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公开(公告)号:US06821339B2
公开(公告)日:2004-11-23
申请号:US10181280
申请日:2002-11-18
申请人: Kristian Eriksson , Juha Nurmi , Jouko Virtanen
发明人: Kristian Eriksson , Juha Nurmi , Jouko Virtanen
IPC分类号: C30B714
CPC分类号: C13B30/027 , C07B63/00 , C07D201/16 , C30B7/00
摘要: The invention relates to a process for the crystallization of substances having a narrow metastable supersaturation zone. In the process the saturation of a solution is gradually increased and the solution is seeded for the crystallization. The seeding is performed at a seeding point which is selected in response to a signal received from said process indicating imminent or initial spontaneous nucleation. The process provides a good crystal yield and a crystalline product having a uniform crystal structure and a narrow crystal size distribution.
摘要翻译: 本发明涉及一种具有窄亚稳态过饱和区物质结晶的方法。 在该过程中,溶液的饱和度逐渐增加,并将溶液接种以进行结晶。 在接种点进行播种,该播种点响应于从所述过程接收到的信号而选择,表明即将发生或初始自发成核。 该方法提供了良好的晶体收率和具有均匀晶体结构和窄晶体尺寸分布的晶体产物。
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公开(公告)号:US08394288B2
公开(公告)日:2013-03-12
申请号:US13319179
申请日:2010-05-06
申请人: Juha Nurmi , Kirsti Jutila , Hannu Paananen , Kristian Eriksson
发明人: Juha Nurmi , Kirsti Jutila , Hannu Paananen , Kristian Eriksson
IPC分类号: C09K3/18 , C07C229/12 , C07C227/40 , E01H10/00 , B01J2/30
CPC分类号: C09K3/185 , C07C227/40 , C07C229/12
摘要: The invention relates to the use of solid betaine for de-icing and/or preventing slipperiness. The solid betaine comprises at least one non-betaine compound affecting water and/or moisture movement in said solid betaine. The invention further relates to a process for the manufacture of solid betaine. A suspension comprising betaine crystals is prepared from a feed liquid and the betaine crystals are separated and washed. The amount of wash liquid is adjusted in order to leave 0.5 to 10 w-% of at least one non-betaine compound in said solid betaine.
摘要翻译: 本发明涉及固体甜菜碱用于除冰和/或防止滑溜的用途。 固体甜菜碱包含影响所述固体甜菜碱中水和/或水分运动的至少一种非甜菜碱化合物。 本发明还涉及制备固体甜菜碱的方法。 由进料液制备包含甜菜碱晶体的悬浮液,分离并洗涤甜菜碱晶体。 调整洗涤液的量以便在所述固体甜菜碱中留下0.5至10w%的至少一种非甜菜碱化合物。
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公开(公告)号:US20120112120A1
公开(公告)日:2012-05-10
申请号:US13319179
申请日:2010-05-06
申请人: Juha Nurmi , Kirsti Jutila , Hannu Paananen , Kristian Eriksson
发明人: Juha Nurmi , Kirsti Jutila , Hannu Paananen , Kristian Eriksson
IPC分类号: C09K3/18
CPC分类号: C09K3/185 , C07C227/40 , C07C229/12
摘要: The invention relates to the use of solid betaine for de-icing and/or preventing slipperiness. The solid betaine comprises at least one non-betaine compound affecting water and/or moisture movement in said solid betaine. The invention further relates to a process for the manufacture of solid betaine. A suspension comprising betaine crystals is prepared from a feed liquid and the betaine crystals are separated and washed. The amount of wash liquid is adjusted in order to leave 0.5 to 10 w-% of at least one non-betaine compound in said solid betaine.
摘要翻译: 本发明涉及固体甜菜碱用于除冰和/或防止滑溜的用途。 固体甜菜碱包含影响所述固体甜菜碱中水和/或水分运动的至少一种非甜菜碱化合物。 本发明还涉及制备固体甜菜碱的方法。 由进料液制备包含甜菜碱晶体的悬浮液,分离并洗涤甜菜碱晶体。 调整洗涤液的量以便在所述固体甜菜碱中留下0.5至10w%的至少一种非甜菜碱化合物。
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公开(公告)号:US5980640A
公开(公告)日:1999-11-09
申请号:US609494
申请日:1996-03-01
申请人: Juha Nurmi , Olli-Pekka Eroma , Kristian Eriksson
发明人: Juha Nurmi , Olli-Pekka Eroma , Kristian Eriksson
IPC分类号: B01D9/00 , B01D9/02 , C13B30/02 , C13B30/04 , C13B30/06 , C13K1/08 , C13K5/00 , C13K13/00 , C13F1/02 , C13F1/00 , C13F3/00
CPC分类号: C13B30/02 , B01D9/0004 , C13B30/06 , C13K1/08 , C13K13/002 , C13K5/00
摘要: The invention relates to a method for recovering a crystallizable organic compound from solutions containing said compound. In accordance with the method, the compound is crystallized substantially by way of nucleation from a solution having high viscosity and high supersaturation in respect of the compound to be recovered, and the formed crystals are recovered.
摘要翻译: 本发明涉及从含有所述化合物的溶液中回收可结晶有机化合物的方法。 根据该方法,化合物基本上通过从待回收化合物的具有高粘度和高过饱和度的溶液中成核而结晶,并回收形成的晶体。
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