公开(公告)号：US06406548B1

公开(公告)日：2002-06-18

申请号：US09618830

申请日：2000-07-18

申请人： Michael Donovan ,  Robert P. Jansen ,  Richard C. Reisig ,  Marc Hlavacek ,  Gordon Walker ,  John C. Williams

发明人： Michael Donovan ,  Robert P. Jansen ,  Richard C. Reisig ,  Marc Hlavacek ,  Gordon Walker ,  John C. Williams

IPC分类号： C13D316

CPC分类号： C13B10/00 ,  C13B20/00 ,  C13B20/165

摘要： A process for producing sugar from cane includes the step of filtering a sucrose-containing feed juice, which has been obtained from macerated sugar cane, through a first ultrafiltration membrane that has a first molecular weight cutoff. This ultrafiltration step produces a first ultrafiltration permeate and a first ultrafiltration retentate. The first ultrafiltration permeate is filtered through a second ultrafiltration membrane that has a second molecular weight cutoff that is lower than the first molecular weight cutoff. This second ultrafiltration step produces a second ultrafiltration permeate and a second ultrafiltration retentate. The second ultrafiltration permeate is nanofiltered through a nanofiltration membrane, thereby producing a nanofiltration permeate and a nanofiltration retentate. The nanofiltration retentate has a higher concentration of sucrose on a dry solids basis than the feed juice in step (a), and can be used in evaporation and crystallization operations to produce crystals of white sugar. The process can optionally include ion exchange and/or electrodialysis purification steps, prior to or after the nanofiltration step. Recycle syrups can be treated with a chromatographic separator to remove excess invert, ash and color.

摘要翻译： 从甘蔗生产糖的方法包括通过具有第一分子量截留值的第一超滤膜过滤从浸出的甘蔗获得的含蔗糖的进料汁的步骤。 该超滤步骤产生第一超滤渗透物和第一超滤滞留物。 第一超滤渗透物通过具有低于第一分子量截止值的第二分子量截止值的第二超滤膜过滤。 该第二超滤步骤产生第二超滤渗透物和第二超滤滞留物。 第二超滤渗透物通过纳滤膜进行纳滤，从而产生纳滤膜渗透物和纳滤膜渗余物。 纳米过滤滞留物在干固体基础上具有比步骤（a）中的进料汁更高的蔗糖浓度，并且可用于蒸发和结晶操作以产生白糖晶体。 该方法可任选地包括在纳滤过程之前或之后的离子交换和/或电渗析纯化步骤。 回收糖浆可以用色谱分离器处理，以去除多余的反转，灰分和颜色。

公开(公告)号：US06406547B1

公开(公告)日：2002-06-18

申请号：US09618416

申请日：2000-07-18

申请人： Michael Donovan ,  Robert P. Jansen ,  Marc Hlavacek ,  Gordon Walker ,  John C. Williams

发明人： Michael Donovan ,  Robert P. Jansen ,  Marc Hlavacek ,  Gordon Walker ,  John C. Williams

IPC分类号： C13D316

CPC分类号： C13B10/00 ,  C13B20/00 ,  C13B20/165

摘要： A process for producing sugar from beets includes the step of filtering a sucrose-containing feed juice, which has been obtained by diffusion from sliced sugar beets, through a first ultrafiltration membrane that has a first molecular weight cutoff. This ultrafiltration step produces a first ultrafiltration permeate and a first ultrafiltration retentate. The first ultrafiltration permeate is filtered through a second ultrafiltration membrane that has a second molecular weight cutoff that is lower than the first molecular weight cutoff. This second ultrafiltration step produces a second ultrafiltration permeate and a second ultrafiltration retentate. The second ultrafiltration permeate is nanofiltered through a nanofiltration membrane, thereby producing a nanofiltration permeate and a nanofiltration retentate. The nanofiltration retentate has a higher concentration of sucrose on a dry solids basis than the feed juice in step (a), and can be used in evaporation and crystallization operations to produce crystals of white sugar. The process can optionally include ion exchange and/or electrodialysis purification steps, prior to or after the nanofiltration step. Recycle syrups can be treated with enzyme or a chromatographic separator to remove raffinose.

摘要翻译： 从甜菜制备糖的方法包括将通过从切片的甜菜中扩散获得的含蔗糖的进料汁通过具有第一分子量截留值的第一超滤膜过滤的步骤。 该超滤步骤产生第一超滤渗透物和第一超滤滞留物。 第一超滤渗透物通过具有低于第一分子量截止值的第二分子量截止值的第二超滤膜过滤。 该第二超滤步骤产生第二超滤渗透物和第二超滤滞留物。 第二超滤渗透物通过纳滤膜进行纳滤，从而产生纳滤膜渗透物和纳滤膜渗余物。 纳米过滤滞留物在干固体基础上具有比步骤（a）中的进料汁更高的蔗糖浓度，并且可用于蒸发和结晶操作以产生白糖晶体。 该方法可任选地包括在纳滤过程之前或之后的离子交换和/或电渗析纯化步骤。 可以用酶或色谱分离器处理回收糖浆以除去棉子糖。

公开(公告)号：US06406546B1

公开(公告)日：2002-06-18

申请号：US09618234

申请日：2000-07-18

申请人： Michael Donovan ,  Marc Hlavacek

发明人： Michael Donovan ,  Marc Hlavacek

IPC分类号： C13D116

CPC分类号： C13B30/12 ,  C13B20/165

摘要： A nanofiltration process for obtaining sucrose uses a feed syrup, such as molasses, that comprises sucrose and no less than about 2% by weight invert sugars (on a dry solids basis). The nanofiltration produces a permeate and retentate. The nanofiltration permeate will comprise invert sugars that have passed from the feed through the nanofiltration membrane, and preferably will also comprise ash from the feed. The nanofiltration retentate has a higher concentration of sucrose and a lower concentration of invert sugars than the feed syrup. Sucrose can then be crystallized from the nanofiltration retentate. The reduction of the invert content in the syrup facilitates crystallization and thus enhances sucrose recovery.

摘要翻译： 用于获得蔗糖的纳滤方法使用包含蔗糖和不少于约2重量％转化糖（基于干固体）的饲料糖浆，例如糖蜜。 纳米过滤产生渗透物和渗余物。 纳米过滤渗透物将包含从进料通过纳滤膜的转化糖，并且优选还包含来自进料的灰分。 纳滤过滤滞留物具有较高浓度的蔗糖和较低浓度的转化糖比饲料糖浆。 然后可以从纳滤过滤滞留物中结晶蔗糖。 糖浆中反转含量的减少有助于结晶，从而提高蔗糖回收率。

公开(公告)号：US5759283A

公开(公告)日：1998-06-02

申请号：US645702

申请日：1996-05-14

申请人： Eric P. Ekern ,  Bimal Goculdas ,  Michael Donovan ,  Marc Hlavacek

发明人： Eric P. Ekern ,  Bimal Goculdas ,  Michael Donovan ,  Marc Hlavacek

IPC分类号： B01D61/14 ,  B01D61/16 ,  C13B20/00 ,  C13B20/02 ,  C13B20/04 ,  C13B20/12 ,  C13B20/16 ,  C13D1/08 ,  C13D1/14 ,  C13D3/12 ,  C13D3/16

CPC分类号： C13B20/02 ,  B01D61/145 ,  B01D61/147 ,  B01D61/16 ,  C13B20/00 ,  C13B20/04 ,  C13B20/12 ,  C13B20/165 ,  Y02P40/44

摘要： An efficient method for manufacturing a purified juice product from sugar beets. Untreated beet juice is initially prelimed using lime and CaCO.sub.3 to produce a prelimed juice product. Instead of subjecting the prelimed product to main liming and dual carbonation stages, the product is delivered to a porous filtration membrane which allows sugar molecules to pass therethrough which preventing the passage of solid matter and dissolved impurities. Optimum results are achieved if the prelimed product flows across the membrane from end to end. The membrane permeate is thereafter combined with CO.sub.2(g) in a single carbonation stage to remove dissolved lime. This step generates a purified juice product which can be processed to manufacture pure crystalline sugar. The membrane retentate can be combined with water and refiltered to collect residual sugar materials. The foregoing process uses less energy and raw materials (e.g. lime) compared with conventional methods.

摘要翻译： 从甜菜制造纯化果汁产品的有效方法。 未处理的甜菜汁最初使用石灰和CaCO3预先制备预制的果汁产品。 代替将预制产物进行主要石灰和双重碳酸化阶段，将产物输送到多孔过滤膜，其允许糖分子通过，从而阻止固体物质和溶解的杂质的通过。 如果预备的产品从端到端流过膜，则获得最佳结果。 然后将膜渗透物与CO 2（g）在单一碳酸化阶段中合并以除去溶解的石灰。 该步骤产生纯化的果汁产品，其可以被加工以制造纯结晶糖。 膜保留物可以与水结合并重新过滤以收集残留的糖材料。 与常规方法相比，上述方法使用更少的能量和原料（例如石灰）。

公开(公告)号：US06440222B1

公开(公告)日：2002-08-27

申请号：US09618831

申请日：2000-07-18

申请人： Michael Donovan ,  Robert P. Jansen ,  Richard C. Reisig ,  Marc Hlavacek ,  Gordon Walker ,  John C. Williams

发明人： Michael Donovan ,  Robert P. Jansen ,  Richard C. Reisig ,  Marc Hlavacek ,  Gordon Walker ,  John C. Williams

IPC分类号： C13D108

CPC分类号： B01D61/142 ,  B01D61/16 ,  B01D2311/04 ,  C13B10/00 ,  C13B20/00 ,  C13B20/165 ,  B01D2311/103 ,  B01D2311/246 ,  B01D2311/2623 ,  B01D2311/268

摘要： A process for producing sugar from beets includes the step of filtering a sucrose-containing feed juice, which has been obtained from macerated sugar beets, through a first ultrafiltration membrane that has a first molecular weight cutoff. This ultrafiltration step produces a first ultrafiltration permeate and a first ultrafiltration retentate. The first ultrafiltration permeate is filtered through a second ultrafiltration membrane that has a second molecular weight cutoff that is lower than the first molecular weight cutoff. This second ultrafiltration step produces a second ultrafiltration permeate and a second ultrafiltration retentate. The second ultrafiltration permeate is nanofiltered through a nanofiltration membrane, thereby producing a nanofiltration permeate and a nanofiltration retentate. The nanofiltration retentate has a higher concentration of sucrose on a dry solids basis than the feed juice in step (a), and can be used in evaporation and crystallization operations to produce crystals of white sugar. The process can optionally include ion exchange and/or electrodialysis purification steps, prior to or after the nanofiltration step. Recycle syrups can be treated with enzyme or a chromatographic separator to remove raffinose.

摘要翻译： 从甜菜制备糖的方法包括通过具有第一分子量截留值的第一超滤膜过滤从浸出的甜菜获得的含蔗糖的进料汁的步骤。 该超滤步骤产生第一超滤渗透物和第一超滤滞留物。 第一超滤渗透物通过具有低于第一分子量截止值的第二分子量截止值的第二超滤膜过滤。 该第二超滤步骤产生第二超滤渗透物和第二超滤滞留物。 第二超滤渗透物通过纳滤膜进行纳滤，从而产生纳滤膜渗透物和纳滤膜渗余物。 纳米过滤滞留物在干固体基础上具有比步骤（a）中的进料汁更高的蔗糖浓度，并且可用于蒸发和结晶操作以产生白糖晶体。 该方法可任选地包括在纳滤过程之前或之后的离子交换和/或电渗析纯化步骤。 可以用酶或色谱分离器处理回收糖浆以除去棉子糖。

公开(公告)号：US06355110B1

公开(公告)日：2002-03-12

申请号：US09441988

申请日：1999-11-17

申请人： Michael Donovan ,  Marc Hlavacek

发明人： Michael Donovan ,  Marc Hlavacek

IPC分类号： C13D316

CPC分类号： C13B30/12 ,  C13B20/165

摘要： A nanofiltration process for obtaining sucrose uses a feed syrup, such as molasses, that comprises sucrose and no less than about 3% by weight invert sugars (on a dry solids basis). The nanofiltration produces a permeate and retentate. The nanofiltration permeate will comprise invert sugars that have passed from the feed through the nanofiltration membrane, and preferably will also comprise ash from the feed. The nanofiltration retentate has a higher concentration of sucrose and a lower concentration of invert sugars than the feed syrup. Sucrose can then be crystallized from the nanofiltration retentate. The reduction of the invert content in the syrup facilitates crystallization and thus enhances sucrose recovery.

摘要翻译： 用于获得蔗糖的纳滤方法使用包含蔗糖和不少于约3重量％转化糖（以干固体为基准）的饲料糖浆，例如糖蜜。 纳米过滤产生渗透物和渗余物。 纳米过滤渗透物将包含从进料通过纳滤膜的转化糖，并且优选还包含来自进料的灰分。 纳滤过滤滞留物具有较高浓度的蔗糖和较低浓度的转化糖比饲料糖浆。 然后可以从纳滤过滤滞留物中结晶蔗糖。 糖浆中反转含量的减少有助于结晶，从而提高蔗糖回收率。

公开(公告)号：US08163172B2

公开(公告)日：2012-04-24

申请号：US13079188

申请日：2011-04-04

申请人： Jean-Luc Beulay ,  Virginie Buisson ,  Sebastien Cirou ,  Cecile Delbos ,  Marc Hlavacek ,  Frans Mels ,  Rene Reinbigler ,  Jean-Louis Weissenbach

发明人： Jean-Luc Beulay ,  Virginie Buisson ,  Sebastien Cirou ,  Cecile Delbos ,  Marc Hlavacek ,  Frans Mels ,  Rene Reinbigler ,  Jean-Louis Weissenbach

IPC分类号： B01D36/00 ,  C12M1/12

CPC分类号： B01D36/00 ,  C12M1/12 ,  C12M47/12 ,  Y10T436/25375 ,  Y10T436/2575

摘要： Installation for treating a biological liquid, including a circulation pump (5), a filter element (9), a container for collecting treated liquid, a first circuit section connecting a source of said biological liquid to an inlet orifice of said filter element (9), including a circuit element adapted to cooperate with said circulation pump (5); a second circuit section, connecting an outlet orifice of said filter element (9) to said treated liquid collecting container; characterized in that said treated liquid collecting container, said first circuit section and said second circuit section are disposable and said installation further includes a first cart (1) carrying said pump (5) and a second cart (2) including a housing (14) for said collecting container, separable from the first cart (1) and adapted to be at least partly nested in said first cart (1).

摘要翻译： 用于处理包括循环泵（5），过滤元件（9），用于收集处理液体的容器的生物液体的安装，将所述生物液体源连接到所述过滤元件（9）的入口孔的第一回路段 ），包括适于与所述循环泵（5）配合的电路元件; 第二电路部分，将所述过滤元件（9）的出口孔连接到所述处理过的液体收集容器; 其特征在于，所述处理过的液体收集容器，所述第一回路部分和所述第二回路部分是一次性的，并且所述装置还包括承载所述泵（5）的第一推车（1）和包括壳体（14）的第二推车（2） 用于所述收集容器，所述收集容器可与所述第一推车（1）分离并且适于至少部分地嵌套在所述第一推车（1）中。

公开(公告)号：US20120168390A1

公开(公告)日：2012-07-05

申请号：US13420906

申请日：2012-03-15

申请人： Jean-Luc Beulay ,  Virginie Buisson ,  Sebastien Cirou ,  Cecile Delbos ,  Marc Hlavacek ,  Frans Mels ,  Rene Reinbigler ,  Jean-Louis Weissenbach

发明人： Jean-Luc Beulay ,  Virginie Buisson ,  Sebastien Cirou ,  Cecile Delbos ,  Marc Hlavacek ,  Frans Mels ,  Rene Reinbigler ,  Jean-Louis Weissenbach

IPC分类号： B01D37/00 ,  B01D37/04

CPC分类号： B01D36/00 ,  C12M1/12 ,  C12M47/12 ,  Y10T436/25375 ,  Y10T436/2575

摘要： Installation for treating a biological liquid, including a circulation pump (5), a filter element (9), a container for collecting treated liquid, a first circuit section connecting a source of said biological liquid to an inlet orifice of said filter element (9), including a circuit element adapted to cooperate with said circulation pump (5); a second circuit section, connecting an outlet orifice of said filter element (9) to said treated liquid collecting container; characterized in that said treated liquid collecting container, said first circuit section and said second circuit section are disposable and said installation further includes a first cart (1) carrying said pump (5) and a second cart (2) including a housing (14) for said collecting container, separable from the first cart (1) and adapted to be at least partly nested in said first cart (1).

摘要翻译： 用于处理包括循环泵（5），过滤元件（9），用于收集处理液体的容器的生物液体的安装，将所述生物液体源连接到所述过滤元件（9）的入口孔的第一回路段 ），包括适于与所述循环泵（5）配合的电路元件; 第二电路部分，将所述过滤元件（9）的出口孔连接到所述处理过的液体收集容器; 其特征在于，所述处理过的液体收集容器，所述第一回路部分和所述第二回路部分是一次性的，并且所述装置还包括承载所述泵（5）的第一推车（1）和包括壳体（14）的第二推车（2） 用于所述收集容器，所述收集容器可与所述第一推车（1）分离并且适于至少部分地嵌套在所述第一推车（1）中。

公开(公告)号：US5147552A

公开(公告)日：1992-09-15

申请号：US735894

申请日：1991-07-25

申请人： Marc Hlavacek ,  John Dodds ,  Jean-Michel Bauer

发明人： Marc Hlavacek ,  John Dodds ,  Jean-Michel Bauer

IPC分类号： B01D61/22 ,  B01D37/04 ,  B01D65/02

CPC分类号： B01D65/02 ,  B01D37/043 ,  B01D2321/2025

摘要： A method of and an apparatus for tangential filtration with filter cleaning in which a fluid to be filtered forms a liquid loop and circulates tangentially to one surface of a membrane at a pressure Ph in which a filtrate flows from the other surface of the membrane through a pipe, provided with a flow meter and a first valve, to a tank at atmospheric pressure Pa, filtration taking place by virtue of a positive transmembranal pressure Ph - Pa. In the filtration phase, the hydrodynamic pressure Ph is adjusted by means of a second regulable valve. During the filter cleaning phase the first valve is closed and at the same time the second valve is slightly opened, the second valve is suddenly opened, the first valve is opened and the second valve is progressively closed. The method and apparatus in particularly suited to the filtration of corrosive liquids.

摘要翻译： 一种用于具有过滤器清洁的切向过滤的方法和装置，其中待过滤的流体形成液体回路并且以压力Ph切向地循环到膜的一个表面，其中滤液从膜的另一表面流过 管道，设有流量计和第一阀，在大气压力Pa下进行过滤，通过正跨膜压力Ph-Pa进行过滤。在过滤阶段，流体动力压力Ph通过第二次 调节阀 在过滤器清洁阶段期间，第一阀关闭，同时第二阀略微打开，第二阀突然打开，第一阀打开，第二阀逐渐关闭。 特别适用于过滤腐蚀性液体的方法和设备。

公开(公告)号：US20110174716A1

公开(公告)日：2011-07-21

申请号：US13079188

申请日：2011-04-04

申请人： Jean-Luc Beulay ,  Virginie Buisson ,  Sebastien Cirou ,  Cecile Delbos ,  Marc Hlavacek ,  Frans Mels ,  Rene Reinbigler ,  Jean-Louis Weissenbach

发明人： Jean-Luc Beulay ,  Virginie Buisson ,  Sebastien Cirou ,  Cecile Delbos ,  Marc Hlavacek ,  Frans Mels ,  Rene Reinbigler ,  Jean-Louis Weissenbach

IPC分类号： B01D29/00

CPC分类号： B01D36/00 ,  C12M1/12 ,  C12M47/12 ,  Y10T436/25375 ,  Y10T436/2575

摘要： Installation for treating a biological liquid, including a circulation pump (5), a filter element (9), a container for collecting treated liquid, a first circuit section connecting a source of said biological liquid to an inlet orifice of said filter element (9), including a circuit element adapted to cooperate with said circulation pump (5); a second circuit section, connecting an outlet orifice of said filter element (9) to said treated liquid collecting container; characterized in that said treated liquid collecting container, said first circuit section and said second circuit section are disposable and said installation further includes a first cart (1) carrying said pump (5) and a second cart (2) including a housing (14) for said collecting container, separable from the first cart (1) and adapted to be at least partly nested in said first cart (1).

摘要翻译： 用于处理包括循环泵（5），过滤元件（9），用于收集处理液体的容器的生物液体的安装，将所述生物液体源连接到所述过滤元件（9）的入口孔的第一回路段 ），包括适于与所述循环泵（5）配合的电路元件; 第二电路部分，将所述过滤元件（9）的出口孔连接到所述处理过的液体收集容器; 其特征在于，所述处理过的液体收集容器，所述第一回路部分和所述第二回路部分是一次性的，并且所述装置还包括承载所述泵（5）的第一推车（1）和包括壳体（14）的第二推车（2） 用于所述收集容器，所述收集容器可与所述第一推车（1）分离并且适于至少部分地嵌套在所述第一推车（1）中。