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    Process for preparing fluorine-containing polymer
    1.
    发明授权
    Process for preparing fluorine-containing polymer 有权
    含氟聚合物的制备方法

    公开(公告)号：US07345124B2

    公开(公告)日：2008-03-18

    申请号：US10521807

    申请日：2003-07-23

    申请人： Masaki Irie ,  Satoshi Tokuno ,  Sadashige Irie ,  Yosuke Nishimura ,  Yoshinori Hori ,  Mitsuru Kishine

    发明人： Masaki Irie ,  Satoshi Tokuno ,  Sadashige Irie ,  Yosuke Nishimura ,  Yoshinori Hori ,  Mitsuru Kishine

    IPC分类号： C08F14/18

    CPC分类号： C08F2/00 ,  C08F214/18 ,  C08F214/22

    摘要： The present invention provides a process for preparing a fluorine-containing polymer having few branched chains and little weight change in high temperatures, which is a new process wherein composition distribution substantially does not occur. The fluorine-containing polymer is prepared by a batch copolymerization process conducted under conditions of reduced temperature of at least 0.95 and reduced pressure of at least 0.80 of the critical constant calculated from critical temperature, critical pressure and composition ratio of each monomer in the gaseous phase of the reaction vessel using the Peng-Robinson formula.

    摘要翻译： 本发明提供一种制备具有很少支链和在高温下重量变化小的含氟聚合物的方法，这是其中组合物分布基本上不发生的新方法。 含氟聚合物是通过间歇共聚方法制备的，所述间歇共聚方法是在降低至少0.95的温度和至少0.80的关键常数的减压条件下进行的，该临界常数由气相中各单体的临界温度，临界压力和组成比计算 的反应容器使用Peng-Robinson公式。

    Process for producing fluoropolymer
    2.
    发明申请
    Process for producing fluoropolymer 有权

    公开(公告)号：US20050250922A1

    公开(公告)日：2005-11-10

    申请号：US10521807

    申请日：2003-07-23

    申请人： Masaki Irie ,  Satoshi Tokuno ,  Sadashige Irie ,  Yosuke Nishimura ,  Yoshinori Hori ,  Mitsuru Kishine

    发明人： Masaki Irie ,  Satoshi Tokuno ,  Sadashige Irie ,  Yosuke Nishimura ,  Yoshinori Hori ,  Mitsuru Kishine

    IPC分类号： C08F2/00 ,  C08F14/18 ,  C08F214/18 ,  C08F214/22

    CPC分类号： C08F2/00 ,  C08F214/18 ,  C08F214/22

    摘要： The present invention provides a process for preparing a fluorine-containing polymer having few branched chains and little weight change in high temperatures, which is a new process wherein composition distribution substantially does not occur. The fluorine-containing polymer is prepared by a batch copolymerization process conducted under conditions of reduced temperature of at least 0.95 and reduced pressure of at least 0.80 of the critical constant calculated from critical temperature, critical pressure and composition ratio of each monomer in the gaseous phase of the reaction vessel using the Peng-Robinson formula; wherein when the number of monomer components in the target polymer is represented as n (n is an integer of 2 or larger), the name of each monomer component is represented as A1, A2, . . . An, the weight percentage of each monomer component A1, A2, . . . An of the target polymer composition is represented as a1, a2, . . . an (%) (a satisfies ∑ n ⁢ a n = 100 ) , the weight percentage of each monomer component of the initial monomer composition is represented as a′1, a′2 . . . a′n (%) (a′ satisfies ∑ n ⁢ a n ′ = 100 and a′1, a′2, . . . a′n is determined in a constant manner depending on predetermined polymerization conditions) and specific gravity of the gaseous phase monomers when polymerizing/specific gravity of the target polymer is represented as B, the composition weight ratio of additional monomers is calculated for each monomer from the formula (a1−a′1×B):(a2−a′2×B) . . . (an−a′n×B) in the order of components A1, A2, . . . An, and additional monomers containing additional monomers in the composition weight ratio of additional monomers are added.

    Method for producing vulcanizable fluorine-containing elastomer
    3.
    发明申请
    Method for producing vulcanizable fluorine-containing elastomer 有权
    可硫化含氟弹性体的制造方法

    公开(公告)号：US20060052548A1

    公开(公告)日：2006-03-09

    申请号：US10542545

    申请日：2004-01-22

    申请人： Yousuke Nishimura ,  Masaki Irie ,  Sadashige Irie ,  Manabu Fujisawa ,  Satoshi Tokuno ,  Mitsuru Kishine

    发明人： Yousuke Nishimura ,  Masaki Irie ,  Sadashige Irie ,  Manabu Fujisawa ,  Satoshi Tokuno ,  Mitsuru Kishine

    IPC分类号： C08C19/20

    CPC分类号： C08F214/28 ,  C08F214/18 ,  C08F214/22

    摘要： The present invention provides a process for preparing a fluorine-containing elastomer in a high productivity comparable to that of non-iodine transfer polymerization process by carrying out an iodine transfer polymerization at high pressure. The present invention also provides a fluorine-containing elastomer prepared by this process, and fluorine-containing molded articles. The process is a batch copolymerization process conducted under conditions that the reduced temperature of the critical constant is at least 0.95 and the reduced pressure of the critical constant is at least 0.80 wherein the reduced temperature and the reduced pressure are calculated using the Peng-Robinson formula from the critical temperature, the critical pressure and the composition ratio of each of the monomers in the gaseous phase in a reaction vessel, in which ethylenically unsaturated compounds containing at least one fluoroolefine are copolymerized in the presence of a compound having the formula: Rf1·Ix wherein Rf1 is a saturated or unsaturated fluorohydrocarbon or chlorofluorohydrocarbon group having 1 to 16 carbon atoms, and x is the number of bonds of Rf1 and an integer of 1 to 4.

    摘要翻译： 本发明提供了一种通过在高压下进行碘转移聚合制备与非碘转移聚合方法相当的高生产率的含氟弹性体的方法。 本发明还提供了通过该方法制备的含氟弹性体和含氟成型体。 该方法是在临界常数降低至少为0.95，临界常数降低至少为0.80的条件下进行的间歇共聚方法，其中降低的温度和减压是使用Peng-Robinson公式 从临界温度，临界压力和反应容器中气相中各单体的组成比

    Process for preparing vulcanizable fluorine-containing elastomer
    4.
    发明申请
    Process for preparing vulcanizable fluorine-containing elastomer 有权
    制备可硫化含氟弹性体的方法

    公开(公告)号：US20070299207A1

    公开(公告)日：2007-12-27

    申请号：US11892702

    申请日：2007-08-27

    申请人： Yousuke Nishimura ,  Masaki Irie ,  Sadashige Irie ,  Manabu Fujisawa ,  Satoshi Tokuno ,  Mitsuru Kishine

    发明人： Yousuke Nishimura ,  Masaki Irie ,  Sadashige Irie ,  Manabu Fujisawa ,  Satoshi Tokuno ,  Mitsuru Kishine

    IPC分类号： C08L27/14

    CPC分类号： C08F214/28 ,  C08F214/18 ,  C08F214/22

    摘要： The present invention provides a process for preparing a fluorine-containing elastomer in a high productivity comparable to that of non-iodine transfer polymerization process by carrying out an iodine transfer polymerization at high pressure. The present invention also provides a fluorine-containing elastomer prepared by this process, and fluorine-containing molded articles. The process is a batch copolymerization process conducted under conditions that the reduced temperature of the critical constant is at least 0.95 and the reduced pressure of the critical constant is at least 0.80 wherein the reduced temperature and the reduced pressure are calculated using the Peng-Robinson formula from the critical temperature, the critical pressure and the composition ratio of each of the monomers in the gaseous phase in a reaction vessel, in which ethylenically unsaturated compounds containing at least one fluoroolefine are copolymerized in the presence of a compound having the formula: Rf1·Ix wherein Rf1 is a saturated or unsaturated fluorohydrocarbon or chlorofluorohydrocarbon group having 1 to 16 carbon atoms, and x is the number of bonds of Rf1 and an integer of 1 to 4.

    摘要翻译： 本发明提供了一种通过在高压下进行碘转移聚合制备与非碘转移聚合方法相当的高生产率的含氟弹性体的方法。 本发明还提供了通过该方法制备的含氟弹性体和含氟成型体。 该方法是在临界常数降低至少为0.95，临界常数降低至少为0.80的条件下进行的间歇共聚方法，其中降低的温度和减压是使用Peng-Robinson公式 在临界温度下，在具有下式的化合物的存在下，在反应容器中的气相中的每种单体的临界压力和组成比共聚，其中含有至少一个氟烯烃的烯键式不饱和化合物在具有下式的化合物的存在下共聚： 其中R 1是饱和或不饱和的氟代烃或其中R 1，R 2，R 3，R 4， 具有1至16个碳原子的氯氟烃基，x是R 1和...的整数1至4的整数。

    Process for preparing vulcanizable fluorine-containing elastomer
    5.
    发明授权
    Process for preparing vulcanizable fluorine-containing elastomer 有权
    制备可硫化含氟弹性体的方法

    公开(公告)号：US08247505B2

    公开(公告)日：2012-08-21

    申请号：US11892702

    申请日：2007-08-27

    申请人： Yousuke Nishimura ,  Masaki Irie ,  Sadashige Irie ,  Manabu Fujisawa ,  Satoshi Tokuno ,  Mitsuru Kishine

    发明人： Yousuke Nishimura ,  Masaki Irie ,  Sadashige Irie ,  Manabu Fujisawa ,  Satoshi Tokuno ,  Mitsuru Kishine

    IPC分类号： C08F14/18

    CPC分类号： C08F214/28 ,  C08F214/18 ,  C08F214/22

    摘要： The present invention provides a process for preparing a fluorine-containing elastomer in a high productivity comparable to that of non-iodine transfer polymerization process by carrying out an iodine transfer polymerization at high pressure. The present invention also provides a fluorine-containing elastomer prepared by this process, and fluorine-containing molded articles. The process is a batch copolymerization process conducted under conditions that the reduced temperature of the critical constant is at least 0.95 and the reduced pressure of the critical constant is at least 0.80 wherein the reduced temperature and the reduced pressure are calculated using the Peng-Robinson formula from the critical temperature, the critical pressure and the composition ratio of each of the monomers in the gaseous phase in a reaction vessel, in which ethylenically unsaturated compounds containing at least one fluoroolefine are copolymerized in the presence of a compound having the formula: Rf1·Ix wherein Rf1 is a saturated or unsaturated fluorohydrocarbon or chlorofluorohydrocarbon group having 1 to 16 carbon atoms, and x is the number of bonds of Rf1 and an integer of 1 to 4.

    摘要翻译： 本发明提供了一种通过在高压下进行碘转移聚合制备与非碘转移聚合方法相当的高生产率的含氟弹性体的方法。 本发明还提供了通过该方法制备的含氟弹性体和含氟成型体。 该方法是在临界常数降低至少为0.95，临界常数降低至少为0.80的条件下进行的间歇共聚方法，其中降低的温度和减压是使用Peng-Robinson公式 在临界温度下，在具有下式的化合物的存在下共聚反应容器中气相中各单体的临界压力和组成比：Rf1· 其中Rf1是具有1至16个碳原子的饱和或不饱和的氟代烃或氯氟烃基，x是Rf1的键数和1至4的整数。

    Process for preparing vulcanizable fluorine-containing elastomer
    6.
    发明授权
    Process for preparing vulcanizable fluorine-containing elastomer 有权
    制备可硫化含氟弹性体的方法

    公开(公告)号：US07375171B2

    公开(公告)日：2008-05-20

    申请号：US10542545

    申请日：2004-01-22

    申请人： Yousuke Nishimura ,  Masaki Irie ,  Sadashige Irie ,  Manabu Fujisawa ,  Satoshi Tokuno ,  Mitsuru Kishine

    发明人： Yousuke Nishimura ,  Masaki Irie ,  Sadashige Irie ,  Manabu Fujisawa ,  Satoshi Tokuno ,  Mitsuru Kishine

    IPC分类号： C08F14/18

    CPC分类号： C08F214/28 ,  C08F214/18 ,  C08F214/22

    摘要： The present invention provides a process for preparing a fluorine-containing elastomer in a high productivity comparable to that of non-iodine transfer polymerization process by carrying out an iodine transfer polymerization at high pressure. The present invention also provides a fluorine-containing elastomer prepared by this process, and fluorine-containing molded articles. The process is a batch copolymerization process conducted under conditions that the reduced temperature of the critical constant is at least 0.95 and the reduced pressure of the critical constant is at least 0.80 wherein the reduced temperature and the reduced pressure are calculated using the Peng-Robinson formula from the critical temperature, the critical pressure and the composition ratio of each of the monomers in the gaseous phase in a reaction vessel, in which ethylenically unsaturated compounds containing at least one fluoroolefine are copolymerized in the presence of a compound having the formula: Rf1.Ix wherein Rf1 is a saturated or unsaturated fluorohydrocarbon or chlorofluorohydrocarbon group having 1 to 16 carbon atoms, and x is the number of bonds of Rf1 and an integer of 1 to 4.

    摘要翻译： 本发明提供了一种通过在高压下进行碘转移聚合制备与非碘转移聚合方法相当的高生产率的含氟弹性体的方法。 本发明还提供了通过该方法制备的含氟弹性体和含氟成型体。 该方法是在临界常数降低至少为0.95，临界常数降低至少为0.80的条件下进行的间歇共聚方法，其中降低的温度和减压是使用Peng-Robinson公式 在临界温度下，在具有下式的化合物的存在下，在反应容器中的气相中的每种单体的临界压力和组成比共聚，其中含有至少一个氟烯烃的烯键式不饱和化合物在具有下式的化合物的存在下共聚： 其中R 1是饱和或不饱和的氟代烃或其中R 1，R 2，R 3，R 4，R 5， 具有1至16个碳原子的氯氟烃基，x是R 1和...的整数1至4的整数。

    Fluorine-containing rubber composition
    7.
    发明授权
    Fluorine-containing rubber composition 有权
    含氟橡胶组合物

    公开(公告)号：US06503986B1

    公开(公告)日：2003-01-07

    申请号：US09743708

    申请日：2001-01-16

    申请人： Hiroyuki Tanaka ,  Sadashige Irie ,  Tsuyoshi Noguchi ,  Mitsuru Kishine

    发明人： Hiroyuki Tanaka ,  Sadashige Irie ,  Tsuyoshi Noguchi ,  Mitsuru Kishine

    IPC分类号： C08L2712

    CPC分类号： C09K3/1009 ,  C08F293/005 ,  C08L27/12 ,  C08L27/16 ,  C08L27/18 ,  C08L53/00 ,  C08L2666/24 ,  C08L2666/02 ,  C08L2666/04

    摘要： To provide a fluorine-containing rubber composition comprising (a-1) a non-perfluoro fluorine-containing rubber and (b-1) a fluorine-containing multi-segment polymer comprising an elastomeric fluorine-containing polymer chain segment and non-elastomeric fluorine-containing polymer chain segment, in which structural units of each of the elastomeric fluorine-containing polymer chain segment and the non-elastomeric fluorine-containing polymer chain segment comprise not less than 90% by mole of a perhalo olefin unit. The fluorine-containing rubber composition is capable of providing a clean sealing material for semi-conductor production apparatuses without using a filler.

    摘要翻译： 为了提供含有（a-1）非全氟含氟橡胶的氟橡胶组合物和（b-1）含有弹性体含氟聚合物链段和非弹性体氟的含氟多段聚合物 聚合物链段，其中弹性体含氟聚合物链段和非弹性含氟聚合物链段的结构单元包括不少于90摩尔％的全卤代烯烃单元。 含氟橡胶组合物能够在不使用填料的情况下为半导体制造装置提供清洁的密封材料。

    Process for preparing fluorine-containing polymer
    9.
    发明授权
    Process for preparing fluorine-containing polymer 有权
    含氟聚合物的制备方法

    公开(公告)号：US06509429B1

    公开(公告)日：2003-01-21

    申请号：US09743188

    申请日：2001-01-05

    申请人： Masanori Kitaichi ,  Hiroshi Aihara ,  Sadashige Irie ,  Mitsuru Kishine ,  Yutaka Ueta ,  Katsuhide Otani ,  Yoshiki Maruya ,  Hideya Saito ,  Mitsuo Tsukamoto

    发明人： Masanori Kitaichi ,  Hiroshi Aihara ,  Sadashige Irie ,  Mitsuru Kishine ,  Yutaka Ueta ,  Katsuhide Otani ,  Yoshiki Maruya ,  Hideya Saito ,  Mitsuo Tsukamoto

    IPC分类号： C08F1418

    CPC分类号： C08F14/26 ,  C08F14/18 ,  C08F14/28 ,  C08F259/08 ,  C08F2/16 ,  C08F2/22 ,  C08F214/18

    摘要： A process for preparing a fluorine-containing polymer through emulsion polymerization method which enhances productivity while maintaining excellent physical properties of the fluorine-containing polymer and comprises (a) a first polymerization step for emulsion-polymerizing a fluorine-containing monomer or a mixture of a fluorine-containing monomer and a non-fluorine-containing monomer in an aqueous medium in the presence of a radical polymerization initiator and an emulsifying agent, (b) a dilution step for diluting the obtained aqueous emulsion of polymer particles with water to reduce the number of emulsified polymer particles per unit amount of aqueous medium in the emulsion and a concentration of emulsifying agent, and (c) a second polymerization step for emulsion-polymerizing a fluorine-containing monomer and/or a non-fluorine-containing monomer in the obtained diluted emulsified solution.

    摘要翻译： 一种通过乳液聚合方法制备含氟聚合物的方法，其提高生产率同时保持含氟聚合物的优异物理性能，并且包括（a）第一聚合步骤，用于将含氟单体或 在自由基聚合引发剂和乳化剂的存在下，在水性介质中含氟单体和非含氟单体，（b）稀释步骤，用水稀释所得聚合物颗粒的水乳液以减少数量 乳液中的乳化聚合物粒子和乳化剂的浓度的乳化聚合物粒子，和（c）在所得到的乳液聚合物粒子中使含氟单体和/或非含氟单体乳化聚合的第二聚合步骤 稀释乳化液。