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13 条记录 (耗时 0.017 秒)

    Continuous process for preparing silanes and siloxanes having SiOC groups
    2.
    发明授权
    Continuous process for preparing silanes and siloxanes having SiOC groups 失效
    制备具有SiOC基团的硅烷和硅氧烷的连续工艺

    公开(公告)号：US4298753A

    公开(公告)日：1981-11-03

    申请号：US209447

    申请日：1980-11-24

    申请人： Anton Schinabeck ,  Norbert Zeller ,  Tassilo Lindner ,  Georg Engelsberger ,  Rudolf Riedle

    发明人： Anton Schinabeck ,  Norbert Zeller ,  Tassilo Lindner ,  Georg Engelsberger ,  Rudolf Riedle

    IPC分类号： C08G77/00 ,  C07F7/18 ,  C08G77/06 ,  C08G77/22 ,  C07F7/04 ,  C07F7/10

    CPC分类号： C07F7/188 ,  C08G77/06

    摘要： A continuous process for preparing silanes and siloxanes having SiOC groups which comprises (a) introducing in a liquid phase a chlorosilane and a hydroxyl-containing aliphatic compound in parallel flow into a first stage of a first reactor in an amount such that from 0.5 to 0.9 gram-mole of hydroxyl group is present per gram-atom of Si-bonded chlorine; (b) removing the liquid reaction mixture from the first reactor; (c) introducing the reaction mixture at the head of a column used as the second reactor which is maintained at an elevated temperature; (d) adding a hydroxyl-containing aliphatic compound as a gas at the lower end of the column or at a point between the lower end and the upper end of the lower one-third of the column, in an amount at least sufficient to completely react with the Si-bonded chlorine present in the reaction mixture obtained from the first stage and (e) removing the silane containing SiOC groups or polysiloxane containing SiOC groups from the column at a point below the point of addition of the hydroxyl-containing aliphatic compound.

    摘要翻译： 一种用于制备具有SiOC基团的硅烷和硅氧烷的连续方法，其包括（a）以液相方式将氯硅烷和含羟基的脂族化合物平行流入第一反应器的第一阶段，其量使得为0.5至0.9 每克原子的硅键合氯存在克分子的羟基; （b）从第一反应器中除去液体反应混合物; （c）将反应混合物引入用作第二反应器的柱头，保持在升高的温度; （d）在柱的下端或在塔的下三分之一的下端和上端之间的点处加入含羟基的脂族化合物作为气体，其量至少足以完全 与从第一阶段获得的反应混合物中存在的Si键合的氯反应，和（e）在含羟基的脂族化合物的加入点以下的点从塔中除去含有SiOC基团的含硅烷的硅烷或聚硅氧烷 。

    Process for the preparation of organosilicon compounds
    4.
    发明授权
    Process for the preparation of organosilicon compounds 失效
    制备有机硅化合物的方法

    公开(公告)号：US4276426A

    公开(公告)日：1981-06-30

    申请号：US98005

    申请日：1979-11-28

    申请人： Tassilo Lindner ,  Norbert Zeller ,  Volker Frey ,  Rudolf Riedle ,  Peter John ,  Georg Engelsberger

    发明人： Tassilo Lindner ,  Norbert Zeller ,  Volker Frey ,  Rudolf Riedle ,  Peter John ,  Georg Engelsberger

    IPC分类号： C07F7/12 ,  C07F7/08 ,  C07F7/14 ,  C07F7/18

    CPC分类号： C07F7/14 ,  C07F7/0879 ,  C07F7/1876

    摘要： This invention relates to the preparation of organosilicon compounds by the addition of a silicon compound containing Si-bonded hydrogen to a compound having an aliphatic multiple bond in the presence of a catalyst which promotes the addition of Si-bonded hydrogen to compounds containing an aliphatic multiple bond. In this process the reactants and the catalyst are continuously introduced into a pipe-shaped reactor while the contents of the reactor, which are maintained in a liquid phase by the application of pressure are circulated in the reactor at a rate of at least 1,000 cm per minute and while the reaction mixture is continuously being removed from the reactor.

    摘要翻译： 本发明涉及有机硅化合物的制备，其中在催化剂存在下，通过加入含有Si键合氢的硅化合物至具有脂肪族多重键的化合物，该催化剂促进将Si键合的氢加成到含有脂族多元素的化合物 键。 在该方法中，将反应物和催化剂连续地引入管状反应器中，同时通过施加压力保持在液相中的反应器的内容物在反应器中以至少1000cm 3的速率循环 同时反应混合物连续地从反应器中除去。

    Process of melting down and purifying silicon
    5.
    发明授权
    Process of melting down and purifying silicon 失效
    熔化和纯化硅的工艺

    公开(公告)号：US4151264A

    公开(公告)日：1979-04-24

    申请号：US872127

    申请日：1978-01-25

    申请人： Anton More ,  Rudolf Riedle ,  Herbert Straussberger ,  Willi Streckel ,  Johann Muschi

    发明人： Anton More ,  Rudolf Riedle ,  Herbert Straussberger ,  Willi Streckel ,  Johann Muschi

    IPC分类号： C01B33/02 ,  C01B33/037

    CPC分类号： C01B33/037

    摘要： A process of melting down and purifying silicon, which comprises melting silicon in at least half of the amount up to double of the amount of a silicate melt heated by resistance heating up to a temperature of at least 1,420.degree. C., said melt consisting of 2-30% by weight of calcium oxide, 5-35% by weight of magnesium oxide, wherein the sum of calcium oxide and magnesium oxide will be 15-38% by weight, 0.5-28% by weight of aluminum oxide and 45-70% by weight of silicon dioxide, and wherein, to the melt are added at least 0.29% by weight of elementary and/or chemically bound copper, preferably 0.50-3% by weight, calculated on the silicon amount.

    摘要翻译： 一种熔化和纯化硅的方法，其包括将至少一半量的硅熔化至通过电阻加热加热至高达至少1420℃的硅酸盐熔体的量的两倍，所述熔体由 2-30重量％的氧化钙，5-35重量％的氧化镁，其中氧化钙和氧化镁的总和为15-38重量％，0.5-28重量％的氧化铝和45- 70重量％的二氧化硅，并且其中向熔体中加入至少0.29重量％的基于硅量的基本和/或化学键合的铜，优选为0.50-3重量％。

    Process for preparing bis-(trimethylsilyl-)urea
    6.
    发明授权
    Process for preparing bis-(trimethylsilyl-)urea 失效
    双（三甲基甲硅烷基）脲制备方法

    公开(公告)号：US3992428A

    公开(公告)日：1976-11-16

    申请号：US655333

    申请日：1976-02-05

    申请人： Horst Muller ,  Ignaz Bauer ,  Edgar Schmidt ,  Rudolf Riedle

    发明人： Horst Muller ,  Ignaz Bauer ,  Edgar Schmidt ,  Rudolf Riedle

    IPC分类号： C07F7/10

    CPC分类号： C07F7/10

    摘要： An improved process for preparing bis-(trimethylsilyl-)urea which comprises reacting urea with hexamethyldisilazane in the presence of a catalytic amount of salts selected from the class consisting of ammonia, basic amine comounds and quaternary ammonium hydroxides.

    摘要翻译： 一种制备双（三甲基甲硅烷基）脲的改进方法，其包括在催化量的选自氨，碱性胺化合物和氢氧化季铵的盐的存在下使脲与六甲基二硅氮烷反应。

    Process for treating silicon and ferrosilicon with slag
    10.
    发明授权
    Process for treating silicon and ferrosilicon with slag 失效
    用渣处理硅和硅铁的方法

    公开(公告)号：US4534791A

    公开(公告)日：1985-08-13

    申请号：US635794

    申请日：1984-07-30

    申请人： Anton More ,  Winfried Lang ,  Rudolf Riedle ,  Herbert Straussberger ,  Willi Streckel

    发明人： Anton More ,  Winfried Lang ,  Rudolf Riedle ,  Herbert Straussberger ,  Willi Streckel

    IPC分类号： C01B33/02 ,  C01B33/037 ,  C01B33/06 ,  C22C33/00 ,  C22B4/00

    CPC分类号： C01B33/037 ,  C22C33/003

    摘要： The invention relates to a process for treating elemental silicon and ferrosilicon with slag having the following analytical composition:______________________________________ K.sub.2 O from 2 to 13% by weight Na.sub.2 O from 0 to 2% by weight .SIGMA. K.sub.2 O + Na.sub.2 O from 2 to 13% by weight SiO.sub.2 from 45 to 72% by weight Al.sub.2 O.sub.3 from 0 to 30% by weight .SIGMA. SiO.sub.2 + Al.sub.2 O.sub.3 from 60 to 78% by weight CaO from 0 to 30% by weight MgO from 0 to 30% by weight .SIGMA. CaO + MgO from 15 to 30% by weight CaF.sub.2 from 0 to 10% by weight MgF.sub.2 from 0 to 10% by weight .SIGMA. CaF.sub.2 + MgF.sub.2 from 0 to 10% by weight .SIGMA. CaO + MgO + CaF.sub.2 + MgF.sub.2 from 15 to 30 % by weight ______________________________________ and impurities resulting from the raw materials.

    摘要翻译： 本发明涉及一种用炉渣处理元素硅和硅铁的方法，具有以下分析组成：2至13重量％的K 2 O，0至2重量％的-Na 2 O，2至13重量％的SIGMA K 2 O + Na 2 O -SiO 2为45〜72重量％-Al 2 O 3 0〜30重量％-SiF 2 SiO 2 + Al 2 O 3 60〜78重量％-C 0 0〜30重量％-M 0 0〜30重量％ - SIGMA CaO + MgO 15〜30重量％-CaF 2 0〜10重量％-MgF 2 0〜10重量％-SiMA CaF 2 + MgF 2 0〜10重量％SIGMA CaO + MgO + CaF 2 + MgF 2由 15至30重量％ - 和由原料产生的杂质。