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    PROCESS FOR ORGANOCHLOROSILANE PRODUCTION IN THE FLUIDIZED BED PROCESS
    1.
    发明申请
    PROCESS FOR ORGANOCHLOROSILANE PRODUCTION IN THE FLUIDIZED BED PROCESS 审中-公开

    公开(公告)号：US20190127398A1

    公开(公告)日：2019-05-02

    申请号：US16093708

    申请日：2016-05-12

    申请人： Wacker Chemie AG

    发明人： Michael MUELLER ,  Natalia SOFINA

    IPC分类号： C07F7/16 ,  B01J23/72 ,  B01J8/18

    CPC分类号： C07F7/16 ,  B01J8/18 ,  B01J23/72

    摘要： A process for producing organochlorosilanes in a fluidized bed reaction comprises reacting haloorganic reaction gas with a catalytic composition comprising silicon, copper catalysts and promoters, in a fluidized bed reactor, wherein the hydraulic diameter of the fluidized bed reactor dhyd,the superficial gas velocity in the fluidized bed reactor uL andthe particle Sauter diameter of the catalytic composition d32 are selected such that,in a Cartesian coordination system in which Ar is plotted against Re, points on the surface are formed wherein the surface is limited by equations 1 and 2 Ar=2·10−5·Re2+0.08*Re−120   Equation 1 Ar=2·10−5·Re2−1.07*Re+14100   Equation 2 wherein the lower limit Ar=0.5 and the upper limit Ar=3000. The invention also relates to a method for selecting reaction parameters for producing organochlorosilanes.

    Method of producing an organic silicon compound
    2.
    发明授权
    Method of producing an organic silicon compound 有权
    有机硅化合物的制造方法

    公开(公告)号：US09260458B2

    公开(公告)日：2016-02-16

    申请号：US14368899

    申请日：2012-12-25

    申请人： Dow Corning Toray Co., Ltd.

    发明人： Yasushi Sugiura ,  Yoshinori Taniguchi

    IPC分类号： C07F7/16 ,  C07F7/18 ,  C07B49/00 ,  C07F7/08 ,  C07F7/12

    CPC分类号： C07F7/1876 ,  C07B49/00 ,  C07F7/0827 ,  C07F7/122

    摘要： A method of producing an organic silicon compound includes a step of reaction of the following: (A) a reactive silane compound represented by General Formula (1) below: R1mSiY(4-m) (wherein R1 is a monovalent organic group (except for the group represented by Y) or a hydrogen atom; Y indicates a chlorine atom or a group represented by —OR2; R2 indicates a monovalent hydrocarbon group having 1 to 30 carbon atoms; and m is a number in the range of 0 to 3), (B) a halogenated organic compound represented by General Formula (2) below: R3—X (wherein R3 indicates a monovalent organic group; and X is a halogen atom), and (C) metallic magnesium (Mg) in the presence of (D) an organic solvent containing at least one type of ether type compound.

    摘要翻译： 有机硅化合物的制造方法包括以下步骤：（A）由通式（1）表示的反应性硅烷化合物：R1mSiY（4-m）（其中R1是一价有机基团（除 Y表示的基团或氢原子; Y表示氯原子或-OR2表示的基团; R2表示碳原子数1〜30的一价烃基，m表示0〜3的数） ，（B）下述通式（2）表示的卤代有机化合物：R3-X（其中R3表示一价有机基团，X表示卤素原子），（C）金属镁（Mg） （D）含有至少一种醚型化合物的有机溶剂。

    Method for the direct synthesis of alkylhalogenosilanes
    4.
    发明授权
    Method for the direct synthesis of alkylhalogenosilanes 有权
    直接合成烷基卤代硅烷的方法

    公开(公告)号：US08957237B2

    公开(公告)日：2015-02-17

    申请号：US14368179

    申请日：2012-12-18

    申请人： Bluestar Silicones France

    发明人： Cécile Rosier

    IPC分类号： C07F7/16 ,  B01J23/80 ,  B01J27/10 ,  B01J23/835

    CPC分类号： C07F7/16 ,  B01J23/80 ,  B01J23/835 ,  B01J27/10

    摘要： An improved industrial method for the direct synthesis of alkylhalogenosilanes is described. Specifically, a method is described for preparing alkylhalogenosilanes by reacting, in a fluidized bed reactor, and alkyl halogenide, preferably CH3Cl, with a solid body, which is referred to as a contact body and which includes powdered silicon and a catalytic system including at least one copper catalyst and β1 and β2 promoter activities.

    摘要翻译： 描述了直接合成烷基卤代硅烷的改进的工业方法。 具体地，描述了通过在流化床反应器和烷基卤化物（优选CH 3 Cl 3）中与称为接触体的固体（其包括粉末状硅）和至少包含至少一种催化体系的催化体系进行反应来制备烷基卤代硅烷的方法 一种铜催化剂和一种和二级启动子活性。

    Ligand Synthesis
    5.
    发明申请
    Ligand Synthesis 有权
    配体合成

    公开(公告)号：US20130310590A1

    公开(公告)日：2013-11-21

    申请号：US13870518

    申请日：2013-04-25

    申请人： Xiaoliang Gao ,  Darryl J. Morrison ,  Charles Ashton Garret Carter

    发明人： Xiaoliang Gao ,  Darryl J. Morrison ,  Charles Ashton Garret Carter

    IPC分类号： C07F7/16

    CPC分类号： C07F7/16 ,  C07F7/0827 ,  C07F7/083

    摘要： Compounds 1,3,4-(SiMe3)(C6F5)(alkyl)C5H3 are made using a simplified synthetic strategy which is readily scalable. On reaction with a suitable transition metal species, a 1,3,4-(SiMe3)(C6F5)(alkyl)C5H3 molecule provides an organotransition metal complex comprising a 1,2-(C6F5)(alkyl) substituted cyclopentadienyl ligand, which is active toward olefin polymerization.

    摘要翻译： 化合物1,3,4-（SiMe 3）（C 6 F 5）（烷基）C 5 H 3是使用易于扩展的简化合成策略制备的。 通过与合适的过渡金属物质的反应，1,3,4-（SiMe 3）（C 6 F 5）（烷基）C 5 H 3分子提供了包含1,2-（C 6 F 5）（烷基）取代的环戊二烯基配体的有机过渡金属络合物， 对烯烃聚合有活性。

    PROCESS FOR PREPARING ORGANOSILANES
    6.
    发明申请
    PROCESS FOR PREPARING ORGANOSILANES 审中-公开
    制备有机硅的方法

    公开(公告)号：US20120296106A1

    公开(公告)日：2012-11-22

    申请号：US13497673

    申请日：2010-10-19

    申请人： Michael Stepp ,  Tobias Weiss

    发明人： Michael Stepp ,  Tobias Weiss

    IPC分类号： C07F7/16

    CPC分类号： C07F7/122 ,  C07F7/123 ,  C07F7/125

    摘要： The invention relates to a process for preparing diorganyldihalosilanes of the general formula (1) R2SiX2 (1), in which dihalodihydrosilanes of the general formula (2) X2SiH2 (2), in a mixture with silanes of the general formula (3) R′3SiH (3), are reacted with halogenated hydrocarbons of the general formula (4) R-X (4), in the presence of a free-radical initiator, which is selected from alkanes, diazenes and organodisilanes, where R is a monovalent C1-C18 hydrocarbon radical, R′ is a monovalent C1-C18 hydrocarbon radical, hydrogen or halogen, and X is halogen.

    摘要翻译： 本发明涉及通式（1）R2SiX2（1）的二有机基二卤代硅烷的制备方法，其中通式（2）X2SiH 2（2）的二卤代二氢化硅烷与通式（3）的硅烷的混合物R' 3SiH（3）与通式（4）RX（4）的卤代烃在选自烷烃，二氮烯和有机二硅烷的自由基引发剂存在下反应，其中R是一价C1-C18 烃基，R'是一价C1-C18烃基，氢或卤素，X是卤素。

    Process for preparing methylchlorosilanes
    8.
    发明授权
    Process for preparing methylchlorosilanes 有权
    甲基氯硅烷的制备方法

    公开(公告)号：US07550620B2

    公开(公告)日：2009-06-23

    申请号：US11856731

    申请日：2007-09-18

    申请人： Wilfried Kalchauer ,  Jochen Gross ,  Wolfgang Zoller

    发明人： Wilfried Kalchauer ,  Jochen Gross ,  Wolfgang Zoller

    IPC分类号： C07F7/16

    CPC分类号： C07F7/16

    摘要： The invention relates to a process for the direct synthesis of methylchlorosilanes by reaction of chloromethane with a contact composition comprising silicon and copper catalyst, wherein the concentration of oxygen in the chloromethane used is reduced by mixing a) chloromethane which contains oxygen, and b) chloromethane which contains a gaseous boron compound.

    摘要翻译： 本发明涉及通过氯甲烷与包含硅和铜催化剂的接触组合物的反应直接合成甲基氯硅烷的方法，其中所用氯甲烷中的氧浓度通过混合a）含有氧的氯甲烷和b）氯甲烷 其含有气态硼化合物。

    Preparation of organohalosilanes
    9.
    发明申请
    Preparation of organohalosilanes 有权
    有机硅烷的制备

    公开(公告)号：US20050209474A1

    公开(公告)日：2005-09-22

    申请号：US11081561

    申请日：2005-03-17

    申请人： Tetsuya Inukai ,  Hajime Ishizaka ,  Mikio Aramata ,  Yukinori Satou

    发明人： Tetsuya Inukai ,  Hajime Ishizaka ,  Mikio Aramata ,  Yukinori Satou

    IPC分类号： B01J27/185 ,  B01J23/835 ,  B01J37/04 ,  C07B61/00 ,  C07F7/04 ,  C07F7/16

    CPC分类号： C07F7/16

    摘要： Organohalosilanes are prepared by reacting metallic silicon particles with an organohalide in the presence of a copper catalyst. A contact mass composed of metallic silicon and copper catalyst contains an effective amount of a catalyst powder obtained by mechanical surface treatment of a powder mixture of tin powder and another metal, typically copper powder, on a ball mill, stamp mill, jet mill, mechanofusion device or the like.

    摘要翻译： 有机卤代硅烷通过在铜催化剂存在下使金属硅颗粒与有机卤化物反应来制备。 由金属硅和铜催化剂组成的接触物质含有有效量的催化剂粉末，其通过在球磨机，印刷机，喷射磨机，机械融合机械表面处理锡粉末和其它金属（通常为铜粉末）的粉末混合物而获得 装置等。