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公开(公告)号：US5766306A
公开(公告)日：1998-06-16
申请号：US657992
申请日：1996-06-04
CPC分类号： H01F1/36 , B22F1/0096 , B22F9/305 , B22F2998/00 , B22F2999/00 , Y10S977/777 , Y10S977/838 , Y10S977/896
摘要： Sononochemistry permits extremely rapid cooling to produce nanoscale particles. If magnetic, these particles are valuable for magnetic recording media, manufacture of permanent magnets, and other uses. In the present invention, we sonicate neat metal carbonyl to produce particles which we separate, generally magnetically, from the metal carbonyl, thereby making the production process as simple as possible and continuous.
摘要翻译： 声子化学允许极快速冷却以产生纳米级颗粒。 如果是磁性的，这些颗粒对于磁记录介质，永磁体的制造和其他用途是有价值的。 在本发明中，我们将纯金属羰基超声波处理以产生通常磁性地从金属羰基分离的颗粒，从而使生产过程尽可能简单和连续。
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公开(公告)号：US5766764A
公开(公告)日：1998-06-16
申请号：US663761
申请日：1996-06-04
CPC分类号： B82Y25/00 , B22F9/305 , G11B5/62 , G11B5/70615 , G11B5/714 , G11B5/8412 , H01F1/0063 , H01F1/1535 , B22F2998/00 , B22F2999/00 , Y10S428/90 , Y10S977/777 , Y10S977/788 , Y10S977/838 , Y10S977/896 , Y10T428/2998
摘要： Sonochemistry permits extremely rapid cooling to form nanoscale amorphous metal particles. If magnetic, these particles are valuable for magnetic recording media, manufacture of permanent magnets, and other uses. The nanoscale particles agglomerate, however, which limits their utility for these magnetic applications. To keep the particles isolated, we extract the particles from the n-alkane reaction solvent in a polar solvent and cast the extracted particles with a polymer, such as polyvinylpyrrolidone.
摘要翻译： Sonochemistry允许非常快速的冷却形成纳米级无定形金属颗粒。 如果是磁性的，这些颗粒对于磁记录介质，永磁体的制造和其他用途是有价值的。 然而，纳米级颗粒附聚物限制了其对这些磁性应用的实用性。 为了保持颗粒分离，我们在极性溶剂中从正烷烃反应溶剂中提取颗粒，并用聚合物如聚乙烯吡咯烷酮浇注提取的颗粒。
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公开(公告)号：US5520717A
公开(公告)日：1996-05-28
申请号：US476973
申请日：1995-06-07
CPC分类号： B22F9/305 , B22F2998/00 , B22F2999/00 , Y10S977/773 , Y10S977/777 , Y10S977/84 , Y10S977/845
摘要： Sonochemistry permits extremely rapid cooling from the melt which is necessary for forming amorphous metals. Sonochemistry also functions at an extremely small scale to produce nanophase particles. If magnetic, these particles are valuable for magnetic recording media, manufacture of permanent magnets, and other uses. The nanophase particles agglomerate, however, which limits their utility for these magnetic applications. To keep the particles isolated, we extract the particles from the n-alkane reaction solvent in a polar solvent and cast the extracted particles with a polymer, such as polyvinylpyrrolidone.
摘要翻译： 声化学允许从形成无定形金属所需的熔体中快速冷却。 声化学也以非常小的规模起作用以产生纳米相颗粒。 如果是磁性的，这些颗粒对于磁记录介质，永磁体的制造和其他用途是有价值的。 然而，纳米相颗粒团聚限制了其对这些磁性应用的效用。 为了保持颗粒分离，我们在极性溶剂中从正烷烃反应溶剂中提取颗粒，并用聚合物如聚乙烯吡咯烷酮浇注提取的颗粒。
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公开(公告)号：US07807229B2
公开(公告)日：2010-10-05
申请号：US12432624
申请日：2009-04-29
CPC分类号： C09J7/10 , C08K5/0025 , C08K5/29 , C09J2205/102 , C09J2433/00 , Y10T428/14 , Y10T428/1476 , Y10T428/2852 , Y10T428/2878
摘要： Methods of forming a pressure sensitive adhesive (PSA) are provided. The methods may be suitable for aircraft exterior applications. A particular method includes mixing together an un-crosslinked acrylic adhesive, a solvent, and a polyisocyanate crosslinker to form a mixture. The method also includes driving off a portion of the solvent. The method further includes reacting the polyisocyanate crosslinker with the un-crosslinked acrylic adhesive. A resultant crosslinked adhesive exhibits a peel strength in a range between around 2 pounds per square inch and around 8 pounds per square inch at temperatures in a range between around 180 degrees Fahrenheit and around 250 degrees Fahrenheit.
摘要翻译： 提供形成压敏粘合剂（PSA）的方法。 这些方法可能适用于飞机外部应用。 一种特定的方法包括将未交联的丙烯酸粘合剂，溶剂和多异氰酸酯交联剂混合在一起以形成混合物。 该方法还包括驱除一部分溶剂。 该方法还包括使多异氰酸酯交联剂与未交联的丙烯酸粘合剂反应。 所得到的交联粘合剂在大约180华氏度和约250华氏度之间的温度范围内显示在约2磅/平方英寸和约8磅/平方英寸之间的范围内的剥离强度。
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公开(公告)号：US07544407B1
公开(公告)日：2009-06-09
申请号：US11228370
申请日：2005-09-17
CPC分类号： C09J7/10 , C08K5/0025 , C08K5/29 , C09J2205/102 , C09J2433/00 , Y10T428/14 , Y10T428/1476 , Y10T428/2852 , Y10T428/2878
摘要： A pressure sensitive adhesive (PSA) suitable for aircraft exterior applications formed by reacting a cross-linker with an un-crosslinked adhesive can resist many aircraft fluids and can maintain a bond to a protective barrier film of an appliqué at low and high temperatures. An exemplary PSA includes at least a first release liner and a crosslinked adhesive releasably bonded thereto. The crosslinked adhesive suitably is formed by reacting a polyisocyanate crosslinker with an un-crosslinked acrylic adhesive. The PSA can exhibit a peel strength between around 2-8 psi at temperatures between around 180-250 degrees Fahrenheit. In an exemplary method to provide a PSA, an un-crosslinked acrylic adhesive, a solvent, and a polyisocyanate crosslinker are mixed together. The mixture is reacted on a release liner. A portion of the solvent is driven off, and the polyisocyanate crosslinker is reacted with itself and with reactive groups remaining on the un-crosslinked acrylic adhesive.
摘要翻译： 适用于通过使交联剂与未交联的粘合剂反应形成的飞行器外部应用的压敏粘合剂（PSA）可以抵抗许多飞行器流体并且可以在低温和高温下保持与贴布贴的保护性屏障膜的结合。 示例性PSA包括至少第一释放衬垫和可释放地结合到其上的交联粘合剂。 交联粘合剂通过多异氰酸酯交联剂与未交联的丙烯酸粘合剂反应形成。 在约180-250华氏度的温度下，PSA可以表现出约2-8psi之间的剥离强度。 在提供PSA的示例性方法中，将未交联的丙烯酸粘合剂，溶剂和多异氰酸酯交联剂混合在一起。 混合物在剥离衬垫上反应。 一部分溶剂被排出，多异氰酸酯交联剂与其自身反应并且反应性基团保留在未交联的丙烯酸粘合剂上。
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公开(公告)号：US06191248B1
公开(公告)日：2001-02-20
申请号：US08994899
申请日：1997-12-19
IPC分类号： C08G1832
CPC分类号： B82Y30/00 , C01P2004/20 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2004/80 , C01P2006/60 , C09C1/64 , C09C1/648 , Y10T428/31551
摘要： Thin film metal particulates are removed from FEP sheetstock cheaply and quickly by immersing the coated FEP first in a base and then in an acid. Occasionally, ultrasonic vibration of the FEP may also be required. The particulates are useful as paint pigments when isolated and conversion coated. The FEP is reusable. A preferred binder for carrying the pigments is a two-component system having a tetraketimine and an isocyanate.
摘要翻译： 通过将涂覆的FEP首先浸入碱中，然后在酸中将FEP片材中的薄膜金属颗粒从FEP片材中去除。 偶尔也可能需要FEP的超声波振动。 当分离和转化涂层时，颗粒可用作油漆颜料。 FEP是可重用的。 用于承载颜料的优选粘合剂是具有四亚胺和异氰酸酯的双组分体系。
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公开(公告)号：US20090214793A1
公开(公告)日：2009-08-27
申请号：US12432624
申请日：2009-04-29
CPC分类号： C09J7/10 , C08K5/0025 , C08K5/29 , C09J2205/102 , C09J2433/00 , Y10T428/14 , Y10T428/1476 , Y10T428/2852 , Y10T428/2878
摘要： Methods of forming a pressure sensitive adhesive (PSA) are provided. The methods may be suitable for aircraft exterior applications. A particular method includes mixing together an un-crosslinked acrylic adhesive, a solvent, and a polyisocyanate crosslinker to form a mixture. The method also includes driving off a portion of the solvent. The method further includes reacting the polyisocyanate crosslinker with the un-crosslinked acrylic adhesive. A resultant crosslinked adhesive exhibits a peel strength in a range between around 2 pounds per square inch and around 8 pounds per square inch at temperatures in a range between around 180 degrees Fahrenheit and around 250 degrees Fahrenheit.
摘要翻译： 提供形成压敏粘合剂（PSA）的方法。 这些方法可能适用于飞机外部应用。 一种特定的方法包括将未交联的丙烯酸粘合剂，溶剂和多异氰酸酯交联剂混合在一起以形成混合物。 该方法还包括驱除一部分溶剂。 该方法还包括使多异氰酸酯交联剂与未交联的丙烯酸粘合剂反应。 所得到的交联粘合剂在大约180华氏度和约250华氏度之间的温度范围内显示在约2磅/平方英寸和约8磅/平方英寸之间的范围内的剥离强度。
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8.发明申请公开(公告)号：US20090169794A1
公开(公告)日：2009-07-02
申请号：US11228370
申请日：2005-09-17
IPC分类号： C09J133/02 , B32B7/12 , B05D5/10 , B32B37/12
CPC分类号： C09J7/10 , C08K5/0025 , C08K5/29 , C09J2205/102 , C09J2433/00 , Y10T428/14 , Y10T428/1476 , Y10T428/2852 , Y10T428/2878
摘要： A pressure sensitive adhesive (PSA) suitable for aircraft exterior applications formed by reacting a cross-linker with an un-crosslinked adhesive can resist many aircraft fluids and can maintain a bond to a protective barrier film of an appliqué at low and high temperatures. An exemplary PSA includes at least a first release liner and a crosslinked adhesive releasably bonded thereto. The crosslinked adhesive suitably is formed by reacting a polyisocyanate crosslinker with an un-crosslinked acrylic adhesive. The PSA can exhibit a peel strength between around 2-8 psi at temperatures between around 180-250 degrees Fahrenheit. In an exemplary method to provide a PSA, an un-crosslinked acrylic adhesive, a solvent, and a polyisocyanate crosslinker are mixed together. The mixture is reacted on a release liner. A portion of the solvent is driven off, and the polyisocyanate crosslinker is reacted with itself and with reactive groups remaining on the un-crosslinked acrylic adhesive.
摘要翻译： 适用于通过使交联剂与未交联的粘合剂反应形成的飞行器外部应用的压敏粘合剂（PSA）可以抵抗许多飞行器流体并且可以在低温和高温下保持与贴布贴的保护性屏障膜的结合。 示例性PSA包括至少第一释放衬垫和可释放地结合到其上的交联粘合剂。 交联粘合剂通过多异氰酸酯交联剂与未交联的丙烯酸粘合剂反应形成。 在约180-250华氏度的温度下，PSA可以表现出约2-8psi之间的剥离强度。 在提供PSA的示例性方法中，将未交联的丙烯酸粘合剂，溶剂和多异氰酸酯交联剂混合在一起。 混合物在剥离衬垫上反应。 一部分溶剂被排出，多异氰酸酯交联剂与其自身反应并且反应性基团保留在未交联的丙烯酸粘合剂上。
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公开(公告)号：US06353135B1
公开(公告)日：2002-03-05
申请号：US09386738
申请日：1999-08-31
申请人： Larry K. Olli
发明人： Larry K. Olli
IPC分类号： C07C27524
CPC分类号： C07D251/66
摘要： Aliphatic tetraketimine of the present invention are a novel class of compounds represented by the formula: wherein Et is ethyl, Me is methyl, and R is a residue of an aliphatic diisocyanate. The tetraketimine is made by condensing a novel ketimine with a diisocyanate. The ketimine has a free secondary amine after a polyamine selected from the group consisting of: H2N—C2H4—NH—C2H4—NH2, H2N—C2H4—NH—C2H4—NH—C2H4—NH2, H2N—(CH2)6—NH—(CH2)6—NH2, or tris(2-aminoethyl)amine is reacted with a ketone.
摘要翻译： 本发明的脂族四亚甲基是由下式表示的新一类化合物：其中Et是乙基，Me是甲基，R是脂族二异氰酸酯的残基。 四亚甲基胺通过将新的酮亚胺与二异氰酸酯缩合而制得。 在选自H2N-C2H4-NH-C2H4-NH2，H2N-C2H4-NH-C2H4-NH-C2H4-NH2，H2N-（CH2）6-NH- （CH 2）6 -NH 2，ortris（2-氨基乙基）胺与甲酮反应。
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公开(公告)号：US06605365B1
公开(公告)日：2003-08-12
申请号：US09169280
申请日：1998-10-08
IPC分类号： B32B1504
CPC分类号： H05K3/389 , B05D3/102 , B05D5/10 , B32B15/04 , C01P2004/80 , C09C1/62 , C09C1/644 , C09C1/648 , C09D4/00 , C09D5/002 , C09D5/086 , C09D183/14 , C09J5/02 , C09J2400/166 , C23C18/1204 , C23C18/1208 , C23C18/1216 , C23C18/122 , C23C18/1225 , C23C18/1241 , C23C18/1254 , C23C18/127 , C23C28/00 , H05K3/383 , Y02T50/67 , Y10T428/256 , Y10T428/31612 , C08G77/00
摘要： A surface treatment, especially for titanium and aluminum alloys, forms a pigmented sol-gel film covalently bonded on the metal surface to produce desired color, gloss, reflectivity, electrical conductivity, emissivity, or a combination thereof usable over a wide temperature range. The coating retains its characteristics and impact resistance following exposures to temperatures at least in the range from −321° F. to 750° F. An aqueous sol containing an alkoxyzirconium and an organosilane with an organic acid catalyst and zirconium stabilizer is applied to etched or grit blasted substrates by dipping, spraying, or drenching, to produce bonds in a single application comparable in strength and performance to standard anodize controls. Parameters affecting performance include the sol composition, the Si/Zr ratio, the ratio of sol ingredients, the concentration of the sol, the carrier solvent, solution age, catalysts, surface pretreatment, application method, curing process, and primer used. The sol-gel coating may be graded in its ceramic character by adjusting the organosilane component between TEOS and silanes that have more distinctive organic character by virtue of organic ligands attached to the silicon.
摘要翻译： 特别是钛和铝合金的表面处理形成了共价键合在金属表面上的着色溶胶 - 凝胶膜，以产生在宽温度范围内可用的所需颜色，光泽度，反射率，电导率，发射率或其组合。 涂层在暴露于-321°F至750°F范围内的温度下保持其特性和耐冲击性。将含有烷氧基锆和有机硅烷的含水溶胶与有机酸催化剂和锆稳定剂一起施加到蚀刻或 通过浸渍，喷涂或浸润，通过浸渍，喷涂或浸润，在单一应用中生产粘结剂，以与标准阳极氧化处理相当的强度和性能。 影响性能的参数包括溶胶组成，Si / Zr比，溶胶成分比例，溶胶浓度，载体溶剂，溶液时间，催化剂，表面预处理，涂布方法，固化过程和使用的引物。 溶胶 - 凝胶涂层可以通过调整TEOS和硅烷之间的有机硅烷组分，借助于与硅连接的有机配体具有更显着的有机特性，可以分级其陶瓷特性。
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