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    CHEMICAL REACTOR HAVING WOVEN WIRE MESH PRODUCT AS A RETAINING DEVICE FOR PARTICLES
    1.
    发明申请
    CHEMICAL REACTOR HAVING WOVEN WIRE MESH PRODUCT AS A RETAINING DEVICE FOR PARTICLES 有权
    具有作为颗粒保留装置的WOVEN MESE产品的化学反应器

    公开(公告)号：US20130296610A1

    公开(公告)日：2013-11-07

    申请号：US13988326

    申请日：2011-11-15

    申请人： Michael Merkel ,  Karl-Heinz Wilke ,  Thomas Knauf

    发明人： Michael Merkel ,  Karl-Heinz Wilke ,  Thomas Knauf

    IPC分类号： B01J8/02

    CPC分类号： B01J8/0292 ,  B01J8/025 ,  B01J8/44 ,  B01J2208/00884 ,  Y10T428/12424

    摘要： In a chemical reactor for heterogeneously catalysed reaction of a fluid, comprising a holding device for catalyst particles and/or inert particles (80, 100) through which the fluid flows, the side of the holding device lying upstream when viewed in the direction of flow of the fluid comprises knitted wire mesh fabric (50), and the average clear mesh width of the knitted wire fabric (50) is smaller than the average particle size x50.3 of the particles (80, 100). The invention furthermore relates to a process for reaction of a fluid, wherein the reaction is carried out in a reactor according to the invention in the presence of heterogeneous catalyst particles (80) and the catalyst particles (80) are arranged in the holding device for catalyst particles (80). The invention also provides the use of knitted wire mesh fabric (50) as a holding device for catalyst particles and/or inert particles (80, 100) in chemical reactors.

    摘要翻译： 在用于流体的异质催化反应的化学反应器中，包括用于催化剂颗粒的保持装置和/或流体流过的惰性颗粒（80,100），当从流动方向观察时，保持装置的侧面位于上游 的流体包括针织丝网织物（50），并且针织线织物（50）的平均透明网格宽度小于颗粒（80,100）的平均粒径×50.3。 本发明还涉及一种流体反应的方法，其中反应在非均相催化剂颗粒（80）存在的情况下在根据本发明的反应器中进行，催化剂颗粒（80）被布置在用于 催化剂颗粒（80）。 本发明还提供了在化学反应器中使用针织丝网织物（50）作为催化剂颗粒和/或惰性颗粒（80,100）的保持装置。

    Chemical reactor with knitted wire mesh fabric as a holding device for particles
    3.
    发明授权
    Chemical reactor with knitted wire mesh fabric as a holding device for particles 有权
    化学反应器用针织丝网织物作为颗粒保持装置

    公开(公告)号：US09364810B2

    公开(公告)日：2016-06-14

    申请号：US13988326

    申请日：2011-11-15

    申请人： Michael Merkel ,  Karl-Heinz Wilke ,  Thomas Knauf

    发明人： Michael Merkel ,  Karl-Heinz Wilke ,  Thomas Knauf

    IPC分类号： B01J8/02 ,  C07C209/00 ,  B01J8/44

    CPC分类号： B01J8/0292 ,  B01J8/025 ,  B01J8/44 ,  B01J2208/00884 ,  Y10T428/12424

    摘要： In a chemical reactor for heterogeneously catalyzed reaction of a fluid, comprising a holding device for catalyst particles and/or inert particles (80, 100) through which the fluid flows, the side of the holding device lying upstream when viewed in the direction of flow of the fluid comprises knitted wire mesh fabric (50), and the average clear mesh width of the knitted wire fabric (50) is smaller than the average particle size x50.3 of the particles (80, 100). The invention furthermore relates to a process for reaction of a fluid, wherein the reaction is carried out in a reactor according to the invention in the presence of heterogeneous catalyst particles (80) and the catalyst particles (80) are arranged in the holding device for catalyst particles (80). The invention also provides the use of knitted wire mesh fabric (50) as a holding device for catalyst particles and/or inert particles (80, 100) in chemical reactors.

    摘要翻译： 在用于流体的非均相催化反应的化学反应器中，包括用于催化剂颗粒的保持装置和/或流体流过的惰性颗粒（80,100），当从流动方向观察时，保持装置的侧面位于上游 的流体包括针织丝网织物（50），并且针织线织物（50）的平均透明网格宽度小于颗粒（80,100）的平均粒径×50.3。 本发明还涉及一种流体反应的方法，其中反应在非均相催化剂颗粒（80）存在的情况下在根据本发明的反应器中进行，催化剂颗粒（80）被布置在用于 催化剂颗粒（80）。 本发明还提供了在化学反应器中使用针织丝网织物（50）作为催化剂颗粒和/或惰性颗粒（80,100）的保持装置。

    PROCESS FOR PREPARING AROMATIC AMINES
    4.
    发明申请
    PROCESS FOR PREPARING AROMATIC AMINES 有权
    制备芳香胺的方法

    公开(公告)号：US20140128638A1

    公开(公告)日：2014-05-08

    申请号：US13978479

    申请日：2012-01-06

    申请人： Michael Merkel ,  Karl-Heinz Wilke ,  Peter Lehner ,  Andre Lago ,  Erwin Dieterich

    发明人： Michael Merkel ,  Karl-Heinz Wilke ,  Peter Lehner ,  Andre Lago ,  Erwin Dieterich

    IPC分类号： C07C209/36

    CPC分类号： C07C209/36 ,  C07C211/46

    摘要： The invention relates to a process for the continuous preparation of aromatic amines by hydrogenation of the corresponding nitroaromatics in the presence of catalysts arranged in reaction spaces, in which an adiabatically operated reaction space RA is connected downstream of an isothermally operated reaction space RI and RA additionally also has a separate feed for the nitroaromatic to be hydrogenated, RI is fed with the nitroaromatic to be hydrogenated from the start to the end of the hydrogenation, and the product mixture emerging from RI is fed into RA from the start to the end of the hydrogenation, wherein RA can additionally be fed via the separate feed with the nitroaromatic to be hydrogenated.

    摘要翻译： 本发明涉及通过在反应空间中排列的催化剂存在下氢化相应的硝基芳族化合物来连续制备芳族胺的方法，其中绝热操作的反应空间RA另外连接等温操作的反应空间RI和RA的下游 还具有用于待氢化的硝基芳族化合物的单独进料，从加氢的开始到结束，将氮源自硝基芳族化合物进行氢化，并将从RI出现的产物混合物从起始到末端进料到RA中 氢化，其中RA可以另外通过单独的进料与待氢化的硝基芳族化合物进料。

    Process for preparing aromatic amines
    6.
    发明授权
    Process for preparing aromatic amines 有权
    制备芳香胺的方法

    公开(公告)号：US09139510B2

    公开(公告)日：2015-09-22

    申请号：US13978479

    申请日：2012-01-06

    申请人： Michael Merkel ,  Karl-Heinz Wilke ,  Peter Lehner ,  Andre Lago ,  Erwin Dieterich

    发明人： Michael Merkel ,  Karl-Heinz Wilke ,  Peter Lehner ,  Andre Lago ,  Erwin Dieterich

    IPC分类号： C07C209/00 ,  C07C209/36

    CPC分类号： C07C209/36 ,  C07C211/46

    摘要： The invention relates to a process for the continuous preparation of aromatic amines by hydrogenation of the corresponding nitroaromatics in the presence of catalysts arranged in reaction spaces, in which an adiabatically operated reaction space RA is connected downstream of an isothermally operated reaction space RI and RA additionally also has a separate feed for the nitroaromatic to be hydrogenated, RI is fed with the nitroaromatic to be hydrogenated from the start to the end of the hydrogenation, and the product mixture emerging from RI is fed into RA from the start to the end of the hydrogenation, wherein RA can additionally be fed via the separate feed with the nitroaromatic to be hydrogenated.

    摘要翻译： 本发明涉及通过在反应空间中排列的催化剂存在下氢化相应的硝基芳族化合物来连续制备芳族胺的方法，其中绝热操作的反应空间RA另外连接等温操作的反应空间RI和RA的下游 还具有用于待氢化的硝基芳族化合物的单独进料，从加氢的开始到结束，将氮源自硝基芳族化合物进行氢化，并将从RI出现的产物混合物从起始到末端进料到RA中 氢化，其中RA可以另外通过单独的进料与待氢化的硝基芳族化合物进料。

    METHOD FOR CONTINUOUS PRODUCTION OF NITROBENZENE
    8.
    发明申请
    METHOD FOR CONTINUOUS PRODUCTION OF NITROBENZENE 有权
    连续生产硝基苯的方法

    公开(公告)号：US20150073180A1

    公开(公告)日：2015-03-12

    申请号：US14240058

    申请日：2012-08-29

    申请人： Thomas Knauf ,  Michael Merkel

    发明人： Thomas Knauf ,  Michael Merkel

    IPC分类号： C07C201/06 ,  C07C205/06

    CPC分类号： C07C201/06 ,  C07C201/08 ,  C07C201/16 ,  C07C205/06 ,  C07C209/36 ,  C07C211/46

    摘要： The invention relates to a method for producing nitrobenzene, in which crude nitrobenzene is first produced by nitrating benzene and said crude nitrobenzene is then washed in succession in at least one acid wash, in at least one alkaline wash and in at least one neutral wash, at least one additional wash with an aqueous solution of a potassium salt being interposed between the last alkaline wash and the first neutral wash.

    摘要翻译： 本发明涉及生产硝基苯的方法，其中首先通过硝化苯生产粗硝基苯，然后将所述粗硝基苯在至少一种酸洗涤液，至少一种碱性洗涤液和至少一种中性洗涤液中连续洗涤， 在最后的碱性洗涤和第一中性洗涤之间插入钾盐水溶液至少一次另外的洗涤。

    METHOD FOR CONTINUOUSLY PRODUCING NITROBENZENE
    9.
    发明申请
    METHOD FOR CONTINUOUSLY PRODUCING NITROBENZENE 审中-公开
    连续生产硝基苯的方法

    公开(公告)号：US20130204043A1

    公开(公告)日：2013-08-08

    申请号：US13812690

    申请日：2011-07-26

    申请人： Thomas Knauf ,  Michael Merkel ,  Andreas Karl Rausch ,  Peter Lehner ,  Jürgen Münnig

    发明人： Thomas Knauf ,  Michael Merkel ,  Andreas Karl Rausch ,  Peter Lehner ,  Jürgen Münnig

    IPC分类号： C07C201/14

    CPC分类号： C07C201/14 ,  C07C201/08 ,  C07C201/16 ,  C07C209/36 ,  C07C205/06 ,  C07C211/46

    摘要： The present invention relates to a continuous process for the production of nitrobenzene by nitration of benzene with nitric acid or mixtures of nitric acid and sulfuric acid to give a crude nitrobenzene, washing of the crude nitrobenzene by means of at least one of each of an acid, alkaline and neutral washing, there being obtained a pre-purified nitrobenzene which, as well as containing nitrobenzene, at least contains also low boilers, optionally middle boilers as well as high boilers and salts, wherein the pre-purified nitrobenzene is purified further by separating off low boilers in a distillation apparatus by evaporation of the low boilers, and separation of nitrobenzene from the resulting further purified nitrobenzene in a distillation apparatus by partial evaporation of nitrobenzene, wherein pure nitrobenzene is removed from the distillation apparatus in gaseous form and is subsequently condensed, and wherein the non-evaporated portion of the further purified nitrobenzene is fed back into the washing at any desired point.

    摘要翻译： 本发明涉及通过用硝酸或硝酸和硫酸的混合物硝化硝酸生产硝基苯的连续方法，得到粗硝基苯，通过以下各项中的至少一种酸洗粗硝基苯 碱性和中性洗涤，得到预纯化的硝基苯以及含有硝基苯，至少还含有低锅炉，任选的中间锅炉以及高锅炉和盐，其中预纯化的硝基苯进一步通过 通过蒸发低沸点锅炉将蒸馏装置中的低锅炉分离出来，并通过硝基苯的部分蒸发在蒸馏装置中将硝基苯与所得到的进一步纯化的硝基苯分离，其中将纯硝基苯以气态从蒸馏装置中除去，随后 冷凝，并且其中进一步纯化的硝基苯的未蒸发部分进料 回到任何想要的点的洗涤。

    Method for continuous production of nitrobenzene
    10.
    发明授权
    Method for continuous production of nitrobenzene 有权
    连续生产硝基苯的方法

    公开(公告)号：US09012700B2

    公开(公告)日：2015-04-21

    申请号：US14240058

    申请日：2012-08-29

    申请人： Thomas Knauf ,  Michael Merkel

    发明人： Thomas Knauf ,  Michael Merkel

    IPC分类号： C07C205/00 ,  C07C209/00 ,  C07C201/06 ,  C07C205/06

    CPC分类号： C07C201/06 ,  C07C201/08 ,  C07C201/16 ,  C07C205/06 ,  C07C209/36 ,  C07C211/46

    摘要： The invention relates to a method for producing nitrobenzene, in which crude nitrobenzene is first produced by nitrating benzene and said crude nitrobenzene is then washed in succession in at least one acid wash, in at least one alkaline wash and in at least one neutral wash, at least one additional wash with an aqueous solution of a potassium salt being interposed between the last alkaline wash and the first neutral wash.

    摘要翻译： 本发明涉及生产硝基苯的方法，其中首先通过硝化苯生产粗硝基苯，然后将所述粗硝基苯在至少一种酸洗涤液，至少一种碱性洗涤液和至少一种中性洗涤液中连续洗涤， 在最后的碱性洗涤和第一中性洗涤之间插入钾盐水溶液至少一次另外的洗涤。