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公开(公告)号：US6124512A
公开(公告)日：2000-09-26
申请号：US156861
申请日：1998-09-18
IPC分类号： B01J23/00 , B01J27/053 , C07B39/00 , C07C17/12 , C07C67/307 , C07C17/00
CPC分类号： C07C17/12 , B01J23/00 , B01J27/053 , C07B39/00 , C07C67/307
摘要： Disclosed is a method of halogenating the ring of an aromatic compound. The aromatic compound is contacted with a halogenating agent in the presence of a heterogeneous catalyst. The catalyst is the calcination reaction product of:(A) 51 to 99 wt % of a support which comprises at least one inorganic oxide or hydroxide of at least one metal that is at least divalent and forms a metal-to-oxygen matrix during calcination; and(B) 1 to 49 wt % of at least one dopant which comprises a compound that places an element that is at least divalent, bonded to oxygen atoms, into said matrix during said calcination, resulting in the formation of an acidic solid.
摘要翻译： 公开了一种卤化芳族化合物的环的方法。 芳香族化合物在多相催化剂存在下与卤化剂接触。 催化剂是以下的煅烧反应产物：（A）51至99重量％的载体，其包含至少一种至少一种至少二价金属的无机氧化物或氢氧化物，并且在煅烧期间形成金属对氧基质 ; 和（B）1至49重量％的至少一种掺杂剂，其包括在所述煅烧期间将与氧原子键合的至少二价的元素放置到所述基质中的化合物，导致形成酸性固体。
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公开(公告)号：US06780960B2
公开(公告)日：2004-08-24
申请号：US10200825
申请日：2002-07-22
申请人： Michael C. Hausladen , Jin-O Choi
发明人： Michael C. Hausladen , Jin-O Choi
IPC分类号： C08G7310
CPC分类号： C08G73/106 , C08G73/1032
摘要： A method of making a solution of a polyimide from a diamine monomer and a dianhydride monomer is disclosed. A solution or slurry of one of the monomers in a solvent that boils at a temperature between about 80° C. and about 160° C. is prepared. The solution or slurry is heated to a temperature between about 80° C. and about 160° C. and the other monomer is slowly added to the solution or slurry. Polyamic acid that is formed quickly imidizes to form the polyimide.
摘要翻译： 公开了从二胺单体和二酐单体制备聚酰亚胺溶液的方法。 制备在约80℃至约160℃的温度下沸腾的溶剂中的一种单体的溶液或浆液。 将溶液或浆液加热至约80℃至约160℃的温度，并将其它单体缓慢加入到溶液或浆液中。 形成的聚酰胺酸快速酰亚胺化以形成聚酰亚胺。
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3.发明授权公开(公告)号：US06549176B2
公开(公告)日：2003-04-15
申请号：US09929123
申请日：2001-08-15
申请人： Michael C. Hausladen
发明人： Michael C. Hausladen
IPC分类号： H01Q136
CPC分类号： H01Q1/2225 , G06K19/07749 , G06K19/0775 , G06K19/07779 , G06K19/07783 , H01Q1/22 , H01Q7/00 , Y10T29/49202
摘要： A radio frequency-identification (RFID) tag comprises a substrate, a single, continuous antenna having a plurality of spiral turns and end portions that are integral with the spiral turns, and an integrated circuit. The spiral turns are disposed on the substrate and at least one of the end portions crosses over at least some of the spiral turns. One end portion of the antenna is integrally connected to the innermost spiral turn and extends toward an outermost spiral turn to cross over at least some of the spiral turns. Another end portion of the antenna may be integrally connected to the outermost spiral turn and extend toward the innermost spiral turn to cross over at least some of the other spiral turns. The end portion(s) may cross over the spiral turns on the side of the substrate on which the spiral turns are disposed or on the opposite side.
摘要翻译： 射频识别（RFID）标签包括基板，具有多个螺旋形匝的单个连续天线和与螺旋形匝成一体的端部，以及集成电路。 螺旋匝设置在基板上，并且至少一个端部与至少一些螺旋匝交叉。 天线的一个端部与最内螺旋线一体地连接，并且朝着最外面的螺旋转弯延伸，以交叉至少一些螺旋线。 天线的另一端部可以一体地连接到最外面的螺旋形转向并且朝向最内螺旋形转弯延伸，以交叉至少一些其它螺旋形匝。 端部可以在其上设置有螺旋匝的基板的侧面上的螺旋形匝上或在相对侧上交叉。
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公开(公告)号：US06451955B1
公开(公告)日：2002-09-17
申请号：US09676295
申请日：2000-09-28
申请人： Michael C. Hausladen , Jin-O Choi
发明人： Michael C. Hausladen , Jin-O Choi
IPC分类号： C08G7310
CPC分类号： C08G73/106 , C08G73/1032
摘要： A method of making a solution of a polyimide from a diamine monomer and a dianhydride monomer is disclosed. A solution or slurry of one of the monomers in a solvent that boils at a temperature between about 80° C. and about 160° C. is prepared. The solution or slurry is heated to a temperature between about 80° C. and about 160° C. and the other monomer is slowly added to the solution or slurry. Polyamic acid that is formed quickly imidizes to form the polyimide.
摘要翻译： 公开了从二胺单体和二酐单体制备聚酰亚胺溶液的方法。 制备在约80℃至约160℃的温度下沸腾的溶剂中的一种单体的溶液或浆液。 将溶液或浆液加热至约80℃至约160℃的温度，并将其它单体缓慢加入到溶液或浆液中。 形成的聚酰胺酸快速酰亚胺化以形成聚酰亚胺。
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公开(公告)号：US5866709A
公开(公告)日：1999-02-02
申请号：US982611
申请日：1997-12-02
IPC分类号： C07C253/28 , C07C253/00 , C07C253/34 , C07C255/50 , C07C255/00
CPC分类号： C07C253/00
摘要： Disclosed is a process for making an aromatic nitrile by reacting a benzotrichloride with an ammonium halide in the presence of an oxygen-donating initiator at a temperature of about 150.degree. to about 250.degree. C. An optional catalyst of a metal oxide or a metal salt can be used if desired.
摘要翻译： 公开了一种在约150至约250℃的温度下，在给氧引发剂存在下，使苯并三氯化物与卤化铵反应制备芳族腈的方法。任选的金属氧化物或金属盐的催化剂 如果需要可以使用。
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公开(公告)号：US06486783B1
公开(公告)日：2002-11-26
申请号：US09665311
申请日：2000-09-19
IPC分类号： G08B1314
CPC分类号： G06K19/07771 , G06K19/077 , G06K19/07749 , G06K19/0776 , G08B13/244
摘要： A composite containing an RFID can be mounted on, in, or adjacent a metal object without de-tuning of the antenna of the RFID. The composite includes a first RFID or a EAS device-containing layer, and a foamable material layer held in proximity with the first layer. The foamable material layer expands in size and reduces in density when subjected to external stimuli, such as heat or microwaves. The foamable layer may comprise an intumescent material, and may have RF radiation-absorbing material filler. Pressure sensitive adhesive, when the composite is in a label form, may be used to mount the composite on or adjacent a metal object after printing of the printable surface of the composite, and the foamable material layer is subjected to the external stimuli after printing and either before or after mounting on or adjacent the metal object.
摘要翻译： 包含RFID的复合材料可以安装在金属物体上，金属物体中或附近，而不会对RFID的天线进行去调谐。 复合材料包括第一RFID或含有EAS的装置的层，以及保持在第一层附近的可发泡材料层。 当受到诸如热或微波之类的外部刺激时，可发泡材料层的尺寸扩大并且密度降低。 可发泡层可以包括膨胀材料，并且可以具有RF辐射吸收材料填料。 当复合材料为标签形式时，压敏粘合剂可用于在复印材料的可印刷表面印刷之后将复合材料安装在金属物体上或附近，并且可发泡材料层在印刷之后受到外部刺激， 在安装在金属物体上或邻近金属物体之前或之后。
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公开(公告)号：US06225514B1
公开(公告)日：2001-05-01
申请号：US09547385
申请日：2000-04-11
IPC分类号： C07C1700
CPC分类号： C07C17/12 , B01J23/00 , B01J27/053 , C07B39/00 , C07C67/307 , C07C25/06 , C07C25/02 , C07C69/76
摘要： Disclosed is a method of halogenating the ring of an aromatic compound. The aromatic compound is contacted with a halogenating agent in the presence of a heterogeneous catalyst. The catalyst is the calcination reaction product of: (A) 51 to 99 wt % of a support which comprises at least one inorganic oxide or hydroxide of at least one metal that is at least divalent and forms a metal-to-oxygen matrix during calcination; and (B) 1 to 49 wt % of at least one dopant which comprises a compound that places an element that is at least divalent, bonded to oxygen atoms, into said matrix during said calcination, resulting in the formation of an acidic solid.
摘要翻译： 公开了一种卤化芳族化合物的环的方法。 芳香族化合物在多相催化剂存在下与卤化剂接触。 催化剂是以下的煅烧反应产物：（A）51至99重量％的载体，其包含至少一种至少一种至少二价金属的无机氧化物或氢氧化物，并且在煅烧期间形成金属对氧基质 ; 和（B）1至49重量％的至少一种掺杂剂，其包括在所述煅烧期间将与氧原子键合的至少二价的元素放置到所述基质中的化合物，导致形成酸性固体。
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公开(公告)号：US5998670A
公开(公告)日：1999-12-07
申请号：US40612
申请日：1998-03-18
IPC分类号： C07C319/24 , C07C321/30 , C07C323/09 , C07C321/00
CPC分类号： C07C319/24
摘要： Disclosed is a method of making a substituted diphenyldisulfide from a substituted thiophenol. A two phase reaction mixture is prepared which comprises a substituted thiophenol having the general formula ##STR1## hydrogen peroxide, water, an organic solvent, a basic salt that will give a pH between about 7 and about 10, and an optional flocculating agent. In the formula, R is selected from the group consisting of halogen, alkyl from C.sub.1 to C.sub.6, alkoxy from C.sub.1 to C.sub.6, or nitro. After the exothermic reaction is complete, the reaction mixture is cooled to crystallize the substituted diphenyldisulfide product. The symmetrical product precipitates preferentially over the unsymmetrical product, thereby enhancing the purity of the product over the purity of the starting material. Optionally, the organic solvent and the aqueous phase are recycled.
摘要翻译： 公开了从取代的苯硫酚制备取代的二苯基二硫化物的方法。 制备两相反应混合物，其包含具有通式过氧化氢，水，有机溶剂，将产生约7至约10的pH的碱性盐和任选的絮凝剂的取代的苯硫酚。 在该式中，R选自卤素，C1至C6的烷基，C1至C6的烷氧基或硝基。 放热反应完成后，冷却反应混合物以结晶取代的二苯基二硫化物产物。 对称产物优先于非对称产物沉淀，从而提高产品的纯度高于起始原料的纯度。 任选地，有机溶剂和水相再循环。
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