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    PRODUCTION METHOD FOR LIQUID CRYSTAL POLYESTER
    3.
    发明申请
    PRODUCTION METHOD FOR LIQUID CRYSTAL POLYESTER 审中-公开
    液晶聚酯的生产方法

    公开(公告)号：US20140088287A1

    公开(公告)日：2014-03-27

    申请号：US14111035

    申请日：2012-04-12

    申请人： Kiichiro Nishimura ,  Lu Shi ,  Satoshi Murouchi

    发明人： Kiichiro Nishimura ,  Lu Shi ,  Satoshi Murouchi

    IPC分类号： C08G63/80

    CPC分类号： C08G63/80 ,  C08G63/605 ,  C09K19/3809

    摘要： A method for producing a liquid crystal polyester according to the present invention is a method for producing a liquid crystal polyester, comprising subjecting a composition in which a dicarboxylic acid compound, a hydroxycarboxylic acid compound, and a dihydroxy compound are contained to melt polycondensation, and subjecting an obtained reaction product to solid phase polycondensation, wherein the composition contains, based on a total of the dicarboxylic acid compound, the hydroxycarboxylic acid compound, and the dihydroxy compound, 2 to 30 mole % of a dicarboxylic acid compound represented by the following formula (1), and 40 to 80 mole % of p-hydroxybenzoic acid, a polycondensation temperature of the above melt polycondensation is 315° C. or less, and a polycondensation temperature of the above solid phase polycondensation is 315° C. or less.

    摘要翻译： 本发明的液晶聚酯的制造方法是一种液晶聚酯的制造方法，其特征在于，将含有二羧酸化合物，羟基羧酸化合物和二羟基化合物的组合物进行熔融缩聚， 将得到的反应产物进行固相缩聚，其中所述组合物以所述二羧酸化合物的总计含有羟基羧酸化合物和二羟基化合物，含有2〜30摩尔％的下式所示的二羧酸化合物 （1）和40〜80摩尔％的对羟基苯甲酸，上述熔融缩聚的缩聚温度为315℃以下，上述固相缩聚的缩聚温度为315℃以下。

    LIQUID CRYSTAL POLYESTER RESIN COMPOSITION FOR CAMERA MODULE
    5.
    发明申请
    LIQUID CRYSTAL POLYESTER RESIN COMPOSITION FOR CAMERA MODULE 有权
    液晶模块的液晶聚酯树脂组合物

    公开(公告)号：US20110114883A1

    公开(公告)日：2011-05-19

    申请号：US12933808

    申请日：2009-03-24

    申请人： Satoshi Murouchi ,  Toshio Nakayama ,  Toru Kitai

    发明人： Satoshi Murouchi ,  Toshio Nakayama ,  Toru Kitai

    IPC分类号： C09K19/06

    CPC分类号： G03B9/08 ,  C08K3/04 ,  C08K7/14 ,  C08K7/26 ,  C08K7/28 ,  C08L67/00

    摘要： A liquid crystal polyester resin composition includes, based on 100 parts by mass of a liquid crystal polyester, 15 to 60 parts by mass of talc having a number average particle size of 10 to 50 μm, 25 to 50 parts by mass of a glass fiber having a number average fiber length of 100 to 200 μm and a number average fiber diameter of 4 to 8 μm, and 2 to 10 parts by mass of carbon black, wherein a melt viscosity as determined at a shear rate of 100 sec−1 at 370° C. is 10 to 100 Pa·S and a deflection temperature under load is 220° C. or more. The liquid crystal polyester resin composition is used to provide a liquid crystal polyester resin composition for a camera module, having good heat resistance, rigidity, strength, and moldability, and also an excellent surface exfoliation property in a well balanced manner and being capable of being surface mounted (SMT).

    摘要翻译： 液晶聚酯树脂组合物包含基于100质量份的液晶聚酯，15至60质量份数均粒径为10至50μm的滑石，25至50质量份的玻璃纤维 数均纤维长度为100〜200μm，数均纤维直径为4〜8μm，炭黑为2〜10质量份，其中，剪切速度为100sec -1时的熔体粘度为 370℃为10〜100Pa·S，负载挠曲温度为220℃以上。 液晶聚酯树脂组合物用于提供相机模块的液晶聚酯树脂组合物，具有良好的耐热性，刚性，强度和成型性，并且还具有良好平衡的优异的表面剥离性能，并且能够 表面贴装（SMT）。

    WHOLLY AROMATIC LIQUID CRYSTAL POLYESTER COMPOSITION AND OPTICAL PICKUP LENS HOLDER USING SAME
    6.
    发明申请
    WHOLLY AROMATIC LIQUID CRYSTAL POLYESTER COMPOSITION AND OPTICAL PICKUP LENS HOLDER USING SAME 有权
    全自动液晶聚合物组合物和使用相同的光学撷取镜头保持器

    公开(公告)号：US20100065777A1

    公开(公告)日：2010-03-18

    申请号：US12307025

    申请日：2007-06-28

    申请人： Satoshi Murouchi ,  Toshio Nakayama

    发明人： Satoshi Murouchi ,  Toshio Nakayama

    IPC分类号： C09K19/12

    CPC分类号： C08K7/14 ,  C08K2201/016 ,  C08L67/03

    摘要： A wholly aromatic liquid crystal polyester resin composition for injection molding, formed by melt-kneading 100 parts by mass of a wholly aromatic liquid crystal polyester resin, and 5 to 20 parts by mass of glass fibers having a number average diameter of 5 to 20 μm and an aspect ratio of 5 or more, the wholly aromatic liquid crystal polyester resin being formed by polycondensation of 60 to 70 mol % of p-hydroxybenzoic acid, 40 to 30 mol % of terephthalic acid and 4,4′-dihydroxydiphenyl combined, and 0 to 5 mol % of isophthalic acid and/or terephthalic acid (for all of these, derivatives thereof are included, and the total of these is 100 mol %). This composition has excellent damping properties, and is suitable for a molding material of an optical pickup lens holder for short type pickups for use in high-speed DVD systems and playback pickups for use in Blu-ray systems.

    摘要翻译： 将100质量份全芳香族液晶聚酯树脂熔融混炼，5〜20质量份数均粒径为5〜20μm的玻璃纤维进行注射成型的全芳香族液晶聚酯树脂组合物 纵横比为5以上，全芳香族液晶聚酯树脂通过缩聚60〜70摩尔％的对羟基苯甲酸，40〜30摩尔％的对苯二甲酸和4,4'-二羟基二苯基组合而形成，以及 0〜5摩尔％的间苯二甲酸和/或对苯二甲酸（其中包括所有这些衍生物，总共为100摩尔％）。 该组合物具有优异的阻尼性能，适用于用于高速DVD系统的短型拾音器的光学拾取透镜保持器和用于蓝光系统的回放拾取器的成型材料。

    Wholly Aromatic Thermotropic Liquid Crystal Polyester Resin Composition, Injection Molded Article Thereof, and Optical Device Using the Molded Article
    7.
    发明申请
    Wholly Aromatic Thermotropic Liquid Crystal Polyester Resin Composition, Injection Molded Article Thereof, and Optical Device Using the Molded Article 有权
    全芳香族热致变液晶聚酯树脂组合物，注射成型品及使用成型品的光学装置

    公开(公告)号：US20090250662A1

    公开(公告)日：2009-10-08

    申请号：US12225567

    申请日：2007-03-22

    申请人： Satoshi Murouchi ,  Toshio Nakayama

    发明人： Satoshi Murouchi ,  Toshio Nakayama

    IPC分类号： C09K19/06

    CPC分类号： C08K9/02 ,  H01L33/60 ,  Y10T428/10 ,  C08L67/00

    摘要： Disclosed is a resin composition produced by melt-kneading a white pigment and a wholly aromatic thermotropic liquid crystal polyester. The resin composition can retain the excellent heat resistance and moldability of the wholly aromatic thermotropic liquid crystal polyester and have a satisfactory level of white light reflectance. The resin composition comprises 35 to 100 parts by weight of a white pigment particle and 100 parts by weight of a wholly aromatic thermotropic liquid crystal polyester, wherein the white pigment particle comprises 3 to 15 mass % of aluminum oxide and 97 to 85 mass % of a white pigment produced by a process including a roasting step and having a surface treated with the aluminum oxide (provided that the sum total of the white pigment and aluminum oxide is defined as 100 mass %). The resin composition can be produced by a process including a melt-kneading step.

    摘要翻译： 公开了通过将白色颜料和全芳族热致变液晶聚酯熔融捏合而制得的树脂组合物。 树脂组合物可以保持全芳族热致变液晶聚酯的优异的耐热性和成型性，并且具有令人满意的白光反射率。 该树脂组合物包含35-100重量份白色颜料颗粒和100重量份全芳族热致液晶聚酯，其中白色颜料颗粒包含3-15质量％的氧化铝和97-85质量％的 通过包括焙烧步骤并具有用氧化铝处理的表面（条件是白色颜料和氧化铝的总和定义为100质量％）的方法生产的白色颜料。 树脂组合物可以通过包括熔融捏合步骤的方法制备。

    Method of producing thermotropic liquid crystalline copolyester, thermotropic liquid crystalline copolyester composition obtained by the same method, and molding made of the same composition
    8.
    发明授权
    Method of producing thermotropic liquid crystalline copolyester, thermotropic liquid crystalline copolyester composition obtained by the same method, and molding made of the same composition 失效
    制造热致液晶共聚酯的方法，通过相同方法获得的热致液晶共聚酯组合物和由相同组成制成的模制品

    公开(公告)号：US06296950B2

    公开(公告)日：2001-10-02

    申请号：US09809520

    申请日：2001-03-15

    申请人： Satoshi Murouchi ,  Yoshikuni Yamada ,  Toshitaka Kobayashi

    发明人： Satoshi Murouchi ,  Yoshikuni Yamada ,  Toshitaka Kobayashi

    IPC分类号： B32B1508

    CPC分类号： C08K5/524 ,  C08G63/605 ,  C08G63/80 ,  Y10T428/12007 ,  Y10T428/12528 ,  Y10T428/12569 ,  Y10T428/31681 ,  Y10T428/31786 ,  Y10T428/31989 ,  C08L67/00

    摘要： A method of producing a thermotropic liquid crystalline copolyester having an extremely small amount of out-gases comprising the steps of: (1) charging in a reactor 5-100 mol % of aromatic hydroxycarboxylic acid, 0-47.5 mol % of aromatic dicarboxylic acid and 0-47.5 mol % of aromatic diol, so that the sum of mol % of each material is 100 mol % and the molt of aromatic dicarboxylic acid and that of aromatic diol are substantially equal; (2) adding acetic anhydride of an amount which satisfies the formula, (B-C)/A≧1.04, “A” representing the total molar number of the hydroxy group in a reaction system, “B” representing the molar number of acetic anhydride to be added, and “C” representing the molar number of water present in the reaction system prior to addition of acetic anhydride; (3) acetylation; (4) melt polymerization; and (5) solid-phase polymerization.

    摘要翻译： 一种制造具有极少量外排气体的热致液晶共聚酯的方法，包括以下步骤：（1）在反应器中装入5-100摩尔％的芳族羟基羧酸，0-47.5摩尔％的芳族二羧酸和 0-47.5摩尔％的芳族二醇，使得每种材料的摩尔％的总和为100摩尔％，芳族二羧酸和芳族二醇的摩尔数基本相等; （2）加入满足式（BC）/ A> = 1.04的量的乙酸酐，表示反应体系中羟基的总摩尔数的“A”，代表乙酸酐摩尔数的“B” 并且“C”表示在加入乙酸酐之前反应体系中存在的水的摩尔数; （3）乙酰化; （4）熔融聚合; 和（5）固相聚合。

    Liquid crystal polyester resin composition for camera module
    10.
    发明授权
    Liquid crystal polyester resin composition for camera module 有权
    相机模组用液晶聚酯树脂组合物

    公开(公告)号：US08192645B2

    公开(公告)日：2012-06-05

    申请号：US12933967

    申请日：2009-03-24

    申请人： Satoshi Murouchi ,  Toshio Nakayama ,  Toru Kitai

    发明人： Satoshi Murouchi ,  Toshio Nakayama ,  Toru Kitai

    IPC分类号： C09K19/38 ,  C09K19/52 ,  C09K19/20 ,  C09K19/54 ,  C08K3/04 ,  C08K3/34 ,  C08K3/40

    CPC分类号： H04N5/2251 ,  C08K3/04 ,  C08K3/22 ,  C08K7/28 ,  C08L67/03 ,  C09K19/3809 ,  G03B9/00 ,  H04N5/2257

    摘要： A resin composition for surface-mountable (SMT) camera modules which is excellent in the balance between heat resistance, rigidity, strength or moldability and surface exfoliation characteristics is provided by using a liquid-crystal polyester resin composition which comprises 100 parts by mass of a liquid-crystal polyester, 15 to 60 parts by mass of talc having a number-mean particle diameter of 10 to 50 μm, 25 to 50 parts by mass of glass fiber having a number-mean fiber length of 100 to 200 μm, 6 to 20 parts by mass of titanium oxide, and 2 to 10 parts by mass of carbon black and which exhibits a melt viscosity of 10 to 100 Pa S as determined at a shear rate of 100 sec−1 and 370° C. and a deflection temperature under load of 220° C. or above.

    摘要翻译： 通过使用液晶聚酯树脂组合物提供了耐热性，刚性，强度或成型性和表面剥离特性之间的平衡优异的表面贴装（SMT）相机模块用树脂组合物，其包含100质量份 液晶聚酯，15〜60质量份的平均粒径为10〜50μm的滑石，25〜50质量份的数均纤维长度为100〜200μm的玻璃纤维，6〜 20质量份氧化钛和2〜10质量份炭黑，并且在剪切速率为100秒-1和370℃下测定的熔体粘度为10〜100Pa·s，挠曲温度 在220°C或以上的负载下。