  Dirk Sprenger ,  Friedrich Siebers ,  Martin Letz ,  Thilo Zachau

    发明人： Karine Seneschal-Merz ,  Bernd Hoppe ,  Dirk Sprenger ,  Friedrich Siebers ,  Martin Letz ,  Thilo Zachau

    IPC分类号： C03B27/012 ,  C03C10/00

    CPC分类号： C09K11/7774 ,  C03B32/02 ,  C03C10/0009 ,  C03C10/0054 ,  H01L33/501 ,  H01L33/502 ,  H01L2924/0002 ,  H01L2924/00

    摘要： The invention proposes a method for producing glass ceramics which is particularly well suited as light conversion material, especially for down conversion. One initially produces a starting glass, containing (on an oxide basis) 5-50% by weight of SiO2, 5-50 % by weight of Al2O3 and 10-80% by weight of at least one oxide selected from the from the group formed by Y2O3, Lu2O3, Sc2O3, Gd2O3, Yb2O3, Ce2O3, as well as 0.1-30% by weight of at least one oxide selected from the group formed by B2O3, Th2O3, and oxides of the lanthanoids, except Lu2O3, Gd2O3, Yb2O3, Ce2O3. Thereafter, the material is heated up for ceramization at a heating rate of at least 100 K/min to a temperature in the range of between 1000° C. to 1400° C. until crystallites are formed that contain a garnet phase. Thereafter, the material is cooled down to room temperature. Alternatively, controlled cooling-down from the molten state is possible.

    摘要翻译： 本发明提出一种特别适合作为光转换材料的玻璃陶瓷的制造方法，特别是用于下转换。 最初产生起始玻璃，其含有（以氧化物为基准）5-50重量％的SiO 2，5-50重量％的Al 2 O 3 > 3重量％和10-80重量％的至少一种氧化物，其选自Y 2 N 3 O 3，Lu 2 3 3 3，3 3 3 3 ，Yb 2 O 3，Ce 2 O 3，以及0.1-30重量％的 选自由B 2 O 3 O 3，Th 2 O 3 3形成的基团中的至少一种氧化物和氧化物 的镧系元素，除了Lu 2 O 3 3，Gd 2 O 3 N 3，Yb 2， 3个O 3，3个O 3，3个O 3。 此后，将材料以至少100K /分钟的加热速率加热至陶瓷化，至1000℃至1400℃的温度，直至形成含有石榴石相的微晶。 此后，将材料冷却至室温。 或者，可以从熔融状态控制冷却。

    Highly transparent impact-resistant plate laminate and armored or bulletproof glass and articles made with same
    7.
    发明申请
    Highly transparent impact-resistant plate laminate and armored or bulletproof glass and articles made with same 审中-公开
    高度透明的耐冲击板层压板和装甲防弹玻璃以及与此相同的制品

    公开(公告)号：US20140162039A1

    公开(公告)日：2014-06-12

    申请号：US13709148

    申请日：2012-12-10

    申请人： Thilo Zachau ,  Friedrich Siebers ,  Ulrich Schiffner ,  Kurt Schaupert

    发明人： Thilo Zachau ,  Friedrich Siebers ,  Ulrich Schiffner ,  Kurt Schaupert

    IPC分类号： F41H5/04 ,  C03C14/00

    CPC分类号： F41H5/0407 ,  B32B17/10045 ,  B32B17/10119 ,  B32B17/10761 ,  B32B2333/12 ,  C03C3/085 ,  C03C10/0027

    摘要： The armored or bulletproof glass include a transparent plate laminate, which includes one or more transparent glass ceramic plates made from a green glass body of the Li2O—Al2O3—SiO2 system, optionally one or more additional plates made of plastic material, and optionally one or more glass plates. The glass ceramic plate preferably has a thermal expansion coefficient of −0.05×10−6/K to −0.10×10−6/K at 30 to 700° C. and a brightness value for transmitted normal light at an angle of 2°≧80 for a 4-mm thick plate. The transparent plate laminate preferably has a total of 4 to 8 plates and a thickness between 40 and 80 mm. A bulletproof vest, a fire prevention glazing, a fireplace viewing window pane, a cooktop, a magnetic storage plate or a substrate for semiconductor materials also advantageously include the transparent plate laminate described here.

    摘要翻译： 装甲防弹玻璃包括透明板层压板，其包括由Li 2 O-Al 2 O 3 -SiO 2系统的绿色玻璃体制成的一个或多个透明玻璃陶瓷板，任选地一个或多个由塑料材料制成的附加板，以及任选地一个或多个 更多的玻璃板。 优选在30〜700℃下，玻璃陶瓷板的热膨胀系数为-0.05×10-6 / K〜-0.10×10-6 / K，透射正常光的亮度值为2°≧ 80为4毫米厚板。 透明板层叠体优选总共为4〜8块，厚度为40〜80mm。 防弹背心，防火玻璃，壁炉观景窗，灶台，磁存储板或半导体材料用基板也有利地包括这里所述的透明板层压板。

    Highly transparent impact-resistant plate laminate and armored or bulletproof glass and articles made with same
    8.
    发明申请
    Highly transparent impact-resistant plate laminate and armored or bulletproof glass and articles made with same 审中-公开
    高度透明的耐冲击板层压板和装甲防弹玻璃以及与此相同的制品

    公开(公告)号：US20150132560A9

    公开(公告)日：2015-05-14

    申请号：US13709148

    申请日：2012-12-10

    申请人： Thilo Zachau ,  Friedrich Siebers ,  Ulrich Schiffner ,  Kurt Schaupert

    发明人： Thilo Zachau ,  Friedrich Siebers ,  Ulrich Schiffner ,  Kurt Schaupert

    IPC分类号： F41H5/04 ,  C03C14/00

    CPC分类号： F41H5/0407 ,  B32B17/10045 ,  B32B17/10119 ,  B32B17/10761 ,  B32B2333/12 ,  C03C3/085 ,  C03C10/0027

    摘要： The armored or bulletproof glass include a transparent plate laminate, which includes one or more transparent glass ceramic plates made from a green glass body of the Li2O—Al2O3—SiO2 system, optionally one or more additional plates made of plastic material, and optionally one or more glass plates. The glass ceramic plate preferably has a thermal expansion coefficient of −0.05×10−6/K to −0.10×10−6/K at 30 to 700° C. and a brightness value for transmitted normal light at an angle of 2°≧80 for a 4-mm thick plate. The transparent plate laminate preferably has a total of 4 to 8 plates and a thickness between 40 and 80 mm. A bulletproof vest, a fire prevention glazing, a fireplace viewing window pane, a cooktop, a magnetic storage plate or a substrate for semiconductor materials also advantageously include the transparent plate laminate described here.

    摘要翻译： 装甲或防弹玻璃包括透明板层压板，其包括由Li 2 O-Al 2 O 3 -SiO 2系统的绿色玻璃体制成的一个或多个透明玻璃陶瓷板，任选的一个或多个由塑料材料制成的附加板，以及任选的一个或 更多的玻璃板。 优选在30〜700℃下，玻璃陶瓷板的热膨胀系数为-0.05×10-6 / K〜-0.10×10-6 / K，透射正常光的亮度值为2°≧ 80为4毫米厚板。 透明板层叠体优选总共为4〜8块，厚度为40〜80mm。 防弹背心，防火玻璃，壁炉观景窗，灶台，磁存储板或半导体材料用基板也有利地包括这里所述的透明板层压板。

    Metal colloid-colored glass ceramic and colorless glass convertible into same
    10.
    发明申请
    Metal colloid-colored glass ceramic and colorless glass convertible into same 失效
    金属胶体色玻璃陶瓷和无色玻璃可转换为相同

    公开(公告)号：US20120283086A1

    公开(公告)日：2012-11-08

    申请号：US13550867

    申请日：2012-07-17

    申请人： Meike Schneider ,  Thilo Zachau ,  Friedrich Siebers ,  Wolfgang Schmidbauer

    发明人： Meike Schneider ,  Thilo Zachau ,  Friedrich Siebers ,  Wolfgang Schmidbauer

    IPC分类号： C03C6/00 ,  C03C6/02

    CPC分类号： C03C1/10 ,  C03C3/085 ,  C03C4/02 ,  C03C10/0027 ,  C03C10/0045 ,  C03C14/004 ,  C03C14/006 ,  C03C2214/20

    摘要： A colorless transparent colloid-former-containing glass that is convertible into a colorless transparent glass ceramic or a metal colloid-colored glass ceramic via respective heat treatments contains a combination of one or more metal colloid formers and one or more redox partners. The metal colloid formers are compounds containing Au, Ag, As, Bi, Nb, Cu, Fe, Pd, Pt, Sb and/or Sn. The redox partners are compounds containing As, Ce, Fe, Mn, Sb, Sn and/or W, with the proviso that the redox partner must be different from the metal colloid former.

    摘要翻译： 通过各自的热处理可转变为无色透明玻璃陶瓷或金属胶体色玻璃陶瓷的无色透明含胶体成分玻璃包含一种或多种金属胶体形成剂和一种或多种氧化还原配合物的组合。 金属胶体形成剂是含有Au，Ag，As，Bi，Nb，Cu，Fe，Pd，Pt，Sb和/或Sn的化合物。 氧化还原配体是含有As，Ce，Fe，Mn，Sb，Sn和/或W的化合物，条件是氧化还原对象必须与金属胶体形成体不同。