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公开(公告)号：US20060252960A1
公开(公告)日：2006-11-09
申请号：US10539802
申请日：2003-12-13
申请人： Martin Sohn , Eckhard Stroefer , Filip Nevejans , Ulrich Penzel , Has-Juergen Pallasch , Rene Leuthold , Andreas Brodhagen , Andreas Woelfert , Wolfgang Mackenroth , Markus Maurer
发明人： Martin Sohn , Eckhard Stroefer , Filip Nevejans , Ulrich Penzel , Has-Juergen Pallasch , Rene Leuthold , Andreas Brodhagen , Andreas Woelfert , Wolfgang Mackenroth , Markus Maurer
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： The invention relates to a process for preparing polyisocyanates by reacting organic amines with phosgene, wherein the reaction is carried out in at least three stages, with the first stage being carried out in a mixing apparatus, the second stage in at least one residence apparatus and the third stage in at least one separation apparatus and the pressure in each successive stage being lower than that in the previous stage.
摘要翻译： 本发明涉及一种通过使有机胺与光气反应制备多异氰酸酯的方法，其中反应进行至少三个阶段，第一阶段在混合装置中进行，第二阶段在至少一个停留装置中进行， 在至少一个分离装置中的第三阶段，并且每个连续阶段中的压力低于前一阶段的压力。
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公开(公告)号：US07851648B2
公开(公告)日：2010-12-14
申请号：US10539802
申请日：2003-12-13
申请人： Martin Sohn , Eckhard Stroefer , Filip Nevejans , Ulrich Penzel , Hans-Juergen Pallasch , Rene Leuthold , Andreas Brodhagen , Andreas Woelfert , Wolfgang Mackenroth , Markus Maurer
发明人： Martin Sohn , Eckhard Stroefer , Filip Nevejans , Ulrich Penzel , Hans-Juergen Pallasch , Rene Leuthold , Andreas Brodhagen , Andreas Woelfert , Wolfgang Mackenroth , Markus Maurer
IPC分类号： C07C249/00
CPC分类号： C07C263/10 , C07C265/14
摘要： The invention relates to a process for preparing polyisocyanates by reacting organic amines with phosgene, wherein the reaction is carried out in at least three stages, with the first stage being carried out in a mixing apparatus, the second stage in at least one residence apparatus and the third stage in at least one separation apparatus and the pressure in each successive stage being lower than that in the previous stage.
摘要翻译： 本发明涉及一种通过使有机胺与光气反应制备多异氰酸酯的方法，其中反应进行至少三个阶段，第一阶段在混合装置中进行，第二阶段在至少一个停留装置中进行， 在至少一个分离装置中的第三阶段，并且每个连续阶段中的压力低于前一阶段的压力。
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公开(公告)号：US08546606B2
公开(公告)日：2013-10-01
申请号：US10546890
申请日：2004-02-20
申请人： Andreas Brodhagen , Martin Sohn , Filip Nevejans , Eckhard Stroefer , Andreas Woelfert , Steffen Oehlenschlaeger
发明人： Andreas Brodhagen , Martin Sohn , Filip Nevejans , Eckhard Stroefer , Andreas Woelfert , Steffen Oehlenschlaeger
IPC分类号： C07C249/00
CPC分类号： B01J19/242 , B01J19/243 , B01J2219/00166 , B01J2219/182 , B01J2219/185 , B01J2219/187 , C07C263/10 , C07C265/14
摘要： The invention relates to a process for preparing polyisocyanates by reacting primary amines with phosgene, which comprises the steps a) mixing the amine with the phosgene, b) reacting the amine with the phosgene in a residence reactor and, if desired, c) transferring the output from the reactor of step b) into a distillation column, wherein the residence reactor in step b) is configured as a tube reactor.
摘要翻译： 本发明涉及通过使伯胺与光气反应制备多异氰酸酯的方法，其包括以下步骤：a）将胺与光气混合，b）使胺与光气在停留反应器中反应，如果需要，c）将 从步骤b）的反应器输出到蒸馏塔中，其中步骤b）中的停留反应器被配置为管式反应器。
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公开(公告)号：US20060223966A1
公开(公告)日：2006-10-05
申请号：US10546890
申请日：2004-02-20
申请人： Andreas Brodhagen , Martin Sohn , Filip Nevejans , Eckhard Stroefer , Andreas Wölfert , Steffen Oehlenschläger
发明人： Andreas Brodhagen , Martin Sohn , Filip Nevejans , Eckhard Stroefer , Andreas Wölfert , Steffen Oehlenschläger
IPC分类号： C08G18/00
CPC分类号： B01J19/242 , B01J19/243 , B01J2219/00166 , B01J2219/182 , B01J2219/185 , B01J2219/187 , C07C263/10 , C07C265/14
摘要： The invention relates to a process for preparing polyisocyanates by reacting primary amines with phosgene, which comprises the steps a) mixing the amine with the phosgene, b) reacting the amine with the phosgene in a residence reactor and, if desired, c) transferring the output from the reactor of step b) into a distillation column, wherein the residence reactor in step b) is configured as a tube reactor.
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公开(公告)号：US07112694B2
公开(公告)日：2006-09-26
申请号：US10513340
申请日：2003-05-19
IPC分类号： C07C263/00 , B01J10/00
CPC分类号： C07C263/10 , C07C265/14
摘要： The present invention relates to a continuous process for preparing isocyanates by reacting primary amines with phosgene, wherein the reaction is carried out in a cascade of at least two tube reactors and the gas phase formed in the reaction is separated off in a phase separator after each reactor and only the liquid phase is passed to the next reactor or to product purification and the reaction volume of the first tube reactor is only a fraction of the total reaction volume.
摘要翻译： 本发明涉及通过使伯胺与光气反应制备异氰酸酯的连续方法，其中反应在至少两个管式反应器的级联中进行，并且在每个反应器中在相分离器中分离反应中形成的气相 反应器，并且只有液相被传送到下一个反应器或产物纯化，并且第一管式反应器的反应体积仅为总反应体积的一部分。
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公开(公告)号：US20050222453A1
公开(公告)日：2005-10-06
申请号：US10513340
申请日：2003-05-19
IPC分类号： C07C263/10 , C07C265/14
CPC分类号： C07C263/10 , C07C265/14
摘要： The present invention relates to a continuous process for preparing isocyanates by reacting primary amines with phosgene, wherein the reaction is carried out in a cascade of at least two tube reactors and the gas phase formed in the reaction is separated off in a phase separator after each reactor and only the liquid phase is passed to the next reactor or to product purification and the reaction volume of the first tube reactor is only a fraction of the total reaction volume.
摘要翻译： 本发明涉及通过使伯胺与光气反应制备异氰酸酯的连续方法，其中反应在至少两个管式反应器的级联中进行，并且在每个反应器中在相分离器中分离反应中形成的气相 反应器，并且只有液相被传送到下一个反应器或产物纯化，并且第一管式反应器的反应体积仅为总反应体积的一部分。
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公开(公告)号：US09132387B2
公开(公告)日：2015-09-15
申请号：US13712536
申请日：2012-12-12
CPC分类号： B01D61/246 , B01D11/0288 , B01D11/0292 , B01D11/0415 , B01D61/243 , C07C41/38
摘要： The invention relates to a process for working-up a reaction mixture (5) comprising polyetherol and dissolved alkali metal comprising catalyst, wherein at least alkali metal ions of the dissolved alkali metal comprising catalyst are partially or completely removed from the mixture by a membrane separation process, the process comprising following steps: (a) feeding the reaction mixture (5) comprising polyetherol and dissolved alkali metal comprising catalyst into a first chamber (1) of a separation unit (3), (b) feeding a solvent into a second chamber (7) of the separation unit (3), the first chamber (1) and the second chamber (7) being separated by a membrane (9), (c) transporting at least the alkali metal ions of the alkali metal comprising catalyst from the first chamber (1) into the second chamber by passing through the membrane (9).
摘要翻译： 本发明涉及一种用于处理包含聚醚醚和包含催化剂的溶解的碱金属的反应混合物（5）的方法，其中至少包含催化剂的溶解的碱金属的碱金属离子通过膜分离部分或完全从混合物中除去 方法包括以下步骤：（a）将包含聚乙烯醇和包含催化剂的溶解的碱金属的反应混合物（5）进料到分离单元（3）的第一室（1）中，（b）将溶剂进料到第二 分离单元（3）的室（7），第一室（1）和第二室（7）被隔膜（9）隔开，（c）至少输送包含催化剂的碱金属的碱金属离子 从第一腔室（1）通过膜（9）进入第二腔室。
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8.发明授权Process for preparing a C4-olefin mixture by selective hydrogenation and metathesis process for using this stream 有权通过选择性氢化和复分解方法制备C4烯烃混合物的方法公开(公告)号：US08362308B2
公开(公告)日：2013-01-29
申请号：US13042142
申请日：2011-03-07
申请人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
发明人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
IPC分类号： C07C5/02
CPC分类号： C07C11/08 , C07C6/04 , C07C2523/44 , C07C11/107 , C07C11/10
摘要： A C4-olefin mixture having a 1,3-butadiene content of from 100 to 500 ppm and a content of 1,2-dienes of less than 10 ppm is described. The present invention further provides a process for preparing this C4-olefin mixture and provides for its use in a metathesis reaction for preparing 2-pentene and/or 3-hexene.
摘要翻译： 描述1,3-丁二烯含量为100-500ppm，1,2-二烯含量小于10ppm的C 4 - 烯烃混合物。 本发明还提供了一种制备该C 4烯烃混合物的方法，并提供其在复分解反应中用于制备2-戊烯和/或3-己烯的用途。
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9.发明授权Process for preparing a C4-olefin mixture by selective hydrogenation and metathesis process for using this stream 有权通过选择性氢化和复分解方法制备C4烯烃混合物的方法公开(公告)号：US07923588B2
公开(公告)日：2011-04-12
申请号：US11665161
申请日：2005-10-13
申请人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
发明人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
CPC分类号： C07C11/08 , C07C6/04 , C07C2523/44 , C07C11/107 , C07C11/10
摘要： A C4-olefin mixture having a 1,3-butadiene content of from 100 to 500 ppm and a content of 1,2-dienes of less than 10 ppm is described. The present invention further provides a process for preparing this C4-olefin mixture and provides for its use in a metathesis reaction for preparing 2-pentene and/or 3-hexene.
摘要翻译： 描述1,3-丁二烯含量为100-500ppm，1,2-二烯含量小于10ppm的C 4 - 烯烃混合物。 本发明还提供了一种制备该C 4烯烃混合物的方法，并提供其在复分解反应中用于制备2-戊烯和/或3-己烯的用途。
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10.发明申请Process For Preparing A C4-Olefin Mixture By Selective Hydrogenation And Metathesis Process For Using This Stream 有权通过选择性氢化和复分解方法制备C4-烯烃混合物的方法公开(公告)号：US20080188696A1
公开(公告)日：2008-08-07
申请号：US11665161
申请日：2005-10-13
申请人： Jurgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Roper , Thomas Hill
发明人： Jurgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Roper , Thomas Hill
CPC分类号： C07C11/08 , C07C6/04 , C07C2523/44 , C07C11/107 , C07C11/10
摘要： A C4-olefin mixture having a 1,3-butadiene content of from 100 to 500 ppm and a content of 1,2-dienes of less than 10 ppm is described. The present invention further provides a process for preparing this C4-olefin mixture and provides for its use in a metathesis reaction for preparing 2-pentene and/or 3-hexene.
摘要翻译： 描述1,3-丁二烯含量为100-500ppm，1,2-二烯含量小于10ppm的C 4 - 烯烃混合物。 本发明还提供了一种制备该C 4烯烃混合物的方法，并提供其在复分解反应中用于制备2-戊烯和/或3-己烯的用途。
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