Method for determining the properties of porous materials
    2.
    发明授权
    Method for determining the properties of porous materials 有权
    确定多孔材料性质的方法

    公开(公告)号:US09574987B2

    公开(公告)日:2017-02-21

    申请号:US14381495

    申请日:2013-02-22

    CPC classification number: G01N15/088 G01N13/00 G01N25/4846

    Abstract: A sample of porous material is placed in a calorimeter cell and a pressure in the cell is increased starting from a pressure value of a first step by filling the cell with a wetting fluid. Measurements are taken of a heat flow to the cell and a fluid volume at each step. Then, the pressure in the cell is decreased to the pressure value of a first step with continued measurements of the heat flow to the cell. Increase and following decrease of the fluid pressure in the cell are repeated at least once. Then a temperature in the cell is decreased below a wetting fluid crystallization point. Once the fluid has been fully crystallized in sample pores, the temperature in the cell is increased above a wetting fluid melting point. Wetting limiting angle of the pores filled with fluid, and pore sizes are determined based on the results of heat flow measurements with due consideration of heat effect of fluid compression.

    Abstract translation: 将多孔材料的样品放置在量热计单元中,并且通过用润湿流体填充电池,从第一步骤的压力值开始增加电池中的压力。 测量在每个步骤中流向细胞的热流和流体体积。 然后,继续测量到电池的热流,电池中的压力降低到第一步骤的压力值。 至少一次重复细胞中流体压力的增加和继续下降。 然后,电池中的温度降低到润湿流体结晶点以下。 一旦流体已经在样品孔中完全结晶,则电池中的温度升高到高于润湿流体熔点。 填充有流体的孔的润湿极限角度和孔径基于热流测量的结果确定,同时考虑到流体压缩的热效应。

    METHOD FOR DETERMINING THE PROPERTIES OF POROUS MATERIALS
    3.
    发明申请
    METHOD FOR DETERMINING THE PROPERTIES OF POROUS MATERIALS 有权
    用于确定多孔材料性质的方法

    公开(公告)号:US20150107339A1

    公开(公告)日:2015-04-23

    申请号:US14381495

    申请日:2013-02-22

    CPC classification number: G01N15/088 G01N13/00 G01N25/4846

    Abstract: A sample of porous material is placed in a calorimeter cell and a pressure in the cell is increased starting from a pressure value of a first step by filling the cell with a wetting fluid. Measurements are taken of a heat flow to the cell and a fluid volume at each step. Then, the pressure in the cell is decreased to the pressure value of a first step with continued measurements of the heat flow to the cell. Increase and following decrease of the fluid pressure in the cell are repeated at least once. Then a temperature in the cell is decreased below a wetting fluid crystallization point. Once the fluid has been fully crystallized in sample pores, the temperature in the cell is increased above a wetting fluid melting point. Wetting limiting angle of the pores filled with fluid, and pore sizes are determined based on the results of heat flow measurements with due consideration of heat effect of fluid compression.

    Abstract translation: 将多孔材料的样品放置在量热计单元中,并且通过用润湿流体填充电池,从第一步骤的压力值开始增加电池中的压力。 测量在每个步骤中流向细胞的热流和流体体积。 然后,继续测量到电池的热流,电池中的压力降低到第一步骤的压力值。 至少一次重复细胞中流体压力的增加和继续下降。 然后,电池中的温度降低到润湿流体结晶点以下。 一旦流体已经在样品孔中完全结晶,则电池中的温度升高到高于润湿流体熔点。 填充有流体的孔的润湿极限角度和孔径基于热流测量的结果确定,同时考虑到流体压缩的热效应。

    METHOD FOR ESTIMATING THERMODYNAMIC EQUILIBRIUM OF A GAS-LIQUID MIXTURE DURING FILTRATION EXPERIMENTS
    6.
    发明申请
    METHOD FOR ESTIMATING THERMODYNAMIC EQUILIBRIUM OF A GAS-LIQUID MIXTURE DURING FILTRATION EXPERIMENTS 审中-公开
    在过滤实验中估算气液混合物的热力学平衡的方法

    公开(公告)号:US20150185064A1

    公开(公告)日:2015-07-02

    申请号:US14406662

    申请日:2013-06-07

    CPC classification number: G01F23/296 G01F15/08 G01N7/10 G01N11/00

    Abstract: A gas phase and a liquid phase with a specified volumetric ratio of phases in a flow and with specified flow rates are injected into a multiphase separator. During the injection gas and liquid phase volumes in the separator are determined and accumulation rates of each phase in the separator are calculated. A thermodynamic equilibrium is estimated based on a discrepancy between the phase injection rates and the calculated phase accumulation rates.

    Abstract translation: 气相和液相中具有规定体积比的流动相和特定流速注入多相分离器。 在注入期间,确定分离器中的气体和液相体积,并计算分离器中各相的累积速率。 基于相位注入速率与计算的相位积累率之间的差异来估计热力学平衡。

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