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公开(公告)号：US5770154A
公开(公告)日：1998-06-23
申请号：US578223
申请日：1995-12-26
CPC分类号： B01J8/0285 , G01N31/10 , B01J2208/00415 , B01J2219/00135
摘要： A device for testing the development of processes or chemical reactions in the presence of solid catalysts comprising a reactor of cylindrical shape, of inside diameter D and of length L, such that 50
摘要翻译： 在固体催化剂存在下测试方法或化学反应的发展的装置，其包括内径为D且长度为L的圆柱形反应器，使得50
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公开(公告)号：US5344554A
公开(公告)日：1994-09-06
申请号：US770265
申请日：1991-10-03
CPC分类号： B01J8/1809 , C10G11/187
摘要： The invention relates to a downflow fluid cracking process and apparatus. More specifically, sampling takes place of the at least partly regenerated catalyst, which must be recycled to the reactor 1 from a dense phase 17a, contained in a regenerator 17 and the stage of introducing the catalyst into the upper part 3 of the reactor 1 takes place under conditions such that the density of the thus formed gas-solid suspension is between 80 and 500 kg/m.sup.3 prior to its contacting with the charge, which is introduced by the injectors 5.
摘要翻译： 本发明涉及一种下流流体破裂过程和装置。 更具体地说，取样至少部分再生的催化剂，其必须从包含在再生器17中的致密相17a再循环到反应器1中，并且将催化剂引入反应器1的上部3中 在如此形成的气固悬浮液的密度在与注射器5引入的电荷接触之前为80至500kg / m 3的条件下放置。
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3.发明授权Process and apparatus for operation of a slurry bubble column with application to the fischer-tropsch synthesis 失效一种应用于费 - 托合成的浆液鼓泡塔的操作方法和装置
公开(公告)号：US6060524A
公开(公告)日：2000-05-09
申请号：US227837
申请日：1999-01-11
IPC分类号： B01J8/00 , B01J8/18 , B01J8/22 , C07C1/02 , C07C1/04 , C07C1/12 , C07C9/00 , C10G2/00 , C07C27/00
CPC分类号： C10G2/342 , B01J8/0005 , B01J8/1836 , B01J8/226 , B01J8/228 , B01J2208/00123 , B01J2208/00132 , B01J2208/0015 , B01J2208/00283
摘要： The invention concerns a process for optimal operation of a slurry bubble column containing a suspension of solid particles in a liquid, characterized in that a gas phase containing the reactant(s) required for the production of the desired products is injected in the form of bubbles close to the lower extremity of said reactor and at least a portion of the liquid fraction and optionally of the solid fraction of said suspension is recirculated, drawn off from close to one extremity of said reactor and reintroduced close to the other extremity of said reactor, with a liquid flow rate U.sub.1 in the reactor which is at least equal to and preferably greater than the sedimentation rate U.sub.s of the solid particles. The invention also concerns an apparatus for optimal operation of the process. Finally, the invention concerns the use of the process and apparatus in the Fischer-Tropsch synthesis.
摘要翻译： 本发明涉及一种在液体中含有固体颗粒悬浮液的浆液气泡塔的最佳操作的方法，其特征在于，以气泡的形式注入含有生产所需产物所需的反应物的气相 接近所述反应器的下端，并且所述液体部分和任选的所述悬浮液的固体部分的至少一部分被再循环，从所述反应器的一个末端附近引出并重新引入所述反应器的另一末端， 反应器中的液体流量U1至少等于并优选大于固体颗粒的沉降速率Us。 本发明还涉及用于该过程的最佳操作的装置。 最后，本发明涉及在费 - 托合成中使用该方法和装置。
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4.发明授权Process for converting liquid or semi-liquid hydrocarbon charges to lighter fractions 失效将液体或半液体碳氢化合物装料转化为较轻馏分的方法
公开(公告)号：US4738769A
公开(公告)日：1988-04-19
申请号：US478428
申请日：1983-03-24
CPC分类号： B01J8/12 , C10G2400/20
摘要： A process for converting liquid or semi-liquid hydrocarbon charges to lighter fractions comprises a first step (a) heating droplets jets of the charge introduced into a pyrolysis chamber by surrounding them with parallel jets of hot solid particles, of relatively large size, of a heat carrier material, not substantially in contact with the droplet jets, so as to maintain a temperature of 700.degree.-1600.degree. C., and introducing a gas so as to obtain a pressure from 1 to 150 bars. A second step involves (b) separating the gaseous fraction from the solid particles. Thereafter (c) at least a portion of the solid particles are heated and fed back to step (a). The gaseous fraction is (d) cooled by means of a cold gas so as to recover light hydrocarbons therefrom.
摘要翻译： 将液体或半液体碳氢化合物装料转化成轻馏分的方法包括第一步骤（a）通过用相当大尺寸的热固体颗粒的平行射流包围引入到热解室中的电荷的液滴射流， 热载体材料，基本上不与液滴射流接触，以保持700〜-1600℃的温度，并引入气体以获得1至150巴的压力。 第二步涉及（b）从固体颗粒中分离气态馏分。 此后（c）将至少一部分固体颗粒加热并反馈到步骤（a）。 气态馏分（d）通过冷气体冷却，以从其中回收轻质烃。
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公开(公告)号：US07588734B2
公开(公告)日：2009-09-15
申请号：US11405677
申请日：2006-04-18
CPC分类号： G01N31/10
摘要： The invention describes a laboratory reactor for the kinetic study of catalytic reactions calling for a gaseous reaction phase and a liquid reaction phase, characterized by a capillary shape, a substantially uniform arrangement of the catalyst grains along the reactor, with, on average, every cross-section of the reactor comprising a defined and constant number of catalyst grains, and this number of grains being between 1 and 4. The reactor that is the object of the invention is especially well suited for studying reactions of hydrogenation, hydrotreatment, and hydrocracking.
摘要翻译： 本发明描述了用于动力学研究催化反应的实验室反应器，其需要气态反应相和液体反应相，其特征在于毛细管形状，沿着反应器的催化剂颗粒的基本均匀排列，平均每个交叉 该反应器包括定义和恒定数量的催化剂颗粒，并且该数目的颗粒在1和4之间。作为本发明目的的反应器特别适用于研究氢化，加氢处理和加氢裂化的反应。
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公开(公告)号：US20070071664A1
公开(公告)日：2007-03-29
申请号：US11405677
申请日：2006-04-18
CPC分类号： G01N31/10
摘要： The invention describes a laboratory reactor for the kinetic study of catalytic reactions calling for a gaseous reaction phase and a liquid reaction phase, characterized by a capillary shape, a substantially uniform arrangement of the catalyst grains along the reactor, with, on average, every cross-section of the reactor comprising a defined and constant number of catalyst grains, and this number of grains being between 1 and 4. The reactor that is the object of the invention is especially well suited for studying reactions of hydrogenation, hydrotreatment, and hydrocracking.
摘要翻译： 本发明描述了用于动力学研究催化反应的实验室反应器，其需要气态反应相和液体反应相，其特征在于毛细管形状，沿着反应器的催化剂颗粒的基本均匀排列，平均每个交叉 该反应器包括定义和恒定数量的催化剂颗粒，并且该数目的颗粒在1和4之间。作为本发明目的的反应器特别适用于研究氢化，加氢处理和加氢裂化的反应。
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公开(公告)号：US06825237B2
公开(公告)日：2004-11-30
申请号：US10239395
申请日：2002-09-26
IPC分类号： C07C2700
CPC分类号： C10G2/342
摘要： A process for synthesising hydrocarbons by reacting a mixture comprising at least carbon monoxide and hydrogen in the presence of a catalyst is carried out in a three-phase reactor in which the liquid Peclet number is in the range 0 (excluded) to about 10, with a superficial gas velocity Ug that is preferably less than 35 cm.s−1, to encourage gas transfer into the liquid phase and avoid too much attrition of the catalyst grains.
摘要翻译： 在催化剂存在下通过使包含至少一氧化碳和氢气的混合物反应合成烃的方法是在三相反应器中进行的，其中液体派佩克数在0（不包括）至约10的范围内，与 表面气体速度Ug优选小于35cm -1，以促进气体转移到液相中并避免催化剂颗粒的过多磨损。
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公开(公告)号：US5129930A
公开(公告)日：1992-07-14
申请号：US710048
申请日：1991-06-04
摘要： A co-current cyclone mixer-separator which makes it possible to separae a light phase L1 contained in a mixture M1 which also contains a dense phase D1 from the dense phase and to mix this phase L1 with a dense phase or with a mixture containing this phase and a light phase. The mixture M1 is introduced at and the phase D1 is recovered at. The dense phase of a mixture is introduced at and enters a second inner enclosure at, at least a part of the phase likewise entering the latter enclosure. A mixture comprising the phases, if it has been introduced, is obtained at. Preferably, the apparatus comprises blades which make it possible to limit the progress of the vortex into the outlet. This apparatus permits of a rapid heat exchange, for exmple the hardening, of a phase by a phase or a mixture. It can also be used for the rapid replacement of a phase contained in a mixture also containing a phase by a phase other than.
摘要翻译： 一种并流旋流混合器分离器，其使得可以将从密相中也含有密相D1的混合物M1中所含的轻相L1分离，并将该相L1与致密相混合，或与含有该相的混合物 相和轻相。 混合物M1被引入并在D1处被回收。 混合物的稠相在同一进入后一个外壳的相的至少一部分处被引入并进入第二内壳。 如果已经引入，则包含相的混合物在 优选地，该装置包括能够将涡流进入出口的叶片。 该装置允许通过相或混合物快速热交换（例如硬化）相。 它也可用于快速更换包含在除了相以外的相的混合物中的相。
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公开(公告)号：US4472264A
公开(公告)日：1984-09-18
申请号：US461413
申请日：1983-01-27
CPC分类号： C10G1/002 , B01J8/12 , C07C1/00 , Y10S585/943
摘要： Process for converting solid carbonaceous materials to methane, comprising (a) converting the carbonaceous material by means of a reducing gas at 300.degree.-500.degree. C. to a semi-oily phase adapted to be pumped and atomized, (b) heating falling droplets of said semi-oily phase to a temperature of 700.degree.-1600.degree. C. with hot solid particles in downward jets in the presence of reducing gas, under a presssure above 20 bars, (c) separating the solid particles of large size (d), heating them and feeding them back to step (b), (e) cooling the remaining fraction consisting of gas and solid particles of small size by means of a cold reducing gas and separating methane therefrom, and (f) treating the remaining solid phase of fine particles with oxygen and steam to produce a reducing gas fed back to steps (a) and (b).
摘要翻译： 将固体碳质材料转化成甲烷的方法，包括（a）将碳质材料通过300-500℃的还原气体转化成适于泵送和雾化的半油相，（b）加热滴液 的所述半油相在700〜1600℃的温度下，在还原气体存在下，在20巴以下的压力下，向下喷射热固体颗粒，（c）分离大尺寸固体颗粒（d ），加热它们并将其送回到步骤（b），（e）通过冷还原气体冷却由气体和小尺寸的固体颗粒组成的剩余部分并从其中分离甲烷，和（f）处理剩余的固体 用氧气和蒸汽将细颗粒的相分离，以产生反馈到步骤（a）和（b）的还原气体。
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10.发明授权Process and apparatus for operation of a slurry bubble column with application to the fischer-tropsch synthesis 失效一种应用于费 - 托合成的浆液鼓泡塔的操作方法和装置
公开(公告)号：US5961933A
公开(公告)日：1999-10-05
申请号：US901521
申请日：1997-07-28
IPC分类号： B01J8/00 , B01J8/18 , B01J8/22 , C07C1/02 , C07C1/04 , C07C1/12 , C07C9/00 , C10G2/00 , B01J8/02 , B01J8/08 , F28D7/00
CPC分类号： C10G2/342 , B01J8/0005 , B01J8/1836 , B01J8/226 , B01J8/228 , B01J2208/00123 , B01J2208/00132 , B01J2208/0015 , B01J2208/00283
摘要： The invention concerns a process for optimal operation of a slurry bubble column containing a suspension of solid particles in a liquid, characterized in that a gas phase containing the reactant(s) required for the production of the desired products is injected in the form of bubbles close to the lower extremity of the reactor and at least a portion of the liquid fraction and optionally of the solid fraction of the suspension is recirculated, drawn off from close to one extremity of the reactor and reintroduced close to the other extremity of the reactor, with a liquid flow rate U.sub.l in the reactor which is at least equal to and preferably greater than the sedimentation rate U.sub.s of the solid particles. The invention also concerns an apparatus for optimal operation of the process. Finally, the invention concerns the use of the process and apparatus in the Fischer-Tropsch synthesis.
摘要翻译： 本发明涉及一种在液体中含有固体颗粒悬浮液的浆液气泡塔的最佳操作的方法，其特征在于，以气泡的形式注入含有生产所需产物所需的反应物的气相 靠近反应器的下肢，并且至少一部分液体部分和任选的悬浮液的固体部分被再循环，从反应器的一个末端排出并重新引入到反应器的另一个末端， 反应器中的液体流量U 1至少等于并且优选大于固体颗粒的沉降速率Us。 本发明还涉及用于该过程的最佳操作的装置。 最后，本发明涉及在费 - 托合成中使用该方法和装置。
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