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1.发明申请SILICA CRUCIBLE WITH PURE AND BUBBLE FREE INNER CRUCIBLE LAYER AND METHOD OF MAKING THE SAME 失效二氧化硅与纯净和无泡内部可溶层的可溶性及其制备方法公开(公告)号：US20100154701A1
公开(公告)日：2010-06-24
申请号：US12370517
申请日：2009-02-12
CPC分类号： C03B19/095 , Y10T117/1032
摘要： A method of making a silica crucible in a mold cavity of the type in which air is drawing through silica grain placed in the mold cavity. A pure silica grain layer is formed on top of a natural silica grain layer. At least a portion of the purse silica grain layer is fused while substantially no air is drawn through the silica grain. Any remaining pure silica grain and a least a portion of the natural silica grain layer is fused while drawing a substantially higher volume of air through the silica. At least a portion of the fused pure silica grain layer is then sublimated.
摘要翻译： 一种将二氧化硅坩埚制成在通过置于模腔中的二氧化硅颗粒吸入空气的类型的模腔中的方法。 在天然二氧化硅颗粒层的顶部形成纯二氧化硅颗粒层。 将二氧化硅颗粒层的至少一部分熔融，而基本上没有空气通过二氧化硅颗粒。 任何剩余的纯二氧化硅颗粒和至少一部分天然二氧化硅颗粒层在通过二氧化硅吸收大体积的空气的同时被熔化。 然后将熔融的纯二氧化硅颗粒层的至少一部分升华。
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公开(公告)号：US20110123738A1
公开(公告)日：2011-05-26
申请号：US12623140
申请日：2009-11-20
CPC分类号： C03B19/095 , Y10T428/131
摘要： A silica crucible is made in a mold cavity of the type in which ambient atmosphere can be drawn through silica grain in the cavity. In one embodiment, a silica grain layer is formed in the mold cavity and gas, which may comprise helium, nitrogen, hydrogen, or a mixture thereof, is introduced into the mold cavity. The silica grain layer is heated while substantially no ambient atmosphere is drawn through the silica grain. Thereafter, at least a portion of the silica grain layer is fused while drawing ambient atmosphere through the silica grain. The gas displaces air in the mold cavity thereby reducing nitrogen oxides and ozone.
摘要翻译： 一种二氧化硅坩埚制成在这样的模腔中，其中环境气氛可以通过空腔中的二氧化硅颗粒被吸入。 在一个实施例中，在模腔中形成二氧化硅颗粒层，并且可以将包含氦，氮，氢或其混合物的气体引入模腔中。 加热二氧化硅颗粒层，同时基本上没有环境气氛通过二氧化硅颗粒。 此后，将二氧化硅粒子层的至少一部分熔融，同时通过二氧化硅粒子吸收环境气氛。 气体置换模腔中的空气，从而减少氮氧化物和臭氧。
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3.发明授权Silica crucible with pure and bubble free inner crucible layer and method of making the same 失效具有纯净和无气泡的内坩埚层的二氧化硅坩埚及其制造方法公开(公告)号：US08272234B2
公开(公告)日：2012-09-25
申请号：US12370517
申请日：2009-02-12
CPC分类号： C03B19/095 , Y10T117/1032
摘要： A method of making a silica crucible in a mold cavity of the type in which air is drawing through silica grain placed in the mold cavity. A pure silica grain layer is formed on top of a natural silica grain layer. At least a portion of the purse silica grain layer is fused while substantially no air is drawn through the silica grain. Any remaining pure silica grain and a least a portion of the natural silica grain layer is fused while drawing a substantially higher volume of air through the silica. At least a portion of the fused pure silica grain layer is then sublimated.
摘要翻译： 一种将二氧化硅坩埚制成在通过置于模腔中的二氧化硅颗粒吸入空气的类型的模腔中的方法。 在天然二氧化硅颗粒层的顶部形成纯二氧化硅颗粒层。 将二氧化硅颗粒层的至少一部分熔融，而基本上没有空气通过二氧化硅颗粒。 任何剩余的纯二氧化硅颗粒和至少一部分天然二氧化硅颗粒层在通过二氧化硅吸收大体积的空气的同时被熔化。 然后将熔融的纯二氧化硅颗粒层的至少一部分升华。
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公开(公告)号：US09003832B2
公开(公告)日：2015-04-14
申请号：US12623140
申请日：2009-11-20
IPC分类号： C03B19/09
CPC分类号： C03B19/095 , Y10T428/131
摘要： A silica crucible is made in a mold cavity of the type in which ambient atmosphere can be drawn through silica grain in the cavity. In one embodiment, a silica grain layer is formed in the mold cavity and gas, which may comprise helium, nitrogen, hydrogen, or a mixture thereof, is introduced into the mold cavity. The silica grain layer is heated while substantially no ambient atmosphere is drawn through the silica grain. Thereafter, at least a portion of the silica grain layer is fused while drawing ambient atmosphere through the silica grain. The gas displaces air in the mold cavity thereby reducing nitrogen oxides and ozone.
摘要翻译： 一种二氧化硅坩埚制成在这样的模腔中，其中环境气氛可以通过空腔中的二氧化硅颗粒被吸入。 在一个实施方案中，在模腔中形成二氧化硅颗粒层，并且将可能包含氦，氮，氢或其混合物的气体引入模腔中。 加热二氧化硅颗粒层，同时基本上没有环境气氛通过二氧化硅颗粒。 此后，将二氧化硅粒子层的至少一部分熔融，同时通过二氧化硅粒子吸收环境气氛。 气体置换模腔中的空气，从而减少氮氧化物和臭氧。
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5.发明授权公开(公告)号：US08496752B2
公开(公告)日：2013-07-30
申请号：US12552960
申请日：2009-09-02
IPC分类号： C30B15/02
CPC分类号： C30B15/10 , C30B35/002 , Y10T117/1052 , Y10T117/106 , Y10T117/1068
摘要： During a CZ or similar process, a silica crucible is held in a graphite or similar susceptor while being heated to above between about 1580 and 1620 degrees C. Vents or grooves formed in at least one of the outer surface of the crucible and the inner surface of the susceptor permit gasses to vent upwardly and out from between the crucible and susceptor. This permits gas evolved from the crucible as a result of the heat to be vented rather than expanding between the crucible and susceptor thereby deforming the crucible.
摘要翻译： 在CZ或类似的过程中，将石英坩埚保持在石墨或类似的基座中，同时被加热到大约在1580和1620摄氏度之间。形成在坩埚的外表面和内表面中的至少一个中的通风口 的基座允许气体从坩埚和基座之间向上排出。 这允许通过排出热量而不是在坩埚和基座之间膨胀从坩埚中逸出的气体，从而使坩埚变形。
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6.发明申请公开(公告)号：US20110048315A1
公开(公告)日：2011-03-03
申请号：US12552960
申请日：2009-09-02
CPC分类号： C30B15/10 , C30B35/002 , Y10T117/1052 , Y10T117/106 , Y10T117/1068
摘要： During a CZ or similar process, a silica crucible is held in a graphite or similar susceptor while being heated to above between about 1580 and 1620 degrees C. Vents or grooves formed in at least one of the outer surface of the crucible and the inner surface of the susceptor permit gasses to vent upwardly and out from between the crucible and susceptor. This permits gas evolved from the crucible as a result of the heat to be vented rather than expanding between the crucible and susceptor thereby deforming the crucible.
摘要翻译： 在CZ或类似的过程中，将石英坩埚保持在石墨或类似的基座中，同时被加热到大约在1580和1620摄氏度之间。形成在坩埚的外表面和内表面中的至少一个中的通风口 的基座允许气体从坩埚和基座之间向上排出。 这允许通过排出热量而不是在坩埚和基座之间膨胀从坩埚中逸出的气体，从而使坩埚变形。
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