-
1.
公开(公告)号:US08709987B2
公开(公告)日:2014-04-29
申请号:US13397081
申请日:2012-02-15
申请人: Perla Duchesne , John McDonald , Sinquin Gilles , Pierre Tequi
发明人: Perla Duchesne , John McDonald , Sinquin Gilles , Pierre Tequi
IPC分类号: C10M169/04 , C10M125/10
CPC分类号: C10M159/24 , C10M167/00 , C10M2205/022 , C10M2207/026 , C10M2207/028 , C10M2207/26 , C10M2207/289 , C10M2209/086 , C10M2215/064 , C10M2215/28 , C10M2219/046 , C10M2223/045 , C10M2229/02 , C10N2210/01 , C10N2210/02 , C10N2230/06 , C10N2230/12 , C10N2230/42 , C10N2230/43 , C10N2230/45 , C10N2240/102 , C10N2260/14 , C10M2205/024 , C10N2260/06
摘要: Provided is a lubricating oil composition comprising: (a) a major amount of an oil of lubricating viscosity; and (b) one or more borated alkaline earth metal alkyltoluene sulfonate detergents; wherein the lubricating oil composition comprises no more than about 0.20 wt. % of phosphorus and no more than about 0.50 wt. % of sulfur.
摘要翻译: 提供一种润滑油组合物,其包含:(a)主要量的润滑粘度的油; 和(b)一种或多种硼酸化碱土金属烷基甲苯磺酸盐洗涤剂; 其中所述润滑油组合物包含不超过约0.20wt。 磷的百分比和不超过约0.50重量% 硫的百分比。
-
2.
公开(公告)号:US20080300154A1
公开(公告)日:2008-12-04
申请号:US11755387
申请日:2007-05-30
申请人: Perla Duchesne , John McDonald , Sinquin Gilles , Pierre Tequi
发明人: Perla Duchesne , John McDonald , Sinquin Gilles , Pierre Tequi
IPC分类号: C10M125/24
CPC分类号: C10M159/24 , C10M167/00 , C10M2205/022 , C10M2207/026 , C10M2207/028 , C10M2207/26 , C10M2207/289 , C10M2209/086 , C10M2215/064 , C10M2215/28 , C10M2219/046 , C10M2223/045 , C10M2229/02 , C10N2210/01 , C10N2210/02 , C10N2230/06 , C10N2230/12 , C10N2230/42 , C10N2230/43 , C10N2230/45 , C10N2240/102 , C10N2260/14 , C10M2205/024 , C10N2260/06
摘要: Provided is a lubricating oil composition comprising: (a) a major amount of an oil of lubricating viscosity; and (b) one or more borated alkaline earth metal alkyltoluene sulfonate detergents; wherein the lubricating oil composition comprises no more than about 0.20 wt. % of phosphorus and no more than about 0.50 wt. % of sulfur.
摘要翻译: 提供一种润滑油组合物,其包含:(a)主要量的润滑粘度的油; 和(b)一种或多种硼酸化碱土金属烷基甲苯磺酸盐洗涤剂; 其中所述润滑油组合物包含不超过约0.20wt。 磷的百分比和不超过约0.50重量% 硫的百分比。
-
3.
公开(公告)号:US20120142564A1
公开(公告)日:2012-06-07
申请号:US13397081
申请日:2012-02-15
申请人: Perla Duchesne , John McDonald , Sinquin Gilles , Pierre Tequi
发明人: Perla Duchesne , John McDonald , Sinquin Gilles , Pierre Tequi
IPC分类号: C10M135/10
CPC分类号: C10M159/24 , C10M167/00 , C10M2205/022 , C10M2207/026 , C10M2207/028 , C10M2207/26 , C10M2207/289 , C10M2209/086 , C10M2215/064 , C10M2215/28 , C10M2219/046 , C10M2223/045 , C10M2229/02 , C10N2210/01 , C10N2210/02 , C10N2230/06 , C10N2230/12 , C10N2230/42 , C10N2230/43 , C10N2230/45 , C10N2240/102 , C10N2260/14 , C10M2205/024 , C10N2260/06
摘要: Provided is a lubricating oil composition comprising: (a) a major amount of an oil of lubricating viscosity; and (b) one or more borated alkaline earth metal alkyltoluene sulfonate detergents; wherein the lubricating oil composition comprises no more than about 0.20 wt. % of phosphorus and no more than about 0.50 wt. % of sulfur.
摘要翻译: 提供一种润滑油组合物,其包含:(a)主要量的润滑粘度的油; 和(b)一种或多种硼酸化碱土金属烷基甲苯磺酸盐洗涤剂; 其中所述润滑油组合物包含不超过约0.20wt。 磷的百分比和不超过约0.50重量% 硫的百分比。
-
4.
公开(公告)号:US07868209B2
公开(公告)日:2011-01-11
申请号:US11755206
申请日:2007-05-30
申请人: Perla Duchesne , John McDonald , Gilles Sinquin , Pierre Tequi
发明人: Perla Duchesne , John McDonald , Gilles Sinquin , Pierre Tequi
IPC分类号: C07F5/02
CPC分类号: C10M159/24 , C10M177/00 , C10M2219/046 , C10N2230/04 , C10N2230/06 , C10N2260/14 , C10N2270/00
摘要: Provided is a new and improved process for preparing a borated alkaline earth metal toluene sulfonate salt.
摘要翻译: 提供了一种新的改进的硼酸盐碱土金属甲苯磺酸盐的制备方法。
-
公开(公告)号:US20080300426A1
公开(公告)日:2008-12-04
申请号:US11755206
申请日:2007-05-30
申请人: Perla Duchesne , John McDonald , Gilles Sinquin , Pierre Tequi
发明人: Perla Duchesne , John McDonald , Gilles Sinquin , Pierre Tequi
IPC分类号: C07F5/02
CPC分类号: C10M159/24 , C10M177/00 , C10M2219/046 , C10N2230/04 , C10N2230/06 , C10N2260/14 , C10N2270/00
摘要: Provided is a new and improved process for preparing a borated alkaline earth metal toluene sulfonate salt.
摘要翻译: 提供了一种新的改进的硼酸盐碱土金属甲苯磺酸盐的制备方法。
-
公开(公告)号:US07479568B2
公开(公告)日:2009-01-20
申请号:US11292404
申请日:2005-11-30
申请人: Jean-Louis Le Coent , Pierre Tequi , John McDonald
发明人: Jean-Louis Le Coent , Pierre Tequi , John McDonald
IPC分类号: C07F5/04
CPC分类号: C07C303/32 , C07C303/06 , C10M135/10 , C10M159/24 , C10M177/00 , C10N2210/02 , C10N2260/14 , C10N2270/00 , C07C309/31
摘要: An improved process for preparing an alkaline earth metal borated sulfonate comprising reacting a mixture of the following materials(A) (1) at least one of an oil soluble sulfonic acid or alkaline earth sulfonate salt or mixtures thereof (2) at least one source of an alkaline earth metal; and (3) at least one source of boron, in the presence of a mixture of comprising (4) at least one hydrocarbon solvent; and (5) at least one low molecular weight alcohol; and (6) from 0 to less than 10 mole percent, relative to the source of boron, of an overbasing acid, other than the source of boron; and (B) heating the reaction product of (A) to a temperature above the distillation temperatures of (4) and (5) to distill (4), (5) and water of reaction, wherein no additional water is added in the process.
摘要翻译: 一种制备碱土金属硼酸化磺酸盐的改进方法,包括使下列物质(A)(1)的混合物与油溶性磺酸或碱土金属磺酸盐或其混合物中的至少一种反应(2)至少一种 碱土金属; 和(3)至少一种硼源,在包含(4)至少一种烃溶剂的混合物存在下, 和(5)至少一种低分子量醇; 和(6)相对于硼源为0至小于10摩尔%的除硼源之外的高碱性酸; 和(B)将(A)的反应产物加热到高于(4)和(5)的蒸馏温度的温度至蒸馏(4),(5)和反应水,其中在该过程中不加入另外的水 。
-
公开(公告)号:US07964611B2
公开(公告)日:2011-06-21
申请号:US12334827
申请日:2008-12-15
申请人: Jean-Louis Le Coent , Pierre Tequi , John McDonald
发明人: Jean-Louis Le Coent , Pierre Tequi , John McDonald
IPC分类号: C07F5/04
CPC分类号: C07C303/32 , C07C303/06 , C10M135/10 , C10M159/24 , C10M177/00 , C10N2210/02 , C10N2260/14 , C10N2270/00 , C07C309/31
摘要: An alkaline earth metal borated sulfonate prepared by a process comprising reacting a mixture of the following materials (A) (1) at least one of an oil soluble sulfonic acid or alkaline earth sulfonate salt or mixtures thereof (2) at least one source of an alkaline earth metal; and (3) at least one source of boron, in the presence of a mixture of comprising (4) at least one hydrocarbon solvent; and (5) at least one low molecular weight alcohol; and (6) from 0 to less than 10 mole percent, relative to the source of boron, of an overbasing acid, other than the source of boron; and (B) heating the reaction product of (A) to a temperature above the distillation temperatures of (4) and (5) to distill (4), (5) and water of reaction, wherein no additional water is added in the process.
摘要翻译: 一种碱土金属硼酸盐磺酸盐,其制备方法包括使以下物质(A)(1)的混合物与油溶性磺酸盐或碱土磺酸盐盐或其混合物中的至少一种反应(2)至少一种 碱土金属; 和(3)至少一种硼源,在包含(4)至少一种烃溶剂的混合物存在下, 和(5)至少一种低分子量醇; 和(6)相对于硼源为0至小于10摩尔%的除硼源之外的高碱性酸; 和(B)将(A)的反应产物加热到高于(4)和(5)的蒸馏温度的温度至蒸馏(4),(5)和反应水,其中在该过程中不加入另外的水 。
-
公开(公告)号:US20090099385A1
公开(公告)日:2009-04-16
申请号:US12334827
申请日:2008-12-15
申请人: Jean-Louis Le Coent , Pierre Tequi , John McDonald
发明人: Jean-Louis Le Coent , Pierre Tequi , John McDonald
IPC分类号: C07F5/04
CPC分类号: C07C303/32 , C07C303/06 , C10M135/10 , C10M159/24 , C10M177/00 , C10N2210/02 , C10N2260/14 , C10N2270/00 , C07C309/31
摘要: An alkaline earth metal borated sulfonate prepared by a process comprising reacting a mixture of the following materials(A) (1) at least one of an oil soluble sulfonic acid or alkaline earth sulfonate salt or mixtures thereof (2) at least one source of an alkaline earth metal; and (3) at least one source of boron, in the presence of a mixture of comprising (4) at least one hydrocarbon solvent; and (5) at least one low molecular weight alcohol; and (6) from 0 to less than 10 mole percent, relative to the source of boron, of an overbasing acid, other than the source of boron; and (B) heating the reaction product of (A) to a temperature above the distillation temperatures of (4) and (5) to distill (4), (5) and water of reaction, wherein no additional water is added in the process.
摘要翻译: 一种碱土金属硼酸盐磺酸盐,其制备方法包括使以下物质(A)(1)的混合物与油溶性磺酸盐或碱土磺酸盐盐或其混合物中的至少一种反应(2)至少一种 碱土金属; 和(3)至少一种硼源,在包含(4)至少一种烃溶剂的混合物存在下, 和(5)至少一种低分子量醇; 和(6)相对于硼源为0至小于10摩尔%的除硼源之外的高碱性酸; 和(B)将(A)的反应产物加热到高于(4)和(5)的蒸馏温度的温度至蒸馏(4),(5)和反应水,其中在该过程中不加入另外的水 。
-
公开(公告)号:US20070123439A1
公开(公告)日:2007-05-31
申请号:US11292404
申请日:2005-11-30
申请人: Jean-Louis Le Coent , Pierre Tequi , John McDonald
发明人: Jean-Louis Le Coent , Pierre Tequi , John McDonald
IPC分类号: C07F5/04 , C10M169/04 , C10M159/24
CPC分类号: C07C303/32 , C07C303/06 , C10M135/10 , C10M159/24 , C10M177/00 , C10N2210/02 , C10N2260/14 , C10N2270/00 , C07C309/31
摘要: An improved process for preparing an alkaline earth metal borated sulfonate comprising reacting a mixture of the following materials(A) (1) at least one of an oil soluble sulfonic acid or alkaline earth sulfonate salt or mixtures thereof (2) at least one source of an alkaline earth metal; and (3) at least one source of boron, in the presence of a mixture of comprising (4) at least one hydrocarbon solvent; and (5) at least one low molecular weight alcohol; and (6) from 0 to less than 10 mole percent, relative to the source of boron, of an overbasing acid, other than the source of boron; and (B) heating the reaction product of (A) to a temperature above the distillation temperatures of (4) and (5) to distill (4), (5) and water of reaction, wherein no additional water is added in the process.
摘要翻译: 一种制备碱土金属硼酸化磺酸盐的改进方法,包括使下列物质(A)(1)的混合物与油溶性磺酸或碱土金属磺酸盐或其混合物中的至少一种反应(2)至少一种 碱土金属; 和(3)至少一种硼源,在包含(4)至少一种烃溶剂的混合物存在下, 和(5)至少一种低分子量醇; 和(6)相对于硼源为0至小于10摩尔%的除硼源之外的高碱性酸; 和(B)将(A)的反应产物加热到高于(4)和(5)的蒸馏温度的温度至蒸馏(4),(5)和反应水,其中在该过程中不加入另外的水 。
-
10.
公开(公告)号:US08916726B2
公开(公告)日:2014-12-23
申请号:US14001346
申请日:2011-03-20
申请人: Pierre Tequi , Curt B. Campbell , Gilles P. Sinquin , Christine Boemare Gandon , Kyle J. Frederic , Eugene E. Spalla
发明人: Pierre Tequi , Curt B. Campbell , Gilles P. Sinquin , Christine Boemare Gandon , Kyle J. Frederic , Eugene E. Spalla
IPC分类号: C07C309/00 , B01J19/00 , C07C2/66 , C07C303/14 , C07C303/06 , C07C303/32 , B01J8/02
CPC分类号: C07C303/06 , B01J8/02 , B01J19/0013 , B01J19/0033 , B01J2219/00166 , B01J2219/00186 , B01J2219/00202 , B01J2219/00231 , C07C2/66 , C07C303/14 , C07C303/32 , C07C2529/08 , C07C2529/70 , C10M159/24 , C10M177/00 , C10M2219/044 , C10M2219/046 , C10N2210/02 , C10N2230/70 , C10N2270/00 , C10N2270/02 , C07C15/107 , C07C309/31
摘要: Disclosed is a method for improving filtration in the preparation of an alkaline earth metal alkyltoluene sulfonate concentrate by selectively controlling the meta, ortho, para isomer distribution of the alkyl group of the alkyltoluene produced by the process comprising alkylating toluene with at least one isomerized normal alpha olefin, having from about 18 to about 30 carbon atoms and having from 20% to 100% branching in an alkylation process which includes monitoring % isomer formation and adjusting an alkylation process parameter in order to provide a target specified isomer content of less than 38% meta-isomer content; and thereafter sulfonating and neutralizing to produce a low base number sulfonated alkyltoluene concentrate having a Base Number of about 2 to 60 (ASTM D 2896).
摘要翻译: 公开了一种通过选择性地控制烷基甲苯的烷基的间位,邻位,对位异构体分布来制备碱土金属烷基甲苯磺酸盐浓缩物的方法,该方法包括使甲苯与至少一种异构化的正常α 烯烃,其具有约18至约30个碳原子并且在烷基化方法中具有20%至100%的支化,其包括监测%异构体形成和调节烷基化方法参数,以提供小于38%的目标特异异构体含量, 间 - 异构体含量; 然后磺化和中和以产生碱值为约2至60(ASTM D 2896)的低碱值磺化烷基甲苯浓缩物。
-
-
-
-
-
-
-
-
-