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公开(公告)号:US5863698A
公开(公告)日:1999-01-26
申请号:US58733
申请日:1998-04-13
申请人: Raj D. Patel , Paul F. Smith , Beverly C. Dutoff , Nan-Xing Hu , Beng S. Ong , Michael A. Hopper
发明人: Raj D. Patel , Paul F. Smith , Beverly C. Dutoff , Nan-Xing Hu , Beng S. Ong , Michael A. Hopper
CPC分类号: G03G9/09741 , G03G9/0804
摘要: A process for the preparation of toner comprising mixing a colorant containing a surfactant and a latex emulsion, and wherein the latex emulsion contains resin and a nonionic hydrolyzable surfactant, and wherein said surfactant is of the Formulas (I) or (II), or optionally mixtures thereof ##STR1## wherein R.sup.1 is a hydrophobic aliphatic, or hydrophobic aromatic group; R.sup.2 is selected from the group consisting of hydrogen, alkyl, aryl, alkylaryl, and alkylarylalkyl; R.sup.3 is hydrogen or alkyl; A is a hydrophilic polymer chain, and m represents the number of A segments; heating below about the resin latex glass transition temperature, followed by the addition of an anionic stabilizer, thereafter heating above about the resin glass transition temperature, and adjusting the pH of the resulting mixture of resin and colorant particles suspended in an aqueous phase containing anionic surfactant, cationic surfactant and nonionic hydrolyzable surfactant, wherein said pH is increased from about 1.7 to about 2.5 to about 6 to about 12 by adding a base during the heating above about said resin glass transition temperature wherein coalescence is being accomplished.
摘要翻译: 一种制备调色剂的方法,包括混合含有表面活性剂的着色剂和胶乳乳液,并且其中所述胶乳乳液含有树脂和非离子可水解表面活性剂,并且其中所述表面活性剂为式(I)或(II),或任选地 (II)其中R1是疏水性脂族或疏水性芳族基团; R2选自氢,烷基,芳基,烷基芳基和烷基芳基烷基; R3是氢或烷基; A是亲水性聚合物链,m表示A链段的数目; 在树脂胶乳玻璃化转变温度以下加热,然后加入阴离子稳定剂,然后加热至高于树脂玻璃化转变温度,并调节悬浮在含有阴离子表面活性剂的水相中的树脂和着色剂颗粒的混合物的pH 阳离子表面活性剂和非离子可水解表面活性剂,其中所述pH通过在加热之前加热约上升约1.7至约2.5至约6至约12,所述树脂玻璃化转变温度高于其中聚结。
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公开(公告)号:US5766818A
公开(公告)日:1998-06-16
申请号:US960176
申请日:1997-10-29
申请人: Paul F. Smith , Nan-Xing Hu , Beverly C. Dutoff , Beng S. Ong , Raj D. Patel , Michael A. Hopper
发明人: Paul F. Smith , Nan-Xing Hu , Beverly C. Dutoff , Beng S. Ong , Raj D. Patel , Michael A. Hopper
CPC分类号: G03G9/08791 , G03G9/0806 , G03G9/0975 , G03G9/09775
摘要: A process for the preparation of toner by mixing a colorant dispersion and a latex emulsion, and wherein the latex emulsion contains resin and a surfactant, wherein the surfactant is, for example, of the Formulas (I) or (II) ##STR1## wherein R.sup.1 is a hydrophobic aliphatic, or hydrophobic aromatic group; R.sup.2 is selected from the group consisting of hydrogen, alkyl, aryl, alkylaryl, and alkylarylalkyl; R.sup.3 is hydrogen or alkyl; A is a hydrophilic polymer, and m represents the number of A segments.
摘要翻译: 一种通过混合着色剂分散体和胶乳乳液制备调色剂的方法,其中胶乳乳液含有树脂和表面活性剂,其中表面活性剂是例如式(I)或(II)的化合物(IMAGE)( 疏水性芳香族基团; R2选自氢,烷基,芳基,烷基芳基和烷基芳基烷基; R3是氢或烷基; A是亲水性聚合物,m表示A段数。
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公开(公告)号:US5994020A
公开(公告)日:1999-11-30
申请号:US58738
申请日:1998-04-13
申请人: Raj D. Patel , Michael A. Hopper , Paul F. Smith , Beng S. Ong , Allan K. Chen
发明人: Raj D. Patel , Michael A. Hopper , Paul F. Smith , Beng S. Ong , Allan K. Chen
CPC分类号: G03G9/08782 , G03G9/0804 , Y10S977/887
摘要: A toner process which comprises mixing(i) a colorant dispersion, and a(ii) a nonionic surfactant, an ionic surfactant or mixtures thereof, with(iii) a latex comprised of resin and a mixture of anionic surfactant and a nonionic surfactant;(iv) heating the resulting blend of (iii) about equal to, or below about the glass transition temperature (Tg) of the resin; and(v) optionally adding additional anionic surfactant to the resulting aggregated suspension of (iv);(vi) heating the resulting mixture of (v) about equal to, or above about the Tg of the resin and(vii) isolating the toner.
摘要翻译: 一种调色剂方法,其包括将(i)着色剂分散体和(ii)非离子表面活性剂,离子表面活性剂或其混合物与(iii)由树脂和阴离子表面活性剂和非离子表面活性剂的混合物组成的胶乳混合; (iv)将所得的(iii)的共混物加热至约等于或低于树脂的玻璃化转变温度(Tg); 和(v)任选地向所得的(iv)的聚集悬浮液中加入另外的阴离子表面活性剂; (vi)加热(v)约等于或高于树脂Tg的混合物,和(vii)分离调色剂。
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公开(公告)号:US5936008A
公开(公告)日:1999-08-10
申请号:US560783
申请日:1995-11-21
申请人: Robert N. Jones , Edward J. Radigan, Jr. , Susan Robinette , Raj D. Patel , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Garland J. Nichols , Beng S. Ong
发明人: Robert N. Jones , Edward J. Radigan, Jr. , Susan Robinette , Raj D. Patel , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Garland J. Nichols , Beng S. Ong
CPC分类号: C09D11/32 , Y10S260/38
摘要: An ink for ink jet printing includes a liquid vehicle comprising water and toner particles with a colorant dispersed in or associated with the toner particles. The ink composition combines the print quality advantages of xerographic printing with the economic advantages of ink jet printing, thereby providing waterfast, archival quality prints.
摘要翻译: 用于喷墨印刷的油墨包括液体载体,其包含水和具有分散在调色剂颗粒中或与调色剂颗粒相关联的着色剂的调色剂颗粒。 油墨组合物将静电印刷的印刷质量优点与喷墨印刷的经济优点相结合,从而提供耐水性,档案质量的印刷品。
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公开(公告)号:US06495302B1
公开(公告)日:2002-12-17
申请号:US09877747
申请日:2001-06-11
申请人: Lu Jiang , Nan-Xing Hu , Raj D. Patel , Walter Mychajlowskij , Michael A. Hopper
发明人: Lu Jiang , Nan-Xing Hu , Raj D. Patel , Walter Mychajlowskij , Michael A. Hopper
IPC分类号: C08J3215
CPC分类号: G03G9/0804 , G03G9/09708
摘要: A toner process including, for example, mixing a latex with a colorant wherein the latex contains resin and an ionic surfactant, and the colorant contains a surfactant and a colorant; adding a polyaluminum chloride; affecting aggregation by heating; adding a chelating component and a base wherein the base increases the pH of the formed aggregates; heating the resulting mixture to accomplish coalescence; and isolating the toner.
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公开(公告)号:US06664017B1
公开(公告)日:2003-12-16
申请号:US10225411
申请日:2002-08-20
IPC分类号: G03G9097
CPC分类号: G03G21/043 , G03G9/0902 , G03G9/0926 , G03G9/0928 , G03G9/09708 , G03G9/09725
摘要: A process comprising applying a toner security mark on a document generated by xerographic means and which mark possesses white glossy characteristics, and wherein said toner is comprised of a polymer and a colorant.
摘要翻译: 一种方法,包括在由静电印刷装置产生的文件上施加调色剂安全标记,并且哪个标记具有白色光泽特性,并且其中所述调色剂由聚合物和着色剂组成。
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公开(公告)号:US5679724A
公开(公告)日:1997-10-21
申请号:US536235
申请日:1995-09-29
申请人: Guerino G. Sacripante , Raj D. Patel , Marcel P. Breton , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Beng S. Ong
发明人: Guerino G. Sacripante , Raj D. Patel , Marcel P. Breton , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Beng S. Ong
摘要: An ink for ink jet printing includes an emulsifiable polymer resin and a pigment, and may be made by: (a) combining (1) an emulsion of an emulsifiable polymer resin in an anionic medium with (2) a pigment and a cationic surfactant; and (b) aggregating particles in the mixture of step (a) to a desired particle size, thereby producing a solution of aggregated particles. The particles can optionally be coalesced to alter the particle size of the particles.
摘要翻译: 用于喷墨印刷的油墨包括可乳化聚合物树脂和颜料,并且可以通过以下制备:(a)将(1)阴离子介质中的可乳化聚合物树脂的乳液与(2)颜料和阳离子表面活性剂组合; 和(b)将步骤(a)的混合物中的颗粒聚集成所需的粒径,从而产生凝集颗粒的溶液。 颗粒可以任选地聚结以改变颗粒的粒度。
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公开(公告)号:US06582873B2
公开(公告)日:2003-06-24
申请号:US10164162
申请日:2002-06-05
申请人: Lu Jiang , Nan-Xing Hu , Raj D. Patel , Walter Mychajlowskij , Michael A. Hopper
发明人: Lu Jiang , Nan-Xing Hu , Raj D. Patel , Walter Mychajlowskij , Michael A. Hopper
IPC分类号: C08J3215
CPC分类号: G03G9/0804 , G03G9/09708
摘要: A toner process including, for example, mixing a latex with a colorant wherein the latex contains resin and an ionic surfactant, and the colorant contains a surfactant and a colorant; adding a polyaluminum chloride; affecting aggregation by heating; adding a chelating component and a base wherein the base increases the pH of the formed aggregates; heating the resulting mixture to accomplish coalescence; and isolating the toner.
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公开(公告)号:US5977210A
公开(公告)日:1999-11-02
申请号:US380550
申请日:1995-01-30
申请人: Raj D. Patel , Marcel P. Breton , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Beng S. Ong
发明人: Raj D. Patel , Marcel P. Breton , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Beng S. Ong
CPC分类号: C09D11/30 , C08F2/26 , Y10S977/902
摘要: A process for the preparation of ink compositions comprising the emulsion polymerization of monomer, water, surfactant, and initiator with stirring and heating to provide a latex; mixing therewith a pigment dispersion of pigment particles, water, and cationic surfactant; blending the mixture; thereafter stirring the mixture; and subsequently adding additional anionic surfactant to stabilize the aggregate particles.
摘要翻译: 一种制备油墨组合物的方法,包括在搅拌和加热下单体,水,表面活性剂和引发剂的乳液聚合以提供胶乳; 与颜料颗粒,水和阳离子表面活性剂的颜料分散体混合; 混合混合物 然后搅拌混合物; 并随后加入另外的阴离子表面活性剂以稳定聚集体颗粒。
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公开(公告)号:US5582951A
公开(公告)日:1996-12-10
申请号:US498284
申请日:1995-07-03
申请人: Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper , Walter Mychajlowskij , Beng S. Ong
发明人: Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper , Walter Mychajlowskij , Beng S. Ong
CPC分类号: G03G9/1133 , G03G9/107 , G03G9/1132
摘要: A process for the preparation of carrier particles which comprises mixing a dispersion of water, submicron magnetic particles, and ionic surfactant with a latex comprised of resin particles suspended in an aqueous solution containing a surfactant that is counterionic in charge to said ionic surfactant, and a nonionic surfactant; thereafter heating the resulting mixture below about the latex resin glass transition temperature (Tg) while stirring to form aggregates, followed by increasing the temperature of said mixture to about above the latex resin Tg, and subsequently adding additional counterionic or nonionic surfactant solution to minimize, or avoid any further growth in particle size during heating of the mixture about above the latex resin Tg, and wherein said resin Tg is in the range of from between about 45.degree. C. to about 100.degree. C.
摘要翻译: 一种制备载体颗粒的方法,其包括将水,亚微米磁性颗粒和离子表面活性剂的分散体与悬浮在含有负离子表面活性剂的水溶液中的树脂颗粒混合到所述离子表面活性剂上的胶乳混合,以及 非离子表面活性剂 然后在搅拌下将所得混合物在胶乳树脂玻璃化转变温度(Tg)以下加热以形成聚集体,随后将所述混合物的温度升高至胶乳树脂Tg的大约,然后加入另外的抗衡离子或非离子表面活性剂溶液, 或者避免混合物加热到胶乳树脂Tg以上时粒径的任何进一步增长,并且其中所述树脂Tg在约45℃至约100℃的范围内。
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