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    HIGH PURITY 1,1-DICARBONYL SUBSTITUTED-1-ALKENES AND METHODS FOR THEIR PREPARATION
    2.
    发明申请
    HIGH PURITY 1,1-DICARBONYL SUBSTITUTED-1-ALKENES AND METHODS FOR THEIR PREPARATION 审中-公开

    公开(公告)号：US20170327454A1

    公开(公告)日：2017-11-16

    申请号：US15346122

    申请日：2016-11-08

    Applicant: SIRRUS, INC.

    Inventor： Jeffery M. Sullivan ,  Kevin Powers ,  William Barrett

    IPC: C07C69/38 ,  C08F222/10

    CPC classification number: C07C69/38 ,  C07C67/333 ,  C08F222/10 ,  C07C69/593

    Abstract: A composition comprising about 97 mole percent or greater of one or more 1,1-dicarbonyl substituted-1-ethylenes and about 3 mole percent or less of one or more 1,1-dicarbonyl substituted-methanes. A process comprising: contacting in a fluid state one or more 1,1-dicarbonyl substituted-1,1 hydroxymethyl-methanes and greater than 200 ppm to about 1000 ppm of one or more strong acids based on the weight of the one or more 1,1-dicarbonyl substituted-1,1 hydroxymethyl-methanes with a zeolite catalyst at a temperature of about 180° C. to about 220° C. for a sufficient time to convert about 96 percent or greater of the one or more 1,1-dicarbonyl substituted-1,1 hydroxymethyl-methanes to one or more 1,1-dicarbonyl substituted-1-ethylenes.

    Polyester macromers containing 1,1-dicarbonyl-substituted 1 alkenes
    4.
    发明授权
    Polyester macromers containing 1,1-dicarbonyl-substituted 1 alkenes 有权

    公开(公告)号：US10087283B2

    公开(公告)日：2018-10-02

    申请号：US15472379

    申请日：2017-03-29

    Applicant: SIRRUS, INC.

    Inventor： Aniruddha Palsule ,  Jeffrey M. Sullivan ,  Kshitij K. Parab ,  Elliott King ,  William Barrett

    IPC: C08G63/60 ,  C08G64/42 ,  C07C69/593 ,  C12P7/62

    Abstract: Disclosed are compositions comprising polyester macromers containing in one or more chains the residue of one or more diols and one or more diesters wherein the residue of the one or more diols and the one or more diesters alternate along the chain and a portion of the diesters are 1,1-diester-1-alkenes, and optionally one or more dihydrocarbyl dicarboxylates, and at least one terminal end comprises the residue of one of the 1,1-diester-1 alkenes and wherein one or more terminal ends may comprise the residue of one or more diols. The chains may contain the residue of the one or more diols and one or more diesters comprising one or more diesters 1,1-diester-1 alkenes and optionally one or more dihydrocarbyl dicarboxylates randomly disposed along the chains. Disclosed are methods of preparing the polyester macromers and incorporating them in a variety of polyester containing compositions such as coatings and films.

    High purity 1,1-dicarbonyl substituted-1-alkenes and methods for their preparation
    6.
    发明授权
    High purity 1,1-dicarbonyl substituted-1-alkenes and methods for their preparation 有权
    高纯度1,1-二羰基取代-1-烯烃及其制备方法

    公开(公告)号：US09518001B1

    公开(公告)日：2016-12-13

    申请号：US15159185

    申请日：2016-05-19

    Applicant: SIRRUS, INC.

    Inventor： Jeffrey M. Sullivan ,  Kevin Powers ,  William Barrett

    IPC: C07C67/327 ,  B01J29/06 ,  C07C67/333 ,  C07C57/13 ,  C08G63/00

    CPC classification number: C07C67/333 ,  C07C51/377 ,  C07C57/13 ,  C07C67/343 ,  C07C69/593 ,  C07C69/675

    Abstract: A composition comprising about 97 mole percent or greater of one or more 1,1-dicarbonyl substituted-1-ethylenes and about 3 mole percent or less of one or more 1,1-dicarbonyl substituted-methanes. A process comprising: contacting in a fluid state one or more 1,1-dicarbonyl substituted-1,1 hydroxymethyl-methanes and greater than 200 ppm to about 1000 ppm of one or more strong acids based on the weight of the one or more 1,1-dicarbonyl substituted-1,1 hydroxymethyl-methanes with a zeolite catalyst at a temperature of about 180° C. to about 220° C. for a sufficient time to convert about 96 percent or greater of the one or more 1,1-dicarbonyl substituted-1,1 hydroxymethyl-methanes to one or more 1,1-dicarbonyl substituted-1-ethylenes.

    Abstract translation: 包含约97摩尔％或更多的一种或多种1,1-二羰基取代的-1-乙烯和约3摩尔％或更少的一种或多种1,1-二羰基取代的甲烷的组合物。 一种方法，其包括：以一种或多种1,1-二羰基取代的-1.1羟甲基 - 甲烷和大于200ppm至约1000ppm的一种或多种强酸的流体状态接触一种或多种强酸， ，1-二羰基取代的-1.1羟甲基 - 甲烷与沸石催化剂在约180℃至约220℃的温度下反应足够的时间以转化约96％或更大的一种或多种1,1 - 二羰基取代的-1.1羟甲基 - 甲烷与一个或多个1,1-二羰基取代的-1-乙烯。

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