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1.发明授权公开(公告)号：US08278624B2
公开(公告)日：2012-10-02
申请号：US11842813
申请日：2007-08-21
CPC分类号： C09K11/7774 , C30B15/04 , C30B29/34
摘要： LSO scintillation crystals with improved scintillation and optical properties are achieved by controlled co-doping a LSO crystal melt with amounts of cerium and an additional codopant such as calcium or other divalent cations. Crystal growth atmosphere is optimized by controlling the amount of oxygen in the atmosphere. Zinc is added as an additional material to restabilize crystal growth where calcium co-dopant is added. The decay time of the scintillation crystal can be controlled by controlling the concentration of co-dopant added.
摘要翻译： 具有改善的闪烁和光学性质的LSO闪烁晶体通过用量的铈和另外的共掺杂剂例如钙或其它二价阳离子控制共掺杂LSO晶体熔体来实现。 通过控制大气中的氧气量来优化晶体生长气氛。 添加锌作为附加材料，以重新稳定晶体生长，其中加入钙共掺杂剂。 闪烁晶体的衰减时间可以通过控制添加的共掺杂剂的浓度来控制。
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公开(公告)号：US20140110588A1
公开(公告)日：2014-04-24
申请号：US13098654
申请日：2011-05-02
CPC分类号： C30B29/12 , C09K11/7733 , C30B11/003 , G01T1/20 , G01T1/202 , G01T3/06 , G21K4/00
摘要： The present disclosure discloses, in one arrangement, a single crystalline iodide scintillator material having a composition of the formula AM1-xEuxI3, A3M1-xEuxI5 and AM2(1-x)Eu2xI5, wherein A consists essentially of any alkali metal element (such as Li, Na K, Rb, Cs) or any combination thereof, M consists essentially of Sr, Ca, Ba or any combination thereof, and 0≦x≦1. In another arrangement, the above single crystalline iodide scintillator material can be made by first synthesizing a compound of the above composition and then forming a single crystal from the synthesized compound by, for example, the Vertical Gradient Freeze method. Applications of the iodide scintillator materials include radiation detectors and their use in medical and security imaging.
摘要翻译： 本公开在一种布置中公开了具有式AM1-xEuxI3，A3M1-xEuxI5和AM2（1-x）Eu2xI5组成的单结晶碘化物闪烁体材料，其中A基本上由任何碱金属元素（例如Li ，Na K，Rb，Cs）或其任何组合，M基本上由Sr，Ca，Ba或其任何组合组成，并且0和n 1; x和n 1; 在另一种布置中，上述单结晶碘化物闪烁体材料可以通过首先合成上述组成的化合物，然后通过例如垂直梯度冷冻法由合成的化合物形成单晶来制备。 碘化物闪烁体材料的应用包括辐射探测器及其在医疗和安全成像中的应用。
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公开(公告)号：US20110272586A1
公开(公告)日：2011-11-10
申请号：US13098662
申请日：2011-05-02
CPC分类号： G21K4/00 , C09K11/7705 , C09K11/772 , C09K11/7773 , C30B11/00 , C30B29/12 , G21K2004/06
摘要： The present disclosure discloses, in one arrangement, a single crystalline chloride scintillator material having a composition of the formula A3MCl6, wherein A consists essentially of Li, Na K, Rb, Cs or any combination thereof, and M consists essentially of Ce, Sc, Y, La, Lu, Gd, Pr, Tb, Yb, Nd or any combination thereof. In another arrangement, a chloride scintillator material is single-crystalline and has a composition of the formula AM2Cl7, wherein A consists essentially of Li, Na K, Rb, Cs or any combination thereof, and M consists essentially of Ce, Sc, Y, La, Lu, Gd, Pr, Tb, Yb, Nd or any combination thereof. Specific examples of these scintillator materials include single-crystalline Cs3CeCl6, CsCe2Cl7, Ce-doped KGd2Cl7 (KGd2(1-x)Ce2xCl7) and Ce-doped CsGd2Cl7 (CsGd2(1-x)Ce2xCl7). In a further arrangement, the Bridgman method can be used to grown single crystals of the chloride scintillator materials compounds synthesized from starting chlorides.
摘要翻译： 本公开在一种布置中公开了具有式A3MCl6组成的单晶氯化物闪烁体材料，其中A主要由Li，NaK，Rb，Cs或其任何组合组成，M基本上由Ce，Sc， Y，La，Lu，Gd，Pr，Tb，Yb，Nd或其任何组合。 在另一种布置中，氯化物闪烁体材料是单晶的并且具有式AM2Cl7的组成，其中A基本上由Li，NaK，Rb，Cs或其任何组合组成，M基本上由Ce，Sc，Y， La，Lu，Gd，Pr，Tb，Yb，Nd或其任何组合。 这些闪烁体材料的具体实例包括单晶Cs3CeCl6，CsCe2Cl7，Ce掺杂的KGd2Cl7（KGd2（1-x）Ce2xCl7）和Ce掺杂的CsGd2Cl7（CsGd2（1-x）Ce2xCl7）。 在另一种布置中，Bridgman方法可用于生长由起始氯化物合成的氯化物闪烁体材料化合物的单晶。
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公开(公告)号：US20110272585A1
公开(公告)日：2011-11-10
申请号：US13098642
申请日：2011-05-02
CPC分类号： C09K11/772 , C30B11/00 , C30B29/12 , G21K4/00
摘要： A halide scintillator material is disclosed. The material is single-crystalline and has a composition of the formula A3MBr6(1-x)Cl6x (such as Cs3CeBr6(1-x)Cl6x) or AM2Br7(1-x)Cl7x (such as CsCe2Br7(1-x)Cl7x), 0≦x≦1, wherein A consists essentially of Li, Na K, Rb, Cs or any combination thereof, and M consists essentially of Ce, Sc, Y, La, Lu, Gd, Pr, Tb, Yb, Nd or any combination thereof. Furthermore, a method of making halide scintillator materials of the above-mentioned compositions is disclosed. In one example, high-purity starting halides (such as CsBr, CeBr3, CsCl and CeCl3) are mixed and melted to synthesize a compound of the desired composition of the scintillator material. A single crystal of the scintillator material is then grown from the synthesized compound by the Bridgman method. The disclosed scintillator materials are suitable for making scintillation detectors used in applications such as medical imaging and homeland security.
摘要翻译： 公开了一种卤化物闪烁体材料。 该材料是单晶的并且具有式A3MBr6（1-x）Cl6x（例如Cs3CeBr6（1-x）Cl6x）或AM2Br7（1-x）Cl7x（例如CsCe2Br7（1-x）Cl7x）的组成） ，其中A基本上由Li，NaK，Rb，Cs或其组合组成，M基本上由Ce，Sc，Y，La，Lu，Gd，Pr，Tb，Yb，Nd或 其任何组合。 此外，公开了制备上述组合物的卤化物闪烁体材料的方法。 在一个实例中，将高纯度起始卤化物（例如CsBr，CeBr 3，CsCl和CeCl 3）混合并熔融以合成所需闪烁体材料组成的化合物。 然后通过Bridgman方法从合成的化合物生长闪烁体材料的单晶。 公开的闪烁体材料适用于制造用于医学成像和国土安全等应用的闪烁检测器。
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公开(公告)号：US08912498B2
公开(公告)日：2014-12-16
申请号：US13098642
申请日：2011-05-02
CPC分类号： C09K11/772 , C30B11/00 , C30B29/12 , G21K4/00
摘要： A halide scintillator material is disclosed. The material is single-crystalline and has a composition of the formula A3MBr6(1-x)Cl6x (such as Cs3CeBr6(1-x)Cl6x) or AM2Br7(1-x)Cl7x (such as CsCe2Br7(1-x)Cl7x), 0≦x≦1, wherein A consists essentially of Li, Na K, Rb, Cs or any combination thereof, and M consists essentially of Ce, Sc, Y, La, Lu, Gd, Pr, Tb, Yb, Nd or any combination thereof. Furthermore, a method of making halide scintillator materials of the above-mentioned compositions is disclosed. In one example, high-purity starting halides (such as CsBr, CeBr3, CsCl and CeCl3) are mixed and melted to synthesize a compound of the desired composition of the scintillator material. A single crystal of the scintillator material is then grown from the synthesized compound by the Bridgman method. The disclosed scintillator materials are suitable for making scintillation detectors used in applications such as medical imaging and homeland security.
摘要翻译： 公开了一种卤化物闪烁体材料。 该材料是单晶的并且具有式A3MBr6（1-x）Cl6x（例如Cs3CeBr6（1-x）Cl6x）或AM2Br7（1-x）Cl7x（例如CsCe2Br7（1-x）Cl7x）的组成） ，其中A基本上由Li，NaK，Rb，Cs或其组合组成，M基本上由Ce，Sc，Y，La，Lu，Gd，Pr，Tb，Yb，Nd或 其任何组合。 此外，公开了制备上述组合物的卤化物闪烁体材料的方法。 在一个实例中，将高纯度起始卤化物（例如CsBr，CeBr 3，CsCl和CeCl 3）混合并熔融以合成所需闪烁体材料组成的化合物。 然后通过Bridgman方法从合成的化合物生长闪烁体材料的单晶。 公开的闪烁体材料适用于制造用于医学成像和国土安全等应用的闪烁检测器。
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公开(公告)号：US08692203B1
公开(公告)日：2014-04-08
申请号：US13098654
申请日：2011-05-02
CPC分类号： C30B29/12 , C09K11/7733 , C30B11/003 , G01T1/20 , G01T1/202 , G01T3/06 , G21K4/00
摘要： The present disclosure discloses, in one arrangement, a single crystalline iodide scintillator material having a composition of the formula AM1−xEuxI3, A3M1−xEuxI5 and AM2(1−x)Eu2xI5, wherein A consists essentially of any alkali metal element (such as Li, Na K, Rb, Cs) or any combination thereof, M consists essentially of Sr, Ca, Ba or any combination thereof, and 0≦x≦1. In another arrangement, the above single crystalline iodide scintillator material can be made by first synthesizing a compound of the above composition and then forming a single crystal from the synthesized compound by, for example, the Vertical Gradient Freeze method. Applications of the iodide scintillator materials include radiation detectors and their use in medical and security imaging.
摘要翻译： 本公开在一种布置中公开了具有式AM1-xEuxI3，A3M1-xEuxI5和AM2（1-x）Eu2xI5组成的单结晶碘化物闪烁体材料，其中A基本上由任何碱金属元素（例如Li ，Na K，Rb，Cs）或其任何组合，M基本上由Sr，Ca，Ba或其任何组合组成，并且0和n 1; x和n 1; 在另一种布置中，上述单结晶碘化物闪烁体材料可以通过首先合成上述组成的化合物，然后通过例如垂直梯度冷冻法由合成的化合物形成单晶来制备。 碘化物闪烁体材料的应用包括辐射探测器及其在医疗和安全成像中的应用。
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公开(公告)号：US08598530B2
公开(公告)日：2013-12-03
申请号：US13098662
申请日：2011-05-02
IPC分类号： G01T1/20
CPC分类号： G21K4/00 , C09K11/7705 , C09K11/772 , C09K11/7773 , C30B11/00 , C30B29/12 , G21K2004/06
摘要： The present disclosure discloses, in one arrangement, a single crystalline chloride scintillator material having a composition of the formula A3MCl6, wherein A consists essentially of Cs and M consists essentially of Ce and Gd. In another arrangement, a chloride scintillator material is single-crystalline and has a composition of the formula AM2Cl7, wherein A consists essentially of Li, Na K, Rb, Cs or any combination thereof, and M consists essentially of Ce, Sc, Y, La, Lu, Gd, Pr, Tb, Yb, Nd or any combination thereof. Specific examples of these scintillator materials include single-crystalline Ce-doped KGd2Cl7 (KGd2(1-x)Ce2xCl7) and Ce-doped CsGd2Cl7(CsGd2(1-x)Ce2xCl7).
摘要翻译： 本公开在一种布置中公开了具有式A3MCl6组成的单晶氯化物闪烁体材料，其中A基本上由Cs组成，M基本上由Ce和Gd组成。 在另一种布置中，氯化物闪烁体材料是单晶的并且具有式AM2Cl7的组成，其中A基本上由Li，NaK，Rb，Cs或其任何组合组成，M基本上由Ce，Sc，Y， La，Lu，Gd，Pr，Tb，Yb，Nd或其任何组合。 这些闪烁体材料的具体实例包括单晶Ce掺杂的KGd2Cl7（KGd2（1-x）Ce2xCl7）和Ce掺杂的CsGd2Cl7（CsGd2（1-x）Ce2xCl7）。
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8.发明授权Rare-earth oxyorthosilicate scintillator crystals and method of making rare-earth oxyorthosilicate scintillator crystals 有权稀土氧原硅酸盐闪烁体晶体及稀土氧原硅酸盐闪烁体晶体的制备方法公开(公告)号：US08062419B1
公开(公告)日：2011-11-22
申请号：US12967442
申请日：2010-12-14
IPC分类号： C30B29/22
摘要： A method of making LSO scintillators with high light yield and short decay times is disclosed. In one arrangement, the method includes codoping LSO with cerium and another dopant from the IIA or IIB group of the periodic table of elements. The doping levels are chosen to tune the decay time of scintillation pulse within a broader range (between about ˜30 ns up to about ˜50 ns) than reported in the literature, with improved light yield and uniformity. In another arrangement, relative concentrations of dopants are chosen to achieve the desired light yield and decay time while ensuring crystal growth stability.
摘要翻译： 公开了一种制造具有高光产量和短衰减时间的LSO闪烁体的方法。 在一种布置中，该方法包括与元素的周期表的IIA或IIB族的铈和另一种掺杂剂的LSO共掺杂。 选择掺杂水平来调节闪烁脉冲在比文献中报道的更宽范围（约〜30ns至约〜50ns）之间的衰减时间，具有改善的光产量和均匀性。 在另一种布置中，选择掺杂剂的相对浓度以获得期望的光产率和衰变时间，同时确保晶体生长稳定性。
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9.发明授权PET scanner with emission and transmission structures in a checkerboard configuration 有权PET扫描仪，带有排列和传输结构的棋盘配置公开(公告)号：US08866086B2
公开(公告)日：2014-10-21
申请号：US13198804
申请日：2011-08-05
申请人： Christian J. Michel , Maurizio Conti , Ronald Grazioso , Piotr Szupryczynski , A. Andrew Carey , Larry Byars
发明人： Christian J. Michel , Maurizio Conti , Ronald Grazioso , Piotr Szupryczynski , A. Andrew Carey , Larry Byars
CPC分类号： G01T1/2985 , A61B6/037 , G01T1/1615 , G01T1/202
摘要： Apparatuses, computer-readable mediums, and methods are provided. In one embodiment, a positron emission tomography (“PET”) detector array is provided which includes a plurality of crystal elements arranged in a two-dimensional checkerboard configuration. In addition, there are empty spaces in the checkerboard configuration. In various embodiments, the empty spaces are filled with passive shielding, transmission source assemblies, biopsy instruments, surgical instruments, and/or electromagnetic sensors. In various embodiments, the crystal elements and the transmission source assemblies simultaneously perform emission/transmission acquisitions.
摘要翻译： 提供了设备，计算机可读介质和方法。 在一个实施例中，提供了包括以二维棋盘配置布置的多个晶体元件的正电子发射断层摄影（“PET”）检测器阵列。 另外，棋盘配置中有空格。 在各种实施例中，空的空间填充有无源屏蔽，传输源组件，活检仪器，外科器械和/或电磁传感器。 在各种实施例中，晶体元件和传输源组件同时执行发射/传输采集。
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10.发明申请Suppression Of Crystal Growth Instabilities During Production Of Rare-Earth Oxyorthosilicate Crystals 有权在稀土氧化硅酸盐晶体生产过程中抑制晶体生长不稳定性公开(公告)号：US20120080645A1
公开(公告)日：2012-04-05
申请号：US12894494
申请日：2010-09-30
摘要： Disclosed are a method of growing a rare-earth oxyorthosilicate crystal and a crystal grown using the method. A melt is prepared by melting a first substance including at least one rare-earth element and a second substance including at least one element from group 7 of the periodic table. A seed crystal is brought into contact with the surface of the melt and withdrawn to grow the crystal.
摘要翻译： 公开了一种生长稀土氧基原硅酸盐晶体的方法和使用该方法生长的晶体。 通过熔融含有至少一种稀土元素的第一物质和包含元素周期表第7族中的至少一种元素的第二物质来制备熔体。 将晶种与熔体的表面接触并取出以使晶体生长。
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