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公开(公告)号：US08016918B2
公开(公告)日：2011-09-13
申请号：US11542895
申请日：2006-10-04
IPC分类号： B01D53/02
CPC分类号： C01B13/0259 , A61M16/101 , B01D53/0473 , B01D2253/104 , B01D2253/108 , B01D2253/30 , B01D2256/12 , B01D2257/102 , B01D2257/80 , B01D2259/40062 , B01D2259/4146 , B01D2259/4533 , C01B2210/0046 , C01B2210/0051 , C01B2210/0062
摘要： Pressure swing adsorption process for producing oxygen comprising (a) providing at least one adsorber vessel having a first layer of adsorbent adjacent the feed end of the vessel and a second layer of adsorbent adjacent the first layer, wherein the surface area to volume ratio of the first layer is in the range of about 0.75 to about 1.8 cm−1; (b) introducing a pressurized feed gas comprising at least oxygen, nitrogen, and water into the feed end, adsorbing at least a portion of the water in the adsorbent in the first layer, and adsorbing at least a portion of the nitrogen in the adsorbent in the second layer, wherein the superficial contact time of the pressurized feed gas in the first layer is between about 0.08 and about 0.50 sec; and (c) withdrawing a product gas enriched in oxygen from the product end of the adsorber vessel.
摘要翻译： 用于生产氧气的变压吸附方法包括（a）提供至少一个吸附容器，该吸附器具有邻近容器的进料端的第一吸附剂层和邻近第一层的第二吸附剂层，其中表面积与体积比 第一层在约0.75至约1.8cm -1的范围内; （b）将至少包含氧气，氮气和水的加压进料气体引入进料端，吸附第一层中的吸附剂中的至少一部分水，吸附吸附剂中至少一部分氮气 在第二层中，其中加压进料气体在第一层中的表面接触时间在约0.08至约0.50秒之间; 和（c）从吸附容器的产品端抽出富含氧气的产物气体。
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公开(公告)号：US20080083331A1
公开(公告)日：2008-04-10
申请号：US11542895
申请日：2006-10-04
IPC分类号： B01D53/02
CPC分类号： C01B13/0259 , A61M16/101 , B01D53/0473 , B01D2253/104 , B01D2253/108 , B01D2253/30 , B01D2256/12 , B01D2257/102 , B01D2257/80 , B01D2259/40062 , B01D2259/4146 , B01D2259/4533 , C01B2210/0046 , C01B2210/0051 , C01B2210/0062
摘要： Pressure swing adsorption process for producing oxygen comprising (a) providing at least one adsorber vessel having a first layer of adsorbent adjacent the feed end of the vessel and a second layer of adsorbent adjacent the first layer, wherein the surface area to volume ratio of the first layer is in the range of about 5 to about 11 cm−1; (b) introducing a pressurized feed gas comprising at least oxygen, nitrogen, and water into the feed end, adsorbing at least a portion of the water in the adsorbent in the first layer, and adsorbing at least a portion of the nitrogen in the adsorbent in the second layer, wherein the superficial contact time of the pressurized feed gas in the first layer is between about 0.08 and about 0.50 sec; and (c) withdrawing a product gas enriched in oxygen from the product end of the adsorber vessel.
摘要翻译： 用于生产氧气的变压吸附方法包括（a）提供至少一个吸附容器，该吸附器具有邻近容器的进料端的第一吸附剂层和邻近第一层的第二吸附剂层，其中表面积与体积比 第一层在约5至约11cm -1范围内; （b）将至少包含氧气，氮气和水的加压进料气体引入进料端，吸附第一层中的吸附剂中的至少一部分水，吸附吸附剂中至少一部分氮气 在第二层中，其中加压进料气体在第一层中的表面接触时间在约0.08至约0.50秒之间; 和（c）从吸附容器的产品端抽出富含氧气的产物气体。
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3.发明申请公开(公告)号：US20090071333A1
公开(公告)日：2009-03-19
申请号：US12275752
申请日：2008-11-21
IPC分类号： B01D53/047
CPC分类号： C01B13/0259 , B01D53/02 , B01D53/047 , B01D53/0473 , B01D2253/104 , B01D2253/108 , B01D2253/304 , B01D2256/12 , B01D2257/102 , B01D2257/11 , B01D2257/80 , B01D2259/4146 , B01D2259/4533 , C01B2210/0046 , C01B2210/0051 , C01B2210/0062 , C01B2210/0082
摘要： PSA process for oxygen production comprising (a) providing an adsorber having a first layer of adsorbent selective for water and a second layer of adsorbent selective for nitrogen, wherein the heat of adsorption of water on the adsorbent in the first layer is equal to or less than about 14 kcal/mole at water loadings less than about 0.05 mmol per gram; (b) passing a feed gas comprising at least oxygen, nitrogen, and water successively through the first and second layers, adsorbing water in the first layer of adsorbent, and adsorbing nitrogen in the second layer of adsorbent, wherein the mass transfer coefficient of water in the first layer is in the range of about 125 to about 400 sec−1 and the superficial contact time of the feed gas in the first layer is between about 0.08 and about 0.50 sec; and (c) withdrawing a product enriched in oxygen from the adsorber.
摘要翻译： 用于氧气生产的PSA方法，包括（a）提供具有对水有选择性的第一吸附剂层和第二层吸附剂的吸附器，其中第一层中吸附剂上的水的吸附热等于或等于 水量大于约14kcal / mol，小于约0.05mmol /克; （b）使至少包含氧，氮和水的进料气体依次通过第一和第二层，吸附第一层吸附剂中的水并吸附第二层吸附剂中的氮，其中水的传质系数 在第一层中在约125至约400秒-1的范围内，并且第一层中进料气体的表面接触时间在约0.08至约0.50秒之间; 和（c）从吸附器中取出富含氧的产物。
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公开(公告)号：US06605136B1
公开(公告)日：2003-08-12
申请号：US10192360
申请日：2002-07-10
申请人： David Ross Graham , Roger Dean Whitley , Robert Ling Chiang , Edward Landis Weist, Jr. , Timothy Christopher Golden , Matthew James Labuda
发明人： David Ross Graham , Roger Dean Whitley , Robert Ling Chiang , Edward Landis Weist, Jr. , Timothy Christopher Golden , Matthew James Labuda
IPC分类号： B01D53047
CPC分类号： B01D53/047 , B01D53/261 , B01D2253/102 , B01D2253/104 , B01D2253/108 , B01D2253/25 , B01D2253/304 , B01D2256/12 , B01D2256/16 , B01D2257/102 , B01D2257/502 , B01D2257/80 , B01D2259/40007 , B01D2259/40062 , B01D2259/4146
摘要： A pressure swing adsorption process which comprises introducing a feed gas mixture into an inlet of an adsorber vessel during a feed period, wherein the feed gas mixture contains a more strongly adsorbable component and a less strongly adsorbable component and the adsorber vessel contains a bed of adsorbent material which selectively adsorbs the more strongly adsorbable component, and withdrawing a product gas enriched in the less strongly adsorbable component from an outlet of the adsorber vessel during at least a portion of the feed period, wherein a dimensionless cycle-compensated mass transfer coefficient defined as K tfeedVads/Vfeed is maintained in the range of about 23 to about 250.
摘要翻译： 一种变压吸附方法，其包括在进料期间将进料气体混合物引入吸附容器的入口，其中所述进料气体混合物包含更强吸附组分和较不强吸附组分，并且所述吸附剂容器含有吸附剂床 选择性吸附较强吸附组分的材料，以及在进料周期的至少一部分期间从吸附剂容器的出口排出富含较不强吸附组分的产物气体，其中无量纲循环补偿传质系数定义为 K tfeedVads / Vfeed保持在约23至约250的范围内。
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5.发明申请公开(公告)号：US20080083332A1
公开(公告)日：2008-04-10
申请号：US11542948
申请日：2006-10-04
IPC分类号： B01D53/047
CPC分类号： B01D53/02 , B01D53/047 , B01D2253/104 , B01D2253/108 , B01D2253/304 , B01D2256/12 , B01D2257/102 , B01D2257/11 , B01D2257/80 , B01D2259/4146 , C01B13/0259 , C01B2210/0046 , C01B2210/0051 , C01B2210/0062 , C01B2210/0082
摘要： PSA process for oxygen production comprising (a) providing an adsorber having a first layer of adsorbent selective for water and a second layer of adsorbent selective for nitrogen, wherein the heat of adsorption of water on the adsorbent in the first layer is ≦ about 14 kcal/mole at water loadings≧ about 0.05 mmol per gram; (b) passing a feed gas comprising at least oxygen, nitrogen, and water successively through the first and second layers, adsorbing water in the first layer of adsorbent, and adsorbing nitrogen in the second layer of adsorbent, wherein the mass transfer coefficient of water in the first layer is in the range of about 125 to about 400 sec−1 and the superficial contact time of the feed gas in the first layer is between about 0.08 and about 0.50 sec; and (c) withdrawing a product enriched in oxygen from the adsorber.
摘要翻译： 用于氧气生产的PSA方法，包括（a）提供具有对水有选择性的第一吸附剂吸附剂和对氮气有选择性的第二吸附剂层的吸附器，其中在第一层中的吸附剂上的水的吸附热< kcal / mole在水负荷下> =约0.05mmol / g; （b）使至少包含氧，氮和水的进料气体依次通过第一和第二层，吸附第一层吸附剂中的水并吸附第二层吸附剂中的氮，其中水的传质系数 在第一层中在约125至约400秒-1的范围内，并且第一层中进料气体的表面接触时间在约0.08至约0.50秒之间; 和（c）从吸附器中取出富含氧的产物。
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6.发明授权公开(公告)号：US07717981B2
公开(公告)日：2010-05-18
申请号：US11542948
申请日：2006-10-04
IPC分类号： B01D53/02
CPC分类号： B01D53/02 , B01D53/047 , B01D2253/104 , B01D2253/108 , B01D2253/304 , B01D2256/12 , B01D2257/102 , B01D2257/11 , B01D2257/80 , B01D2259/4146 , C01B13/0259 , C01B2210/0046 , C01B2210/0051 , C01B2210/0062 , C01B2210/0082
摘要： PSA process for oxygen production comprising (a) providing an adsorber having a first layer of adsorbent selective for water and a second layer of adsorbent selective for nitrogen, wherein the heat of adsorption of water on the adsorbent in the first layer is ≦about 14 kcal/mole at water loadings ≧about 0.05 to about 3 mmol per gram; (b) passing a feed gas comprising at least oxygen, nitrogen, and water successively through the first and second layers, adsorbing water in the first layer of adsorbent, and adsorbing nitrogen in the second layer of adsorbent, wherein the mass transfer coefficient of water in the first layer is in the range of about 125 to about 400 sec−1 and the superficial contact time of the feed gas in the first layer is between about 0.08 and about 0.50 sec; and (c) withdrawing a product enriched in oxygen from the adsorber.
摘要翻译： 用于氧气生产的PSA方法包括（a）提供具有对水有选择性的第一吸附剂层和第二层选择性氮吸附剂的吸附器，其中在第一层中的吸附剂上的水的吸附热为约14; kcal / mol，水含量≥约0.05至约3mmol /克; （b）使至少包含氧，氮和水的进料气体依次通过第一和第二层，吸附第一层吸附剂中的水并吸附第二层吸附剂中的氮，其中水的传质系数 在第一层中在约125至约400秒-1的范围内，并且第一层中进料气体的表面接触时间在约0.08至约0.50秒之间; 和（c）从吸附器中取出富含氧的产物。
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公开(公告)号：US06658894B2
公开(公告)日：2003-12-09
申请号：US10208078
申请日：2002-07-29
申请人： Timothy Christopher Golden , Thomas Stephen Farris , Robert Ling Chiang , Roger Dean Whitley , Fred William Taylor
发明人： Timothy Christopher Golden , Thomas Stephen Farris , Robert Ling Chiang , Roger Dean Whitley , Fred William Taylor
IPC分类号： F25J300
CPC分类号： C01B23/0068 , B01D53/04 , B01D2253/106 , B01D2253/108 , B01D2253/304 , B01D2253/306 , B01D2256/18 , B01D2257/11 , B01D2259/40083 , B01D2259/416 , B01D2259/4533 , B01D2259/4575 , B01J20/186 , C01B2210/0035 , C01B2210/0037 , C01B2210/0045 , F25J3/04757 , F25J2205/60
摘要： Xenon and/or krypton are recovered from oxygen containing gas, typically derived from liquid oxygen bottoms in a cryogenic air separation plant, by selective adsorption on a Li and Ag exchange zeolite containing 5 to 40% Ag exchange capacity on an equivalents basis, with periodic thermal regeneration of the adsorbent.
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公开(公告)号：US09945608B2
公开(公告)日：2018-04-17
申请号：US13555680
申请日：2012-07-23
申请人： Jason Michael Ploeger , Timothy Christopher Golden , Jeffrey Raymond Hufton , John Eugene Palamara
发明人： Jason Michael Ploeger , Timothy Christopher Golden , Jeffrey Raymond Hufton , John Eugene Palamara
CPC分类号： F25J3/08 , C10L3/10 , C10L3/101 , F25J3/0209 , F25J3/0233 , F25J3/0238 , F25J2200/02 , F25J2200/70 , F25J2205/04 , F25J2205/40 , F25J2205/60 , F25J2205/64 , F25J2210/06 , F25J2240/02 , F25J2290/80
摘要： The invention provides systems and methods for separating ethane and heavier hydrocarbons from a natural gas stream. In aspects of the invention, an adsorption unit is integrated with a cryogenic gas processing plant in order to overcome methane recovery limitations by sending the tail gas from the adsorption unit to the cryogenic gas processing plant to recover methane that would otherwise be lost.
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公开(公告)号：US08535414B2
公开(公告)日：2013-09-17
申请号：US13236112
申请日：2011-09-19
申请人： Andrew David Johnson , Richard Vincent Pearce , Thomas Stephen Farris , Timothy Christopher Golden , Matthew John Bosco , Eugene Joseph Karwacki, Jr. , David Charles Winchester , Jeffrey Raymond Hufton
发明人： Andrew David Johnson , Richard Vincent Pearce , Thomas Stephen Farris , Timothy Christopher Golden , Matthew John Bosco , Eugene Joseph Karwacki, Jr. , David Charles Winchester , Jeffrey Raymond Hufton
IPC分类号： B01D53/047 , C01B23/00
CPC分类号： B01D53/0476 , B01D2253/102 , B01D2253/104 , B01D2253/106 , B01D2253/108 , B01D2256/10 , B01D2256/18 , B01D2257/102 , B01D2257/11 , B01D2257/2047 , B01D2257/2066 , B01D2257/55 , B01D2257/80 , C01B23/0057 , C01B23/0068 , C01B2210/0037 , C01B2210/0045 , C01B2210/0051 , C01B2210/0056 , C01B2210/0062 , Y02P20/154
摘要： The present invention discloses the improvements to a vacuum swing adsorption (VSA) process used for Xe recovery. By only collecting the recovered gas mixture after the initial evacuation of N2 from the adsorbent vessel and void space, the recovered Xe is not diluted by N2 contained in the adsorbent vessel and void space. The concentration of the recovered Xe can by increased (high purity), simultaneously little Xenon is lost. During the initial evacuation of N2, the vessel has been evacuated to a pressure less than 1 atmospheric pressure, for example, from 100 to 1 torr.
摘要翻译： 本发明公开了用于Xe回收的真空挥发吸附（VSA）方法的改进。 通过在从吸附剂容器和空隙空间初始抽出N 2之后仅收集回收的气体混合物，回收的Xe不被包含在吸附剂容器和空隙空间中的N 2稀释。 回收的Xe的浓度可以通过增加（高纯度），同时少量的氙被丢失。 在N2初始抽真空期间，将容器抽真空至小于1大气压，例如100至1托。
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公开(公告)号：US08323602B2
公开(公告)日：2012-12-04
申请号：US12832156
申请日：2010-07-08
CPC分类号： B01D53/75 , B01D53/002 , B01D53/0462 , B01D53/047 , B01D53/1456 , B01D53/229 , B01D53/864 , B01D53/8646 , B01D2255/2073 , B01D2255/20761 , B01D2256/22 , B01D2257/302 , B01D2257/404 , B01D2257/502 , B01D2257/80 , B01D2258/0283 , F23G7/07 , F23J2215/40 , F23J2215/50 , F25J3/067 , F25J2205/40 , F25J2205/66 , F25J2205/80 , F25J2205/82 , F25J2210/70 , F25J2220/02 , F25J2220/04 , F25J2220/82 , F25J2220/84 , F25J2230/30 , F25J2230/32 , F25J2230/80 , F25J2240/90 , Y02C10/12 , Y02E20/12 , Y02E20/344
摘要： Carbon monoxide (CO) may be removed from flue gas generated by oxyfuel combustion of a hydrocarbon or carbonaceous fuel, by contacting the flue gas, or a CO-containing gas derived therefrom, at a first elevated temperature, e.g. at least 80° C., and at a first elevated pressure, e.g. at least 2 bar (0.2 MPa), with at least one catalyst bed comprising a CO-oxidation catalyst in the presence of oxygen (O2) to convert CO to carbon dioxide and produce carbon dioxide-enriched gas. The carbon dioxide produced from the CO may be recovered from the carbon dioxide-enriched gas using conventional carbon dioxide recovery techniques. NO in the flue gas may also be oxidized to nitrogen dioxide (NO2) and removed using conventional NO2 removal techniques, or may be reduced in the presence of a reducing gas to nitrogen (N2) which does not have to be removed from the gas.
摘要翻译： 一氧化碳（CO）可以通过烃或碳质燃料的氧燃料燃烧产生的烟道气中除去，通过在第一升高的温度例如，通过使烟道气或其衍生的含CO气体接触。 至少80℃，并且在第一高压下，例如， 至少2巴（0.2MPa），其中至少一个催化剂床在氧气（O 2）存在下包含CO氧化催化剂，以将CO转化为二氧化碳并产生富含二氧化碳的气体。 可以使用常规的二氧化碳回收技术从CO生成的二氧化碳从富含二氧化碳的气体中回收。 废气中的NO也可以被氧化成二氧化氮（NO 2）并且使用常规的NO 2去除技术去除，或者可以在还原气体存在下将氮气（N 2）还原，而不需要从气体中除去。
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