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1.发明申请公开(公告)号：US20140329017A1
公开(公告)日：2014-11-06
申请号：US14125837
申请日：2012-06-17
申请人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Booth , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
发明人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Booth , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
IPC分类号： C03C25/30
CPC分类号： C03C25/30 , C08F32/02 , C08G61/08 , C08G2261/3325 , C08G2261/418 , C08K5/0025 , C08K5/14 , C08K5/29 , C08K2201/014 , C08L65/00
摘要： This invention relates to compositions and methods for improving the adhesion of resin compositions to substrate materials, pre-treating substrate materials to improve the adhesion of resin compositions to the substrate materials, and/or controlling gel formation of resin compositions. More particularly, the invention relates to compositions and methods for improving the adhesion of ring opening metathesis polymerization (ROMP) compositions to substrate materials using adhesion promoters containing isocyariate groups in a resin composition. The invention also relates to methods for improving the adhesion of resin compositions to substrate materials by pre-treating substrate materials with adhesion promoters containing isocyanate groups. The invention further relates to a method of providing a gel-modified ROMP composition, in which a hydroperoxide is added to a ROMP polymerizable resin composition in order to control gel formation of the polymerizing resin. An improved ROMP composition is further disclosed, comprising a cyclic olefin, a ROMP metathesis catalyst, an adhesion promoter, and an added hydroperoxide gel modifier. The polymer products produced via ROMP reactions of the invention may be utilized for a wide range of materials and composite applications. The invention has utility in the fields of catalysis, organic synthesis, and polymer and materials chemistry and manufacture.
摘要翻译： 本发明涉及用于改善树脂组合物与基材的粘合性，预处理基材以改善树脂组合物与基材的粘合性和/或控制树脂组合物凝胶形成的组合物和方法。 更具体地，本发明涉及使用在树脂组合物中含有异质基团的粘合促进剂来改善开环易位聚合（ROMP）组合物与基材的粘合性的组合物和方法。 本发明还涉及通过用含有异氰酸酯基团的粘合促进剂预处理底物材料来改善树脂组合物对基材的粘附性的方法。 本发明还涉及一种提供凝胶改性的ROMP组合物的方法，其中将氢过氧化物加入到ROMP可聚合树脂组合物中以控制聚合树脂的凝胶形成。 进一步公开了改进的ROMP组合物，其包含环烯烃，ROMP复分解催化剂，粘合促进剂和加入的氢过氧化物凝胶改性剂。 通过本发明的ROMP反应生产的聚合物产品可用于广泛的材料和复合材料应用。 本发明可用于催化，有机合成，聚合物和材料的化学和制造领域。
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公开(公告)号：US10457597B2
公开(公告)日：2019-10-29
申请号：US14125837
申请日：2012-06-17
申请人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Boothe , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
发明人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Boothe , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
摘要： This invention relates to compositions and methods for improving the adhesion of resin compositions to substrate materials, pre-treating substrate materials to improve the adhesion of resin compositions to the substrate materials, and/or controlling gel formation of resin compositions. More particularly, the invention relates to compositions and methods for improving the adhesion of ring opening metathesis polymerization (ROMP) compositions to substrate materials using adhesion promoters containing isocyariate groups in a resin composition. The invention also relates to methods for improving the adhesion of resin compositions to substrate materials by pre-treating substrate materials with adhesion promoters containing isocyanate groups. The invention further relates to a method of providing a gel-modified ROMP composition, in which a hydroperoxide is added to a ROMP polymerizable resin composition in order to control gel formation of the polymerizing resin. An improved ROMP composition is further disclosed, comprising a cyclic olefin, a ROMP metathesis catalyst, an adhesion promoter, and an added hydroperoxide gel modifier. The polymer products produced via ROMP reactions of the invention may be utilized for a wide range of materials and composite applications. The invention has utility in the fields of catalysis, organic synthesis, and polymer and materials chemistry and manufacture.
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公开(公告)号：US08324334B2
公开(公告)日：2012-12-04
申请号：US13060058
申请日：2009-08-21
CPC分类号： C08G61/08 , C08G2261/3322 , C08G2261/418
摘要： Olefin metathesis polymerization reactions are disclosed, and more particularly ring-opening metathesis polymerization of cyclic olefins with olefinic compounds, such as are derived from seed oils and the like, to form telechelic polymers. In one aspect, a method is provided for carrying out a catalytic ring-opening metathesis polymerization reaction, comprising contacting at least one olefinic compound with at least one cyclic olefin, in the presence of a ruthenium alkylidene olefin metathesis catalyst under conditions effective to allow ring-opening metathesis polymerization of the cyclic olefin, whereby the cyclic olefin polymer formed is terminated with the olefinic compound. The invention has utility in the fields of catalysis, organic synthesis, polymer chemistry, and industrial chemistry.
摘要翻译： 公开了烯烃易位聚合反应，更具体地说，环烯烃与烯烃化合物如来自种子油等的开环易位聚合反应形成遥爪聚合物。 在一个方面，提供了一种用于进行催化开环易位聚合反应的方法，包括在钌亚烷基烯烃复分解催化剂存在下使至少一种烯烃化合物与至少一种环烯烃接触，所述条件有效地允许环 开环环烯烃的易位聚合，由此所形成的环烯烃聚合物用烯烃化合物终止。 本发明可用于催化，有机合成，聚合物化学和工业化学领域。
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公开(公告)号：US20110294971A1
公开(公告)日：2011-12-01
申请号：US13060058
申请日：2009-08-21
IPC分类号： C08F216/04 , C08F232/06 , C08F232/04 , C08F4/80 , C08F222/20 , C08F220/68 , C08F216/10
CPC分类号： C08G61/08 , C08G2261/3322 , C08G2261/418
摘要： Olefin metathesis polymerization reactions are disclosed, and more particularly ring-opening metathesis polymerization of cyclic olefins with olefinic compounds, such as are derived from seed oils and the like, to form telechelic polymers. In one aspect, a method is provided for carrying out a catalytic ring-opening metathesis polymerization reaction, comprising contacting at least one olefinic compound with at least one cyclic olefin, in the presence of a ruthenium alkylidene olefin metathesis catalyst under conditions effective to allow ring-opening metathesis polymerization of the cyclic olefin, whereby the cyclic olefin polymer formed is terminated with the olefinic compound. The invention has utility in the fields of catalysis, organic synthesis, polymer chemistry, and industrial chemistry.
摘要翻译： 公开了烯烃易位聚合反应，更具体地说，环烯烃与烯烃化合物如来自种子油等的开环易位聚合反应形成遥爪聚合物。 在一个方面，提供了一种用于进行催化开环易位聚合反应的方法，包括在钌亚烷基烯烃复分解催化剂存在下使至少一种烯烃化合物与至少一种环烯烃接触，所述条件有效地允许环 开环环烯烃的易位聚合，由此所形成的环烯烃聚合物用烯烃化合物终止。 本发明可用于催化，有机合成，聚合物化学和工业化学领域。
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5.发明授权Method for purifying electroluminescent material, electroluminescent material and electroluminescent device 有权电致发光材料的净化方法，电致发光材料和电致发光器件公开(公告)号：US07507351B2
公开(公告)日：2009-03-24
申请号：US10559273
申请日：2004-06-04
申请人： Yoshihiro Tsuda , Yoshii Morishita , Satoyuki Nomura , Seiji Tai , Yousuke Hoshi , Shigeaki Funyuu , Farshad J. Motamedi , Li-Sheng Wang
发明人： Yoshihiro Tsuda , Yoshii Morishita , Satoyuki Nomura , Seiji Tai , Yousuke Hoshi , Shigeaki Funyuu , Farshad J. Motamedi , Li-Sheng Wang
CPC分类号： C08G61/124 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1014 , C09K2211/1029 , C09K2211/1416 , C09K2211/1425 , C09K2211/1433 , C09K2211/1475 , C09K2211/1483 , Y10S428/917
摘要： Objects of the present invention are to provide a purification process that enables Pd to be removed effectively, and to provide an electroluminescent material and an electroluminescent device obtained by employing the process. The present invention relates to a process for purifying an electroluminescent material, the process involving treating, with a phosphorus-containing material, an electroluminescent material that contains Pd as an impurity so as to remove the Pd.
摘要翻译： 本发明的目的是提供能够有效除去Pd的纯化方法，并提供通过使用该方法获得的电致发光材料和电致发光器件。 本发明涉及一种电致发光材料的纯化方法，该方法涉及用含磷材料处理含有Pd作为杂质的电致发光材料，以除去Pd。
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公开(公告)号：US08075943B2
公开(公告)日：2011-12-13
申请号：US11317253
申请日：2005-12-27
申请人： Yoshihiro Tsuda , Yoshii Morishita , Satoyuki Nomura , Yousuke Hoshi , Shigeaki Funyuu , Farshad J. Motamedi , Li-Sheng Wang
发明人： Yoshihiro Tsuda , Yoshii Morishita , Satoyuki Nomura , Yousuke Hoshi , Shigeaki Funyuu , Farshad J. Motamedi , Li-Sheng Wang
CPC分类号： H01L51/0025 , H01L51/0036 , H01L51/0039 , H01L51/0043 , H01L51/0059 , H01L51/56
摘要： Objects of the present invention are to provide a purification process that enables Pd contained in an organic electronics material to be removed effectively, to provide an electroluminescent device middle layer material purified by the process, and to provide an electroluminescent device employing the middle layer material. The present invention relates to a process for purifying an organic electronics material, the process involving treating, with a phosphorus-containing material, an organic electronics material that contains Pd as an impurity so as to remove the Pd.
摘要翻译： 本发明的目的是提供一种使有机电子材料中包含的Pd能够被有效去除以提供通过该方法纯化的电致发光器件中间层材料并提供使用中间层材料的电致发光器件的纯化方法。 本发明涉及一种纯化有机电子材料的方法，该方法涉及用含磷材料处理含有Pd作为杂质的有机电子材料，以除去Pd。
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公开(公告)号：US07714099B2
公开(公告)日：2010-05-11
申请号：US10966370
申请日：2004-10-15
申请人： Yoshii Morishita , Satoyuki Nomura , Yoshihiro Tsuda , Seiji Tai , Matthew L. Marrocco, III , Farshad J. Motamedi , Li-Sheng Wang , Yongchao Liang
发明人： Yoshii Morishita , Satoyuki Nomura , Yoshihiro Tsuda , Seiji Tai , Matthew L. Marrocco, III , Farshad J. Motamedi , Li-Sheng Wang , Yongchao Liang
CPC分类号： C07D249/20 , C07D209/88 , C07D409/14 , C08G61/122 , C08G61/124 , C08G61/125 , C08G61/126 , C08G73/18 , C08G73/22 , Y10S428/917
摘要： High quantum yield luminescent monomers, oligomers, and polymers, comprising benzotriazole repeating units and derivatives thereof have been discovered and utilized in optical devices and components therefor, including electroluminescent devices, light emitting devices, photoluminescent devices, organic light emitting diodes (OLEDs), OLED displays, sensors, and the like.
摘要翻译： 包括苯并三唑重复单元及其衍生物的高量子产率发光单体，低聚物和聚合物已被发现并用于其光学器件及其组件中，包括电致发光器件，发光器件，光致发光器件，有机发光二极管（OLED），OLED 显示器，传感器等。
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8.发明授权Purification process of electroluminescent material, electroluminescent material and electroluminescent device 有权电致发光材料，电致发光材料和电致发光器件的净化过程公开(公告)号：US08242235B2
公开(公告)日：2012-08-14
申请号：US10559280
申请日：2004-06-04
申请人： Yoshihiro Tsuda , Yoshii Morishita , Satoyuki Nomura , Seiji Tai , Yousuke Hoshi , Shigeaki Funyuu , Matthew L. Marrocco, III , Farshad J. Motamedi , Li-Sheng Wang
发明人： Yoshihiro Tsuda , Yoshii Morishita , Satoyuki Nomura , Seiji Tai , Yousuke Hoshi , Shigeaki Funyuu , Matthew L. Marrocco, III , Farshad J. Motamedi , Li-Sheng Wang
IPC分类号： C08G85/00
CPC分类号： C09K11/01 , C08G61/02 , C08G73/026 , C08G73/08 , Y02W30/72
摘要： Objects of the present invention are to provide a purification process that enables Pd and P to be removed effectively, and to provide an electroluminescent material and an electroluminescent device obtained by employing the process. The present invention relates to a process for purifying an electroluminescent material, the process involving treating, with an oxidizing agent and then with a column, an electroluminescent material that contains Pd and/or P as impurities so as to remove the Pd and/or P.
摘要翻译： 本发明的目的是提供能够有效除去Pd和P的纯化方法，并提供通过采用该方法获得的电致发光材料和电致发光器件。 本发明涉及一种纯化电致发光材料的方法，该方法包括用氧化剂，然后用柱子处理含有Pd和/或P作为杂质的电致发光材料，以除去Pd和/或P 。
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公开(公告)号：US07262265B1
公开(公告)日：2007-08-28
申请号：US10779207
申请日：2004-02-13
CPC分类号： C08G65/4006 , C08G75/20
摘要： A new family of high temperature thermoset resins having high glass transition temperatures and enhanced hygrothermal stability that are synthesized using inexpensive starting materials in essentially a single step process. A trifunctional aromatic, wherein at least one of the three functional groups comprises a halogen and the balance thereof comprises OH groups and wherein said aromatic has electron withdrawing properties, is polymerized using an excess of a diol.
摘要翻译： 一系列高温热固性树脂，具有高玻璃化转变温度和增强的湿热稳定性，它们使用廉价的起始原料在基本上单一步骤中合成。 三官能芳族化合物，其中三个官能团中的至少一个包含卤素，余量包含OH基团，并且其中所述芳族化合物具有吸电子性质，使用过量的二醇聚合。
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公开(公告)号：US08822633B2
公开(公告)日：2014-09-02
申请号：US11816911
申请日：2006-02-22
CPC分类号： H01L51/0035 , C08G61/02 , C08G61/10 , C09K2211/1029 , C09K2211/1416 , C09K2211/1425 , C09K2211/1433 , C09K2211/1466 , C09K2211/185 , H01L51/0039 , H01L51/0043 , H01L51/0085 , H01L51/5012 , H05B33/14 , Y02E10/549
摘要： Luminescent polymers having sterically twisted arylene repeat units are provided, which are particularly suited as electroluminescent polymers. Monomers necessary for the synthesis of the sterically twisted polyarylene are provided, as are electroluminescent device utilizing these polymers.
摘要翻译： 提供具有空间扭曲的亚芳基重复单元的发光聚合物，其特别适用于电致发光聚合物。 提供了空间扭转聚亚芳基合成所需的单体，以及利用这些聚合物的电致发光器件。
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