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公开(公告)号：US06358419B1
公开(公告)日：2002-03-19
申请号：US08641514
申请日：1996-05-01
申请人： Mariola Rötzheim , Wolfgang Greb , Wolfgang Zgorzelski , Carl Dieter Frohning , Klaus Denkmann , Heinz Kalbfell
发明人： Mariola Rötzheim , Wolfgang Greb , Wolfgang Zgorzelski , Carl Dieter Frohning , Klaus Denkmann , Heinz Kalbfell
IPC分类号： C02F144
CPC分类号： C02F1/26 , C02F2101/34 , C02F2103/36 , C02F2209/06 , Y10S210/05 , Y10S210/908 , Y10S210/909
摘要： Wastewater from the aldolization reaction is purified by adjusting its pH to 0 to 6, followed by extraction with monohydric alcohols having at least 8 carbon atoms, hydrocarbons having at least 6 carbon atoms, and mixtures thereof. In some cases, adjustment of the pH causes the formation of an organic phase, which is separated from the remaining wastewater before extraction.
摘要翻译： 通过将其pH调节至0至6，然后用具有至少8个碳原子的一元醇，具有至少6个碳原子的烃及其混合物进行萃取来纯化来自醛糖醛酸化反应的废水。 在某些情况下，pH的调节会导致有机相的形成，其在萃取之前与剩余废水分离。
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公开(公告)号：US6096931A
公开(公告)日：2000-08-01
申请号：US204597
申请日：1998-12-03
IPC分类号： B01J23/755 , C07B61/00 , C07C29/141 , C07C31/02 , C07C29/14
CPC分类号： C07C29/141
摘要： In a process for preparing alcohols comprising the hydrogenation of aldehydes in the presence of a hydrogenation catalyst in the gas phase, the improvement comprising adding nitrogen-containing bases to the aldehyde to be hydrogenated, whereby the formation of by-products is largely suppressed and isolation of the desired alcohols in high selectivity and correspondingly high yield is made possible.
摘要翻译： 在包含在气相中的氢化催化剂存在下醛的氢化制备醇的方法中，改进包括向待氢化的醛中加入含氮碱，从而大大抑制副产物的形成和分离 的所需醇以高选择性和相应的高收率成为可能。
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公开(公告)号：US07259279B2
公开(公告)日：2007-08-21
申请号：US11274079
申请日：2005-11-15
摘要： Process for the hydroformylation of olefins by linkage of the input parameters prevailing in the hydroformylation reaction to the target parameters of a hydroformylation reaction, wherein the linkage is achieved by means of at least one synthetic neuronal network.
摘要翻译： 通过将加氢甲酰化反应中盛行的输入参数与加氢甲酰基化反应的目标参数的连接将烯烃加氢甲酰化的方法，其中通过至少一个合成神经元网络实现连接。
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公开(公告)号：US5663445A
公开(公告)日：1997-09-02
申请号：US453919
申请日：1995-05-30
IPC分类号： B01J23/80 , B01J23/84 , B01J23/847 , B01J23/85 , B01J23/889 , B01J35/10 , C07B61/00 , C07C29/149 , C07C29/17 , C07C31/125 , C07C209/48 , C07C211/03 , C07C209/14
CPC分类号： B01J37/031 , B01J23/80 , B01J23/84 , B01J35/0053 , C07C209/48 , C07C29/149 , C07C29/177 , B01J35/1014 , B01J35/1019
摘要： A process for the catalytic preparation of alcohols or amines by reaction of esters, fatty acids, or nitriles with hydrogen at elevated temperature and pressure. The unreduced catalyst contains, per 100 parts by weight of CuO, 40 to 130 parts by weight of ZnO, 2 to 50 parts by weight of Al.sub.2 O.sub.3, and optionally 0.5 to 8 parts by weight of oxide of Mn, Mo, V, Zr, and/or alkaline earth metal. It has a BET total area of 80 to 175 m.sup.2 /g of catalyst in the unreduced state, and 75% to 95% of the BET total area is formed by pores having a radius r.sub.p .ltoreq.15 nm.
摘要翻译： 通过酯，脂肪酸或腈在高温和高压下与氢反应来催化制备醇或胺的方法。 未还原的催化剂相对于100重量份的CuO含有40〜130重量份的ZnO，2〜50重量份的Al 2 O 3，以及任选的0.5〜8重量份的Mn，Mo，V，Zr， 和/或碱土金属。 在未还原状态下，BET总面积为80〜175m2 / g，催化剂的总面积为75％〜95％，由半径rp <15nm的孔形成。
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公开(公告)号：US06700021B2
公开(公告)日：2004-03-02
申请号：US10188986
申请日：2002-07-03
申请人： Hans Bohnen , Carl Dieter Frohning , Ernst Wiebus
发明人： Hans Bohnen , Carl Dieter Frohning , Ernst Wiebus
IPC分类号： C07C4549
CPC分类号： B01J31/2404 , B01J23/46 , B01J31/24 , B01J2231/321 , B01J2531/822 , B01J2531/96 , C07C45/50 , C07C47/02
摘要： The present invention relates to a process for preparing aldehydes by reaction of olefinically unsaturated compounds with carbon monoxide and hydrogen, wherein, during the process, rhodium is added in the form of a reaction product from the reaction of metallic rhodium and/or more than one rhodium compound with rhodium-complexing compounds and with carbon monoxide and hydrogen, the use of said reaction product in catalytic processes and also the preparation of a catalytic composition with addition of said reaction product.
摘要翻译： 本发明涉及通过烯属不饱和化合物与一氧化碳和氢气反应来制备醛的方法，其中在该方法中，铑以反应产物的形式从金属铑和/或多于一种的反应中加入 铑化合物与铑络合化合物和一氧化碳和氢气，所述反应产物在催化过程中的用途，以及加入所述反应产物的催化组合物的制备。
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公开(公告)号：US5684215A
公开(公告)日：1997-11-04
申请号：US999191
申请日：1992-12-28
IPC分类号： B01J23/755 , B01J21/04 , B01J21/06 , C07B61/00 , C07C29/141 , C07C29/145 , C07C29/153 , C07C29/17 , C07C31/02 , C07C31/12 , C07C29/14
CPC分类号： C07C29/172 , C07C29/141 , C07C29/145
摘要： A process for the preparation of alcohols by reaction of organic carbonyl compounds or mixtures containing them with hydrogen over a supported catalyst containing nickel, aluminum oxide, and zirconium dioxide at elevated temperature and, if appropriate, under elevated pressure. Ketones, aldehydes and derivatives thereof are reacted as the carbonyl compounds at temperatures of 60.degree. to 150.degree. C.
摘要翻译： 通过有机羰基化合物或含有它们的混合物与氢气在升高的温度和适当的高压下在含有镍，氧化铝和二氧化锆的负载催化剂上反应来制备醇的方法。 酮，醛及其衍生物在60℃至150℃的温度下作为羰基化合物反应。
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