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    Method for preparation of mesoporous zeolites
    2.
    发明授权
    Method for preparation of mesoporous zeolites 有权
    介孔沸石的制备方法

    公开(公告)号：US09403690B2

    公开(公告)日：2016-08-02

    申请号：US13974154

    申请日：2013-08-23

    申请人： SAMSUNG TOTAL PETROCHEMICALS CO., LTD. ,  KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY

    发明人： Jeong Rang Kim ,  Yeon Shick Yoo ,  Jin Suk Lee ,  Ho Sik Chang ,  Yun Jo Lee ,  Ki Won Jun ,  Jo Yong Park ,  Kyoung Su Ha

    IPC分类号： C01B39/02 ,  C01B39/38

    CPC分类号： C01B39/38 ,  C01B39/02

    摘要： Provided is a preparation method for a mesoporous zeolite, particularly a method for preparing mesoporous zeolite through a simple process without using costly materials such as an organic amine template or a surfactant. The method includes 1) forming a synthetic zeolite gel by mixing a silica precursor, an aluminum precursor and water and aging the resulted mixture; 2) carrying out zeolite synthesis by subjecting the synthetic zeolite gel to a hydrothermal reaction; 3) cooling the synthesized zeolite from the above step 2), then adding a basic solution thereto and allowing them to react, thereby obtaining a mesoporous zeolite slurry; and 4) washing the mesoporous zeolite slurry with water, drying and firing it, thereby obtaining a mesoporous zeolite.

    摘要翻译： 提供了介孔沸石的制备方法，特别是通过简单的方法制备介孔沸石的方法，而不使用昂贵的材料如有机胺模板或表面活性剂。 该方法包括：1）通过混合二氧化硅前体，铝前体和水形成合成的沸石凝胶，并使所得混合物老化; 2）通过使合成沸石凝胶进行水热反应进行沸石合成; 3）从上述步骤2）中冷却合成的沸石，然后向其中加入碱性溶液并使其反应，从而获得介孔沸石浆料; 和4）用水洗涤介孔沸石浆料，干燥并焙烧，得到介孔沸石。