Production of silver sulfate grains using a fluorinated additive
    4.
    发明授权
    Production of silver sulfate grains using a fluorinated additive 有权
    使用氟化添加剂生产硫酸银颗粒

    公开(公告)号:US07655212B2

    公开(公告)日:2010-02-02

    申请号:US12101237

    申请日:2008-04-11

    IPC分类号: C01G5/00 C08K3/00

    摘要: An aqueous precipitation process for the preparation of particles comprising primarily silver sulfate, comprising reacting an aqueous soluble silver salt and an aqueous soluble source of inorganic sulfate ion in an agitated precipitation reactor vessel and precipitating particles comprising primarily silver sulfate, wherein the reaction and precipitation are performed in the presence of an aqueous soluble fluorinated additive, the amount of additive being a minor molar percentage, relative to the molar amount of silver sulfate precipitated, and effective to result in precipitation of particles comprising primarily silver sulfate having a mean grain-size of less than 50 micrometers.

    摘要翻译: 一种用于制备主要包含硫酸银的颗粒的水性沉淀方法,包括将水溶性银盐和无机硫酸根离子的水溶性来源在搅拌的沉淀反应器容器中反应并沉淀出主要包含硫酸银的颗粒,其中反应和沉淀是 在水溶性氟化添加剂的存在下进行,相对于沉淀的硫酸银的摩尔量,添加剂的量为次摩尔百分数,并且有效地导致主要包含平均粒径为 小于50微米。

    Process for preparing aluminum trisquinoline complex
    5.
    发明授权
    Process for preparing aluminum trisquinoline complex 有权
    制备三羟基喹啉络合物的方法

    公开(公告)号:US07321036B2

    公开(公告)日:2008-01-22

    申请号:US10834827

    申请日:2004-04-29

    IPC分类号: C07D401/14 C07D215/30

    CPC分类号: C07F5/069

    摘要: A process for forming the facial isomer of an aluminum trisquinoline complex comprises heating the solid aluminum trisquinoline complex material at a temperature at least 50° C. below the melting point temperature of the solid for a time sufficient to convert the aluminum trisquinoline complex to at least 99 mol % of one polymorph of the facial-isomer that fluoresces with a maximum intensity below 510 nm.

    摘要翻译: 形成三羟基喹啉铝复合物的面部异构体的方法包括在固体的熔点温度以下至少50℃的温度下加热固体三羟基喹啉络合物材料足够的时间以将铝三羟基喹啉复合物转化为至少 99mol%的面部异构体的一个多晶型物以最大强度在510nm以下发荧光。

    Process for forming a composite including an aluminum trisquinoline complex
    6.
    发明授权
    Process for forming a composite including an aluminum trisquinoline complex 有权
    用于形成包含三羟基喹啉铝复合物的复合物的方法

    公开(公告)号:US07169484B2

    公开(公告)日:2007-01-30

    申请号:US10834621

    申请日:2004-04-29

    IPC分类号: H01L51/50 H05B33/14

    摘要: A process for forming a film of the facial-isomer of an aluminum trisquinoline complex comprises depositing a film of an aluminum trisquinoline complex on a support, depositing an inert barrier layer over the layer of aluminum trisquinoline complex that encapsulates aluminum trisquinoline complex to form a multilayer composite, and then heating the composite at a temperature below the melting point temperature of the complex for a time sufficient to convert the aluminum trisquinoline complex to at least 99 mol % of the facial-isomer that fluoresces with a maximum emission intensity below 510 nm. The product has a blue hue.

    摘要翻译: 形成铝三喹啉复合物的面体异构体的膜的方法包括在载体上沉积三羟基喹啉铝复合物的膜,在包封铝三羟基喹啉复合物的铝层上沉积惰性阻挡层,形成多层 复合物,然后在低于复合物熔点温度的温度下将复合物加热足够的时间,足以将铝三喹啉复合物转化为具有低于510nm的最大发射强度发荧光的至少99mol%的面状异构体。 该产品具有蓝色色调。