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63 条记录 (耗时 0.033 秒)

    Process for producing 2-(halomethyl)phenylacetic acid esters
    1.
    发明授权
    Process for producing 2-(halomethyl)phenylacetic acid esters 失效
    2-（卤代甲基）苯乙酸酯的制备方法

    公开(公告)号：US5886211A

    公开(公告)日：1999-03-23

    申请号：US981449

    申请日：1998-03-18

    申请人： Kenji Hirai ,  Katsuyuki Masuda ,  Yoshihiro Takao ,  Masahide Sugiyama ,  Yukio Ono ,  Masahumi Matsuzawa

    发明人： Kenji Hirai ,  Katsuyuki Masuda ,  Yoshihiro Takao ,  Masahide Sugiyama ,  Yukio Ono ,  Masahumi Matsuzawa

    IPC分类号： C07C67/24 ,  C07C69/65 ,  C07D311/76 ,  C07C69/76

    CPC分类号： C07D311/76 ,  C07C67/24 ,  C07C69/65

    摘要： 2-(Halomethyl)phenylacetic acid esters (3) which are useful as intermediates for producing agricultural fungicides are produced efficiently and conveniently by reacting a 3-isochromanone derivative (1) with a hydrogen halide and an alcohol or reacting (1) with a halomethyl alkyl ether and then reacting the product with an alcohol in the presence of a base. The starting compound, 3-isochromanone (1), is produced in good yield by reacting an .alpha.,.alpha.'-o-xylene dihalide (4) with carbon monoxide and water in an organic solvent in the presence of a palladium catalyst and an inorganic base and then treating the product with an acid. ##STR1##

    摘要翻译： PCT No.PCT / JP96 / 01677 Sec。 371日期1998年3月18日 102（e）1998年3月18日PCT PCT 1996年6月19日PCT公布。 公开号WO97 / 00850 PCT 日本1 9 9 2年1月9日 - 用于制备农药杀菌剂的中间体的（卤代甲基）苯乙酸酯（3）通过使3-异色满酮衍生物（1）与卤化氢和醇反应（或 1）与卤代甲基烷基醚反应，然后在碱的存在下使产物与醇反应。 通过使α，α'-二甲苯二卤化物（4）与一氧化碳和水在有机溶剂中在钯催化剂和无机物存在下反应，以良好的产率制备起始化合物3-异色满酮（1） 然后用酸处理产物。 + TR

    Process for the preparation of 3-(substituted phenyl)-5-alkylidene-1,3-oxazolidine-2,4-dione derivatives
    2.
    发明授权
    Process for the preparation of 3-(substituted phenyl)-5-alkylidene-1,3-oxazolidine-2,4-dione derivatives 失效
    3-（取代苯基）-5-亚烷基-1,3-恶唑烷-2,4-二酮衍生物的制备方法

    公开(公告)号：US6090946A

    公开(公告)日：2000-07-18

    申请号：US894655

    申请日：1997-12-15

    申请人： Kenji Hirai ,  Katsuyuki Masuda ,  Tomoyuki Yano ,  Ryuta Ohno ,  Tomoko Matsukawa ,  Kiyomi Imai ,  Natsuko Okano ,  Tomoko Yoshii ,  Takehito Mouri

    发明人： Kenji Hirai ,  Katsuyuki Masuda ,  Tomoyuki Yano ,  Ryuta Ohno ,  Tomoko Matsukawa ,  Kiyomi Imai ,  Natsuko Okano ,  Tomoko Yoshii ,  Takehito Mouri

    IPC分类号： C07C67/31 ,  C07D263/44

    CPC分类号： C07D263/44 ,  C07C67/31

    摘要： The present invention provides an industrial process for efficiently preparing a 3-(substituted phenyl)-5-isopropylidene-1,3-oxazolidine-2,4-dione derivative having a potent herbicidal activity without using phosgene or the like. The present invention relates to a process for preparing a 3-(substituted phenyl)-5-alkylidene-1,3-oxazolidine-2,4-dione derivative represented by general formula (III), which comprises reaction of an N-(substituted phenyl)carbamate represented by general formula (I) with a 2-hydroxy-3-alkenoate represented by-general formula (II) or with a 3-alkoxy-2-hydroxyalkanoate represented by general formula (IV): ##STR1## (wherein Ar is a substituted phenyl group, R.sup.1 is an alkyl group having a carbon number of from 1 to 6, R.sup.2 and R.sup.3 are independently hydrogen atoms or alkyl groups having carbon numbers of from 1 to 12, and R.sup.4 and R.sup.5 are independently alkyl groups having carbon numbers of from 1 to 6).

    摘要翻译： PCT No.PCT / JP96 / 00430 Sec。 371 1997年12月15日第 102（e）日期1997年12月15日PCT提交1996年2月26日PCT公布。 公开号WO96 / 26930 PCT。 日本1996年9月6日本发明提供了一种不使用光气等有效制备具有强效除草活性的3-（取代苯基）-5-异亚丙基-1,3-恶唑烷-2,4-二酮衍生物的工业方法 。 本发明涉及一种制备由通式（III）表示的3-（取代苯基）-5-亚烷基-1,3-恶唑烷-2,4-二酮衍生物的方法，该方法包括N-（取代的 苯基）氨基甲酸酯与由通式（II）表示的2-羟基-3-烯酸酯或由通式（IV）表示的3-烷氧基-2-羟基链烷酸酯反应：（其中Ar为 取代的苯基，R1是碳数为1至6的烷基，R2和R3独立地为氢原子或碳数为1至12的烷基，R4和R5独立地为碳数为 从1到6）。

    Pyrazole-1-carboxylate derivatives, process for the production thereof and process for the production of pyrazole derivatives
    4.
    发明授权
    Pyrazole-1-carboxylate derivatives, process for the production thereof and process for the production of pyrazole derivatives 失效
    吡唑-1-羧酸酯衍生物，其制备方法和吡唑衍生物的制备方法

    公开(公告)号：US07767827B2

    公开(公告)日：2010-08-03

    申请号：US11915016

    申请日：2006-05-22

    申请人： Atsushi Uchida ,  Wakako Yokota ,  Kenji Hirai ,  Tomoyuki Yano

    发明人： Atsushi Uchida ,  Wakako Yokota ,  Kenji Hirai ,  Tomoyuki Yano

    IPC分类号： C07D231/10

    CPC分类号： C07D231/20

    摘要： Disclosed are pyrazole-1-carboxylate derivatives of the general formula (1), (wherein symbols are as defined in the specification), a process for the production thereof and processes for producing herbicidally active 3-aryloxypyrazole-1-carboxamide derivatives from the above compound and an intermediate therefor. According to this invention, there can be industrially advantageously produced 3-aryloxypyrazole-1-carboxamide derivatives that does not cause chemical damage on crops but exhibits excellent herbicidal activity against weeds that impair the growth of such crops.

    摘要翻译： 公开了通式（1）的吡唑-1-羧酸酯衍生物（其中符号如说明书中所定义），其制备方法和从上述产生除草活性3-芳氧基吡唑-1-甲酰胺衍生物的方法 化合物及其中间体。 根据本发明，可以在工业上有利地生产不对作物造成化学损害的3-芳氧基吡唑-1-甲酰胺衍生物，但是对于损害这些作物生长的杂草显示出优异的除草活性。

    THERMOSENSITIVE RECORDING MEDIUM
    5.
    发明申请
    THERMOSENSITIVE RECORDING MEDIUM 失效
    耐热记录介质

    公开(公告)号：US20100062935A1

    公开(公告)日：2010-03-11

    申请号：US12593116

    申请日：2008-03-14

    申请人： Ken Takagi ,  Jun Makihara ,  Akihito Ogino ,  Kenji Hirai ,  Makoto Hasegawa ,  Shin Suzuki ,  Takeshi Hirose

    发明人： Ken Takagi ,  Jun Makihara ,  Akihito Ogino ,  Kenji Hirai ,  Makoto Hasegawa ,  Shin Suzuki ,  Takeshi Hirose

    IPC分类号： B41M5/323

    CPC分类号： B41M5/3372 ,  B41M5/44 ,  B41M2205/04 ,  B41M2205/40

    摘要： The present invention presents a thermosensitive recording medium having excellent color development, image quality and preservation properties as well as excellent stamp receptivity, anti-scratching ability, printability and water blocking resistance.The present invention is a thermosensitive recording medium having a thermosensitive recording layer comprising at least a colorless or pale colored basic leuco dye and an electron accepting developing agent as a coating layer on a substrate, wherein at least an outermost layer among the thermosensitive recording layer and other optionally prepared coated layers contains rice starch particles.

    摘要翻译： 本发明提供了具有优异的显色性，图像质量和保存性以及优异的印模接受性，抗刮擦能力，可印刷性和耐水粘性的热敏记录介质。 本发明是一种热敏记录介质，其具有热敏记录层，该热敏记录层至少包含无色或浅色的碱性无色染料和作为涂层的电子接受显影剂，其中至少在热敏记录层和 其它任选制备的涂层含有米淀粉颗粒。

    Laser Recording Thermally Sensitive Recording Medium
    6.
    发明申请
    Laser Recording Thermally Sensitive Recording Medium 审中-公开

    公开(公告)号：US20080194403A1

    公开(公告)日：2008-08-14

    申请号：US10585895

    申请日：2005-01-13

    申请人： Junpei Natsui ,  Yoshihide Kimura ,  Kenji Hirai

    发明人： Junpei Natsui ,  Yoshihide Kimura ,  Kenji Hirai

    IPC分类号： B41M5/30

    CPC分类号： B41M5/3375 ,  B41M5/465

    摘要： A laser recording thermally sensitive recording medium comprising, at least a photo absorbing material which absorbs laser ray and covert the laser ray to heat, colorless or pale colored basic leuco dye and organic color developing agent on a substrate as main components, wherein said photo absorbing material is a compound represented by general formula (1), wherein, n indicates an integer of from 1 to 4, and structural formula of Xn, Yn and Zn− are indicated in Table 1. TABLE 1 n = 1n = 2 XnN(C2H5)2N(C2H5)2 YnN(C2H5)2N(C2H5)2 Zn− n = 3n = 4 XnN(CH3)2N(C2H5)2 YnHOCH3 Zn−CF3SO3−CF3SO3−

    Thermally Sensitive Recording Medium
    8.
    发明申请
    Thermally Sensitive Recording Medium 失效
    热敏记录介质

    公开(公告)号：US20070231513A1

    公开(公告)日：2007-10-04

    申请号：US10564808

    申请日：2004-07-16

    申请人： Mizuho Shimoyama ,  Kaoru Hamada ,  Seiki Yoneshige ,  Kenji Hirai

    发明人： Mizuho Shimoyama ,  Kaoru Hamada ,  Seiki Yoneshige ,  Kenji Hirai

    IPC分类号： B41M5/30

    CPC分类号： B41M5/42 ,  B41M5/3372

    摘要： Provision of a thermally sensitive recording medium comprising an undercoating layer containing a pigment and a binder as main components and a thermally sensitive color developing layer containing colorless or pale colored basic leuco dye and a color developing agent which develops color by reacting with said basic leuco dye as main components on a substrate, wherein said undercoating layer contains a water-retention agent and a pigment whose oil absorbing capacity prescribed by JIS K 5105 is from 80 cc/100 g to 120 cc/100 g as a pigment, further solid concentration of a coating for the undercoating layer is from 25% to 45% and dynamic water-retention capacity, which is Water retention measured with AA-GWR, is 350 g/m2 or less.

    摘要翻译： 提供热敏记录介质，其包含含有颜料和粘合剂作为主要成分的底涂层和含有无色或浅色的碱性无色染料的热敏显色层和通过与所述碱性无色染料反应而显色的彩色显影剂 作为基材上的主要组分，其中所述底涂层含有保水剂和由JIS K 5105规定的吸油能力为80cc / 100g至120cc / 100g的颜料作为颜料，进一步固体浓度 底涂层的涂层为25％〜45％，动态保水性为用AA-GWR测定的保水性为350g / m 2以下。