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公开(公告)号：US5997715A
公开(公告)日：1999-12-07
申请号：US112659
申请日：1998-07-09
IPC分类号： C07D301/26 , C25B3/02 , C25B3/04 , C25B3/00
CPC分类号： C07D301/14 , C07D301/26 , C25B3/04 , Y02P20/582
摘要： Describes a method of electrochemically converting .alpha.-halohydrins, e.g., 1-chloro-2-hydroxypropane and 1,3-dichloro-2-hydroxypropane, to epoxides, e.g., propylene oxide and epichlorohydrin. A three compartment electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and anion exchange membrane, (2) an anolyte compartment containing an anode assembly comprising an anode and a cation exchange membrane, and (3) an intermediate compartment partitioned from the catholyte and anolyte compartments by the anion and cation exchange membranes respectively. An aqueous solution of .alpha.-halohydrin is charged to the catholyte compartment, while hydrogen halide solutions are charged to the intermediate and anolyte compartments. Direct current is passed through the electrolytic cell and an aqueous solution comprising epoxide is removed from the catholyte compartment.
摘要翻译： 描述了将α-卤代醇如1-氯-2-羟基丙烷和1,3-二氯-2-羟基丙烷电化学转化为环氧化物如环氧丙烷和表氯醇的方法。 提供一种三室电解池，其具有（1）阴极电解室，其包含阴极组件和阴离子交换膜;（2）阳极室，其包含阳极和阳离子交换膜;以及（3） 中间隔室分别由阴离子和阳极电解质隔室分隔开。 将α-卤代醇的水溶液加入到阴极电解液室中，同时将卤化氢溶液加入到中间体和阳极电解液室中。 直流电流通过电解槽，从阴极电解液隔室除去包含环氧化物的水溶液。
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公开(公告)号：US5900133A
公开(公告)日：1999-05-04
申请号：US914600
申请日：1997-08-18
摘要： Describes a method of electrochemically converting amine hydrohalide, e.g., ethyleneamine hydrochloride, into free amine, e.g., free ethyleneamine. A three compartment electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and anion exchange membrane, (2) an anolyte compartment containing an anode assembly comprising an anode and a cation exchange membrane, and (3) an intermediate compartment separated from the catholyte and anolyte compartments by the anion and cation exchange membranes respectively. An aqueous solution of amine hydrohalide is charged to the catholyte compartment, while hydrogen halide solutions are charged to the intermediate and anolyte compartments. Direct current is passed through the electrolytic cell and an aqueous solution comprising free amine is removed from the catholyte compartment.
摘要翻译： 描述了将胺氢卤化物（例如乙烯胺盐酸盐）电化学转化成游离胺，例如游离亚乙基胺的方法。 提供一种三室电解池，其具有（1）阴极电解室，其包含阴极组件和阴离子交换膜;（2）阳极室，其包含阳极和阳离子交换膜;以及（3） 中间室分别通过阴离子和阳离子交换膜与阴极电解液和阳极电解质隔室分离。 将胺氢卤化物的水溶液加入到阴极电解液室中，同时将卤化氢溶液装入中间体和阳极电解液室。 直流电流通过电解槽，并从阴极电解液隔室除去包含游离胺的水溶液。
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公开(公告)号：US5972195A
公开(公告)日：1999-10-26
申请号：US112658
申请日：1998-07-09
CPC分类号： C25B3/04
摘要： Describes a method of electrochemically converting .alpha.-halohydrin, e.g., 1-chloro-2-hydroxypropane and 1,3-dichloro-2-hydroxypropane, to epoxide, e.g., propylene oxide and epichlorohydrin. An aqueous solution of .alpha.-halohydrin is charged to the catholyte compartment of an electrolytic cell, which contains a cathode, hydrogen gas is charged to the anode compartment of the cell, which contains an anode assembly comprising a hydrogen consuming gas diffusion anode fixedly held between a current collecting electrode and an anion exchange membrane. The catholyte and anode compartments of the cell are separated by the anion exchange membrane. An aqueous solution containing epoxide is removed from the catholyte compartment.
摘要翻译： 描述了将α-卤代醇例如1-氯-2-羟基丙烷和1,3-二氯-2-羟基丙烷电化学转化为环氧化物的方法，例如环氧丙烷和表氯醇。 将α-卤代醇的水溶液加入到包含阴极的电解池的阴极电解液室中，氢气被加入到电池的阳极室中，该阳极室包含阳极组件，阳极组件包括固定保持在 集电极和阴离子交换膜。 细胞的阴极电解液和阳极室被阴离子交换膜分离。 从阴极电解液室除去含有环氧化物的水溶液。
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公开(公告)号：US5882501A
公开(公告)日：1999-03-16
申请号：US914602
申请日：1997-08-18
IPC分类号： B01D61/44 , B01D61/52 , C07C209/68 , C07C211/10 , C25B3/00 , C25B9/08 , C25B9/16 , C25B1/00 , C25B7/00 , C25B9/00
摘要： Describes a method of electrochemically converting amine hydrohalide, e.g., ethyleneamine hydrochloride, into free amine, e.g., free ethyleneamine, by charging an aqueous solution of amine hydrohalide to the catholyte compartment of an electrolytic cell, which contains a cathode, charging hydrogen gas to the anode compartment of the cell, which contains an anode assembly comprised of a hydrogen consuming gas diffusion anode fixedly held between a current collecting electrode and an anion exchange membrane. The catholyte and anode compartments of the cell are separated by the anion exchange membrane. An amine hydrohalide solution containing free amine is removed from the catholyte compartment.
摘要翻译： 描述了通过将胺氢卤化物的水溶液加入到含有阴极的电解池的阴极电解液室中，将胺氢卤化物（例如，乙烯胺盐酸盐）电化学转化成游离胺，例如游离亚乙基胺的方法，将氢气加入到 阳极室，其包含阳极组件，阳极组件由固定保持在集电电极和阴离子交换膜之间的消耗氢的气体扩散阳极组成。 细胞的阴极电解液和阳极室被阴离子交换膜分离。 从阴极电解液室除去含有游离胺的胺氢卤酸盐溶液。
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公开(公告)号：US5906722A
公开(公告)日：1999-05-25
申请号：US914603
申请日：1997-08-18
摘要： Describes a method of electrochemically converting amine hydrohalide, e.g., ethyleneamine hydrochloride, into free amine, e.g., free ethyleneamine. A three compartment electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and an anion exchange membrane, (2) an anode compartment containing an anode assembly comprising either (a) a hydrogen consuming gas diffusion anode and a current collecting electrode or (b) a hydrogen consuming gas diffusion anode which is fixedly held between a hydraulic barrier and a current collecting electrode, and (3) an intermediate compartment separated from the catholyte and anode compartments by the anion exchange membrane and either (i) the hydrogen consuming gas diffusion anode or (ii) the hydraulic barrier respectively. An aqueous solution of amine hydrohalide is charged to the catholyte compartment, while hydrogen gas is charged to the anode compartment and an aqueous conductive electrolyte solution is charged to the intermediate compartment. Direct current is passed through the electrolytic cell and an aqueous solution comprising free amine is removed from the catholyte compartment.
摘要翻译： 描述了将胺氢卤化物（例如乙烯胺盐酸盐）电化学转化成游离胺，例如游离亚乙基胺的方法。 提供一种三室电解池，其具有：（1）阴极电解室，其包含阴极组件，阴极组件包括阴极和阴离子交换膜;（2）阳极室，其包含阳极组件，阳极组件包括（a）消耗氢的气体扩散阳极和 电流收集电极或（b）固定保持在液压屏障和集电电极之间的消耗氢的气体扩散阳极，以及（3）通过阴离子交换膜与阴极电解液和阳极隔室分离的中间室和（i ）氢消耗气体扩散阳极或（ii）液压屏障。 将胺氢卤化物的水溶液加入到阴极电解液室中，同时将氢气加入到阳极室中，并将水性导电电解质溶液装入中间室。 直流电流通过电解槽，并从阴极电解液隔室除去包含游离胺的水溶液。
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公开(公告)号：US5980724A
公开(公告)日：1999-11-09
申请号：US112657
申请日：1998-07-09
CPC分类号： C25B3/04
摘要： Described is a method of electrochemically converting .alpha.-halohydrins, e.g., 1-chloro-2-hydroxypropane and 1,3-dichloro-2-hydroxypropane, to epoxides, e.g., propylene oxide and epichlorohydrin. An electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and a bipolar ion exchange membrane, (2) an anode compartment containing an anode assembly comprising either (a) a hydrogen consuming gas diffusion anode and a current collecting electrode or (b) a hydrogen consuming gas diffusion anode which is fixedly held between a hydraulic barrier and a current collecting electrode, and (3) at least one pair of intermediate compartments separating the catholyte and anode compartments and separated from each other by an anion exchange membrane. The following are introduced into the cell: a first aqueous conductive electrolyte solution into the catholyte compartment; hydrogen gas into the anode compartment; an aqueous solution of .alpha.-halohydrin into the first compartment of the pair of intermediate compartments; and a second aqueous conductive electrolyte solution into the second compartment of the pair of intermediate compartments. Direct current is passed through the electrolytic cell, and an aqueous solution comprising epoxide is removed from the first compartment.
摘要翻译： 描述了将α-卤代醇如1-氯-2-羟基丙烷和1,3-二氯-2-羟基丙烷电化学转化为环氧化物，例如环氧丙烷和表氯醇的方法。 提供一种电解池，其具有（1）阴极电解液室，其包含阴极组件，阴极组件包括阴极和双极离子交换膜，（2）阳极室，其包含阳极组件，阳极组件包括（a）消耗氢的气体扩散阳极和电流 收集电极或（b）固定保持在液压屏障和集电电极之间的消耗氢的气体扩散阳极，以及（3）至少一对隔离阴极电解液室和阳极室的中间隔室， 阴离子交换膜。 将以下物质引入电池中：将第一水性导电电解质溶液引入到阴极电解液室中; 氢气进入阳极室; 将α-卤代醇的水溶液注入到该对中间隔室的第一隔室中; 以及第二水性导电电解质溶液进入所述一对中间隔室中的第二隔室。 直流电流通过电解槽，从第一隔室除去包含环氧化物的水溶液。
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公开(公告)号：US5904829A
公开(公告)日：1999-05-18
申请号：US914601
申请日：1997-08-18
CPC分类号： B01D61/445 , C07C209/68 , C25B3/00
摘要： Describes a method of electreochemically converting amine hydrohalide, e.g., amine hydrochloride, into free amine, e.g., free ethyleneamine. An electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and a bipolar ion exchange membrane, (2) an anode compartment containing an anode assembly comprising either (a) a hydrogen consuming gas diffusion anode and a current collecting electrode or (b) a hydrogen consuming gas diffusion anode which is fixedly held between a hydraulic barrier and a current collecting electrode, and (3) at least one pair of intermediate compartments separating the catholyte and anode compartments and separated from each other by an anion exchange membrane. The following are introduced into the cell: a first aqueous conductive electrolyte solution into the catholyte compartment; hydrogen gas into the anode compartment; an aqueous solution of amine hydrohalide into the first compartment of the pair of intermediate compartments; and a second aqueous conductive electrolyte solution into the second compartment of the pair of intermediate compartments. Direct current is passed through the electrolytic cell, and an aqueous solution comprising free amine is removed from the first compartment.
摘要翻译： 描述了将胺氢卤化物（例如胺盐酸盐）电化学转化成游离胺，例如游离亚乙基胺的方法。 提供一种电解池，其具有（1）阴极电解液室，其包含阴极组件，阴极组件包括阴极和双极离子交换膜，（2）阳极室，其包含阳极组件，阳极组件包括（a）消耗氢的气体扩散阳极和电流 收集电极或（b）固定保持在液压屏障和集电电极之间的消耗氢的气体扩散阳极，以及（3）至少一对隔离阴极电解液室和阳极室的中间隔室， 阴离子交换膜。 将以下物质引入电池中：将第一水性导电电解质溶液引入到阴极电解液室中; 氢气进入阳极室; 胺氢卤酸盐的水溶液进入该对中间隔室的第一隔室; 以及第二水性导电电解质溶液进入所述一对中间隔室中的第二隔室。 直流电流通过电解槽，从第一隔室除去包含游离胺的水溶液。
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公开(公告)号：US5997716A
公开(公告)日：1999-12-07
申请号：US112660
申请日：1998-07-09
IPC分类号： C25B3/00
CPC分类号： C25B3/00
摘要： Described is a method of electrochemically converting .alpha.-halohydrins, e.g., 1-chloro-2-hydroxypropane and 1,3-dichloro-2-hydroxypropane, to epoxides, e.g., propylene oxide and epichlorohydrin. A three compartment electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and an anion exchange membrane, (2) an anode compartment containing an anode assembly comprising either (a) a hydrogen consuming gas diffusion anode and a current collecting electrode or (b) a hydrogen consuming gas diffusion anode which is fixedly held between a hydraulic barrier and a current collecting electrode, and (3) an intermediate compartment separated from the catholyte and anode compartments by the anion exchange membrane and either (i) the hydrogen consuming gas diffusion anode or (ii) the hydraulic barrier respectively. An aqueous solution of .alpha.-halohydrin is charged to the catholyte compartment, while hydrogen gas is charged to the anode compartment and an aqueous electrolyte solution is charged to the intermediate compartment. Direct current is passed through the electrolytic cell and an aqueous solution comprising epoxide is removed from the catholyte compartment.
摘要翻译： 描述了将α-卤代醇如1-氯-2-羟基丙烷和1,3-二氯-2-羟基丙烷电化学转化为环氧化物，例如环氧丙烷和表氯醇的方法。 提供一种三室电解池，其具有：（1）阴极电解室，其包含阴极组件，阴极组件包括阴极和阴离子交换膜;（2）阳极室，其包含阳极组件，阳极组件包括（a）消耗氢的气体扩散阳极和 电流收集电极或（b）固定保持在液压屏障和集电电极之间的消耗氢的气体扩散阳极，以及（3）通过阴离子交换膜与阴极电解液和阳极隔室分离的中间室和（i ）氢消耗气体扩散阳极或（ii）液压屏障。 将α-卤代醇的水溶液加入到阴极电解液室中，同时将氢气加入到阳极室中，并将电解质水溶液装入中间室。 直流电流通过电解槽，从阴极电解液隔室除去包含环氧化物的水溶液。
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9.发明授权System for accessing control to a peripheral device utilizing a synchronization primitive within the peripheral device 失效用于使用外围设备内的同步原语访问对外围设备的控制的系统
公开(公告)号：US5931923A
公开(公告)日：1999-08-03
申请号：US602199
申请日：1996-02-16
申请人： David G. Roberts
发明人： David G. Roberts
CPC分类号： G06F9/52 , G06F13/126
摘要： Method and system aspects control access through a synchronization primitive to a peripheral device in a processing system. A processing system in accordance with the present invention includes at least one central processing unit (CPU), and at least one peripheral device coupled to the at least one CPU, where the at least one peripheral device includes a synchronization primitive for controlling acquisition by at least one thread of execution from the at least one CPU. In a system aspect for controlling access, the system includes a circuit for sending a first signal from a component of the processing system to a synchronization primitive within the peripheral device to determine a state of the synchronization primitive, and acquiring control of the peripheral device when the synchronization primitive is in a released state. In a method for gaining control of a peripheral device in a processing system, the method includes sending a first signal from a component of the processing system to a semaphore register within the peripheral device to determine a bit pattern in the semaphore register, and acquiring control of the peripheral device when the semaphore register stores a first bit pattern.
摘要翻译： 方法和系统方面通过同步原语控制对处理系统中的外围设备的访问。 根据本发明的处理系统包括至少一个中央处理单元（CPU）和耦合到至少一个CPU的至少一个外围设备，其中所述至少一个外围设备包括同步原语，用于控制在 至少一个CPU执行的至少一个执行线程。 在用于控制访问的系统方面中，系统包括用于将第一信号从处理系统的组件发送到外围设备内的同步原语的电路，以确定同步原语的状态，以及获取外围设备的控制 同步原语处于释放状态。 在一种用于在处理系统中获得对外围设备的控制的方法中，所述方法包括将来自所述处理系统的组件的第一信号发送到所述外围设备内的信号量寄存器，以确定所述信号量寄存器中的位模式，以及获取控制 的信号量寄存器存储第一位模式。
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公开(公告)号：US5860025A
公开(公告)日：1999-01-12
申请号：US677406
申请日：1996-07-09
申请人： David G. Roberts , Robert Alan Williams , Glen William Gibson , Jiu An , RamKrishna Vepa , Henry Yeh , Din-I Tsai
发明人： David G. Roberts , Robert Alan Williams , Glen William Gibson , Jiu An , RamKrishna Vepa , Henry Yeh , Din-I Tsai
CPC分类号： G06F12/1081 , G06F13/28
摘要： A data transfer method with peripheral precharge wherein a starting portion of an output data block targeted for a peripheral is transferred to an output buffer for the peripheral using programmed I/O or slave cycles and wherein a virtual address of the output data block is translated into a physical address while the peripheral begins transferring the starting portion from the output buffer and over an output path. A direct memory access operation by the peripheral transfers a remainder portion of the output data block into the output buffer.
摘要翻译： 一种具有外围预充电的数据传输方法，其中针对外设的输出数据块的起始部分使用编程的I / O或从属周期传送到外围设备的输出缓冲器，并且其中输出数据块的虚拟地址被转换为 物理地址，而外设开始从输出缓冲器和输出路径传送起始部分。 由外设的直接存储器存取操作将输出数据块的剩余部分传送到输出缓冲器。
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