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    Alkyl esters of 1-alkanoyl cycloalkanols and organoleptic uses thereof
    1.
    发明授权
    Alkyl esters of 1-alkanoyl cycloalkanols and organoleptic uses thereof 失效
    1-烷酰基环烷醇的烷基酯及其感官用途

    公开(公告)号：US4374055A

    公开(公告)日：1983-02-15

    申请号：US314002

    申请日：1981-10-22

    申请人： Ronald P. Schreck ,  Kenneth K. Light ,  John B. Hall ,  Frederick L. Schmitt ,  Manfred H. Vock ,  William L. Schreiber ,  Joaquin F. Vinals ,  Jacob Kiwala

    发明人： Ronald P. Schreck ,  Kenneth K. Light ,  John B. Hall ,  Frederick L. Schmitt ,  Manfred H. Vock ,  William L. Schreiber ,  Joaquin F. Vinals ,  Jacob Kiwala

    IPC分类号： A24B15/34 ,  C11B9/00 ,  C11D3/50 ,  A61K7/46

    CPC分类号： A24B15/34 ,  C11B9/0026 ,  C11D3/50

    摘要： Described is a process for preparing several substituted or unsubstituted cycloalkyl acyl alkanoates defined according to the generic structure: ##STR1## wherein R.sub.1 and R.sub.2 taken together complete a cycloalkyl moiety or methyl, dimethyl or trimethyl substituted cycloalkyl moiety containing five or six carbon atoms in the ring and wherein R.sub.3 is C.sub.1 -C.sub.3 lower alkyl and R.sub.4 is methyl or hydrogen by reacting a compound having the generic structure: ##STR2## in an aqueous silver-ion containing solution having a weakly acidic pH at elevated temperatures. The compounds so produced are useful for their organoleptic properties in consumable materials, such as foodstuffs, foodstuff flavorants, chewing gums, chewing gum flavorants, toothpastes, toothpaste flavorants, medicinal products, medicinal product flavorants, chewing tobaccos, chewing tobacco flavorants, smoking tobaccos, smoking tobacco flavorants, perfume compositions, perfumed articles, such as cationic, anionic, nonionic and zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, textile sizing agents and optical brighteners for textiles as well as colognes.

    摘要翻译： 描述了根据通用结构定义的若干取代或未取代的环烷基酰基链烷酸酯的方法：其中R 1和R 2一起完成环烷基部分或含有5或6个碳原子的甲基，二甲基或三甲基取代的环烷基部分 环，其中R 3是C 1 -C 3低级烷基，R 4是甲基或氢，通过使具有通式结构的化合物：在高温下具有弱酸性pH的含水银离子溶液中。 如此生产的化合物可用于消费材料如食品，食品香料，口香糖，口香糖调味剂，牙膏，牙膏调味剂，药用产品，药用香料，咀嚼烟草，咀嚼烟草香料，烟草烟草， 吸烟烟草调味剂，香料组合物，香料制品，例如阳离子，阴离子，非离子和两性离子洗涤剂，织物柔软剂组合物，干燥剂添加的织物柔软剂制品，纺织品上浆剂和用于纺织品的荧光增白剂以及古龙水。

    Process for enhancing the organoleptic properties of perfumed articles using alkyl esters of 1-alkanolyl cycloalkanols
    3.
    发明授权
    Process for enhancing the organoleptic properties of perfumed articles using alkyl esters of 1-alkanolyl cycloalkanols 失效
    使用1-链烷酰基环烷醇的烷基酯增强香料制品的感官特性的方法

    公开(公告)号：US4359395A

    公开(公告)日：1982-11-16

    申请号：US314003

    申请日：1981-10-22

    申请人： Ronald P. Schreck ,  Kenneth K. Light ,  John B. Hall ,  Frederick L. Schmitt ,  Manfred H. Vock ,  William L. Schreiber ,  Joaquin F. Vinals ,  Jacob Kiwala

    发明人： Ronald P. Schreck ,  Kenneth K. Light ,  John B. Hall ,  Frederick L. Schmitt ,  Manfred H. Vock ,  William L. Schreiber ,  Joaquin F. Vinals ,  Jacob Kiwala

    IPC分类号： A24B15/34 ,  C11D3/50 ,  D06M13/00

    CPC分类号： D06M13/005 ,  A24B15/34 ,  C11D3/50

    摘要： Described is a process for preparing several substituted or unsubstituted cycloalkyl acyl alkanolates defined according to the generic structure: ##STR1## wherein R.sub.1 and R.sub.2 taken together complete a cycloalkyl moiety or methyl, dimethyl or trimethyl substituted cycloalkyl moiety containing five or six carbon atoms in the ring and wherein R.sub.3 is C.sub.1 -C.sub.3 lower alkyl and R.sub.4 is methyl or hydrogen by reacting a compound having the generic structure: ##STR2## in an aqueous silver-ion containing solution having a weakly acidic pH at elevated temperatures. The compounds so produced are useful for their organoleptic properties in consumable materials, such as foodstuffs, foodstuff flavorants, chewing gums, chewing gum flavorants, toothpastes, toothpaste flavorants, medicinal products, medicinal product flavorants, chewing tobaccos, chewing tobacco flavorants, smoking tobaccos, smoking tobacco flavorants, perfume compositions, perfumed articles, such as cationic, anionic, nonionic and zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, textile sizing agents and optical brighteners for textiles as well as colognes.

    摘要翻译： 描述了根据以下通用结构定义的几种取代或未取代的环烷基酰基链烷醇酯的方法：其中R1和R2一起完成环烷基部分或含有5或6个碳原子的甲基，二甲基或三甲基取代的环烷基部分 环，其中R 3是C 1 -C 3低级烷基，R 4是甲基或氢，通过使具有通式结构的化合物：在高温下具有弱酸性pH的含水银离子溶液中。 如此生产的化合物可用于消费材料如食品，食品香料，口香糖，口香糖调味剂，牙膏，牙膏调味剂，药用产品，药用香料，咀嚼烟草，咀嚼烟草香料，烟草烟草， 吸烟烟草调味剂，香料组合物，香料制品，例如阳离子，阴离子，非离子和两性离子洗涤剂，织物柔软剂组合物，干燥剂添加的织物柔软剂制品，纺织品上浆剂和用于纺织品的荧光增白剂以及古龙水。

    Alkyl esters of 1-alkanoyl cycloalkanols, process for preparing same and organoleptic uses thereof
    4.
    发明授权
    Alkyl esters of 1-alkanoyl cycloalkanols, process for preparing same and organoleptic uses thereof 失效
    1-烷酰基环烷醇的烷基酯，其制备方法及其感官用途

    公开(公告)号：US4327749A

    公开(公告)日：1982-05-04

    申请号：US133828

    申请日：1980-03-25

    申请人： Ronald P. Schreck ,  Kenneth K. Light ,  John B. Hall ,  Frederick L. Schmitt ,  Manfred H. Vock ,  William L. Schreiber ,  Joaquin F. Vinals ,  Jacob Kiwala

    发明人： Ronald P. Schreck ,  Kenneth K. Light ,  John B. Hall ,  Frederick L. Schmitt ,  Manfred H. Vock ,  William L. Schreiber ,  Joaquin F. Vinals ,  Jacob Kiwala

    IPC分类号： A24B15/34 ,  A24B15/30

    CPC分类号： A24B15/34

    摘要： Described is a process for preparing several substituted or unsubstituted cycloalkyl acyl alkanoates defined according to the generic structure: ##STR1## wherein R.sub.1 and R.sub.2 taken together complete a cycloalkyl moiety or methyl, dimethyl or trimethyl substituted cycloalkyl moiety containing five or six carbon atoms in the ring and wherein R.sub.3 is C.sub.1 -C.sub.3 lower alkyl and R.sub.4 is methyl or hydrogen by reacting a compound having the generic structure: ##STR2## in an aqueous silver-ion containing solution having a weakly acidic pH at elevated temperatures. The compounds so produced are useful for their organoleptic properties in consumable materials, such as foodstuffs, foodstuff flavorants, chewing gums, chewing gum flavorants, toothpastes, toothpaste flavorants, medicinal products, medicinal product flavorants, chewing tobaccos, chewing tobacco flavorants, smoking tobaccos, smoking tobacco flavorants, perfume compositions, perfumed articles, such as cationic, anionic, nonionic and zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, textile sizing agents and optical brighteners for textiles as well as colognes.

    摘要翻译： 描述了根据通用结构定义的若干取代或未取代的环烷基酰基链烷酸酯的方法：其中R 1和R 2一起完成环烷基部分或含有5或6个碳原子的甲基，二甲基或三甲基取代的环烷基部分 环，其中R 3是C 1 -C 3低级烷基，R 4是甲基或氢，通过使具有通式结构的化合物：在高温下具有弱酸性pH的含水银离子溶液中。 如此生产的化合物可用于消费材料如食品，食品香料，口香糖，口香糖调味剂，牙膏，牙膏调味剂，药用产品，药用香料，咀嚼烟草，咀嚼烟草香料，烟草烟草， 吸烟烟草调味剂，香料组合物，香料制品，例如阳离子，阴离子，非离子和两性离子洗涤剂，织物柔软剂组合物，干燥剂添加的织物柔软剂制品，纺织品上浆剂和用于纺织品的荧光增白剂以及古龙水。

    1(1,3-Dioxobutane)-3,3-dimethylcyclohexane useful in perfumes
    6.
    发明授权
    1(1,3-Dioxobutane)-3,3-dimethylcyclohexane useful in perfumes 失效
    1（1,3-二恶丁烷）-3,3-二甲基环己烷可用于香料

    公开(公告)号：US4541951A

    公开(公告)日：1985-09-17

    申请号：US650709

    申请日：1984-09-14

    申请人： John B. Hall ,  Mark A. Sprecker

    发明人： John B. Hall ,  Mark A. Sprecker

    IPC分类号： C07C51/02 ,  C07C59/80 ,  C11B9/00

    CPC分类号： C11B9/0034 ,  C07C403/16 ,  C07C51/02 ,  C07C59/80 ,  C07C2101/14 ,  Y10S514/844 ,  Y10S514/881

    摘要： Described is a process for preparing the compound having the structure: ##STR1## comprising the steps of reacting 1-acetyl-3,3-dimethylcyclohexane having the structure: ##STR2## with an alkyl acetate defined according to the structure: ##STR3## wherein R.sub.2 is C.sub.1 -C.sub.5 alkyl such as methylethyl, n-propyl, i-propyl, n-butyl, 2-butyl and tertiary butyl, thereby forming a diketone having the structure: ##STR4## reacting the said diketone with an allyl halide having the structure: ##STR5## (wherein X represents bromo or iodo) to form a substituted diketone having the structure: ##STR6## and then transforming the compound having the structure: ##STR7## into the compound having the structure: ##STR8## by means of a retro-Claisen reaction. Also described is the use in augmenting or enhancing the aroma of perfume compositions, colognes or perfumed articles of the compound having the structure: ##STR9##

    摘要翻译： 描述了一种制备具有以下结构的化合物的方法：包括以下步骤：使具有以下结构的1-乙酰基-3,3-二甲基环己烷与以下结构所定义的乙酸烷基酯反应：其中 R2是C1-C5烷基，例如甲基乙基，正丙基，异丙基，正丁基，2-丁基和叔丁基，从而形成具有以下结构的二酮：将所述二酮与烯丙基卤反应， 结构：（其中X表示溴或碘）以形成具有以下结构的取代的二酮：然后将具有以下结构的化合物转化成具有以下结构的化合物：通过 复古克莱森反应。 还描述了用于增强或增强具有以下结构的化合物的香料组合物，古龙水或香料制品的香味：

    Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof
    9.
    发明授权
    Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof 失效

    公开(公告)号：US4418010A

    公开(公告)日：1983-11-29

    申请号：US456979

    申请日：1983-01-10

    申请人： Mark A. Sprecker ,  John B. Hall

    发明人： Mark A. Sprecker ,  John B. Hall

    IPC分类号： A24B15/34 ,  C07C29/09 ,  C07C29/17 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C11B9/00

    CPC分类号： C11B9/0042 ,  A24B15/345 ,  C07C29/095 ,  C07C29/172 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C2102/42

    摘要： Described are substituted tricyclodecane derivatives having the generic structure: ##STR1## wherein Y is a moiety having a structure selected from the group consisting of: ##STR2## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 and R.sub.2 represent hydrogen or methyl with the proviso that one of R.sub.1 and R.sub.2 is hydrogen and the other of R.sub.1 and R.sub.2 is methyl; wherein R.sub.3 is hydrogen, C.sub.1 -C.sub.3 acyl, C.sub.3 or C.sub.4 alkyl or C.sub.3 or C.sub.4 alkenyl; wherein R.sub.4, R.sub.5 and R.sub.6 represent hydrogen or methyl with the additional proviso that one of R.sub.4, R.sub.5 and R.sub.6 is methyl and the other two of R.sub.4, R.sub.5 and R.sub.6 is hydrogen. Also described are processes for preparing such substituted tricyclodecane derivatives and processes for using the above defined substituted tricyclodecane derivatives for their organoleptic properties and compositions containing said substituted tricyclodecane derivatives including perfumes, perfumed articles, such as solid or liquid anionic, cationic, nonionic and zwitterionic detergents, fabric softeners and cosmetic powders; foodstuffs, chewing gums, toothpastes, medicinal products and chewing tobaccos; smoking tobacco compositions and smoking tobacco flavoring compositions and smoking tobacco articles containing such smoking tobacco compositions.

    Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof
    10.
    发明授权
    Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof 失效

    公开(公告)号：US4386023A

    公开(公告)日：1983-05-31

    申请号：US335564

    申请日：1981-12-29

    申请人： Mark A. Sprecker ,  John B. Hall

    发明人： Mark A. Sprecker ,  John B. Hall

    IPC分类号： A24B15/34 ,  C07C29/09 ,  C07C29/17 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C49/643 ,  C11B9/00 ,  A61K7/00

    CPC分类号： C11B9/0042 ,  A24B15/345 ,  C07C29/095 ,  C07C29/172 ,  C07C29/70 ,  C07C35/37 ,  C07C35/46 ,  C07C45/29 ,  C07C49/643 ,  C07C2103/60 ,  C07C2103/66

    摘要： Described are substituted tricyclodecane derivatives having the generic structure: ##STR1## wherein Y is a moiety having a structure selected from the group consisting of: ##STR2## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 and R.sub.2 represent hydrogen or methyl with the proviso that one of R.sub.1 and R.sub.2 is hydrogen and the other of R.sub.1 and R.sub.2 is methyl; wherein R.sub.3 is hydrogen, C.sub.1 -C.sub.3 acyl, C.sub.3 or C.sub.4 alkyl or C.sub.3 or C.sub.4 alkenyl; wherein R.sub.4, R.sub.5 and R.sub.6 represent hydrogen or methyl with the additional proviso that one of R.sub.4, R.sub.5 and R.sub.6 is methyl and the other two of R.sub.4, R.sub.5 and R.sub.6 is hydrogen. Also described are processes for preparing such substituted tricyclodecane derivatives and processes for using the above defined substituted tricyclodecane derivatives for their organoleptic properties and compositions containing said substituted tricyclodecane derivatives including perfumes, perfumed articles, such as solid or liquid anionic, cationic, nonionic and zwitterionic detergents, fabric softeners and cosmetic powders; foodstuffs, chewing gums, toothpastes, medicinal products and chewing tobaccos; smoking tobacco compositions and smoking tobacco flavoring compositions and smoking tobacco articles containing such smoking tobacco compositions.