摘要:
A method of preparing N,N-disubstituted 3,3′-dithiodipropionamide of formula (2) is provided. In the method, 3-mercaptopropi-onamide of formula (4) reacts with an aqueous solution of amine to prepare N-substituted-3-mercaptopropionamide of formula (3) and N-substituted-3-mercaptopropionamide reacts with an aqueous solution of hydrogen peroxide. In addition, a method of preparing substituted 3-isothiazolone is provided. In the method, the produced N,N-disubstituted-3,3′-dithiodipropionamide reacts with a halogenating agent, wherein X and Z are same or different and each selected from the group consisting of hydrogen or a lower alkyl group; Y is selected from the group consisting of hydrogen, an alkyl group of 1 to 18 carbon atoms, a cycloalkyl group of up to 10 carbon atoms, an aralkyl group of up to 10 carbon atoms, an alkyl group of up to 10 carbon atoms, a halogen-, lower alkyl- or lower alkoxy-substituted aryl group, cyano alkyl group, a carboalkoxyalkyl group, a haloalkyl group, an alkoxyalkyl group, an aryloxyalkyl group of up to 12 carbon atoms, an aralkoxyalkyl group of up to 12 carbon atoms, a dialkylaminoalkyl group, an alkylacyl group of up to 8 carbon atoms, a lower alkylsulfonyl group, an arylsulfonyl group of up to 10 carbon atoms, a cyano group and a carbamoyl group.
摘要:
A method of preparing N,N-disubstituted-3,3′-dithiodipropionamide of formula (2) is provided. In the method, 3-mercaptopropionamide of formula (4) reacts with an aqueous solution of amine to prepare N-substituted-3-mercaptopropionamide of formula (3) and N-substituted-3-mercaptopropionamide reacts with an aqueous solution of hydrogen peroxide. In addition, a method of preparing substituted 3-isothiazolone is provided. In the method, the produced N,N-disubstituted-3,3′-dithiodipropionamide reacts with a halogenating agent, wherein X and Z are same or different and each selected from the group consisting of hydrogen or a lower alkyl group; Y is selected from the group consisting of hydrogen, an alkyl group of 1 to 18 carbon atoms, a cycloalkyl group of up to 10 carbon atoms, an aralkyl group of up to 10 carbon atoms, an aryl group of up to 10 carbon atoms, a halogen-, lower alkyl- or lower alkoxy-substituted aryl group, a cyano alkyl group, a carboalkoxyalkyl group, a haloalkyl group, an alkoxyalkyl group, an aryloxyalkyl group of up to 12 carbon atoms, an aralkoxyalkyl group of up to 12 carbon atoms, a dialkylaminoalkyl group, an alkylacyl group of up to 8 carbon atoms, a lower alkylsulfonyl group, an arylsulfonyl group of up to 10 carbon atoms, a cyano group and a carbamoyl group.
摘要:
A method of preparing water free isothiazolone having the steps of obtaining an extract from an aqueous solution containing isothiazolone by using a halogenationed hydrocarbon or nitrated hydrocarbon, removing the halogenationed hydrocarbon or nitrated hydrocarbon from the extract, and adding a organic solvent such as glycol, alcohol and glycol ether provides a water free isothiazolone having a high stability without forming wastes and harmful gas.
摘要:
The present invention relates to antibacterial and antifungal compositions having 3-isothiazolone and polyhexamethyleneguanidine phosphate. These new antiseptic compositions demonstrate a superior degree of effectiveness on a wide spectrum of pathogens. The present invention also relates to the use of these new antiseptic compositions to kill and/or restrain the growth of bacteria and fungi in a variety of applications.
摘要:
The present invention relates to antibacterial and antifungal compositions having 3-isothiazolone and polyhexamethyleneguanidine phosphate. These new antiseptic compositions demonstrate a superior degree of effectiveness on a wide spectrum of pathogens. The present invention also relates to the use of these new antiseptic compositions to kill and/or restrain the growth of bacteria and fungi in a variety of applications.
摘要:
A method of preparing a microbial culture for wastewater treatment comprising the steps of supplying an aerated material derived from an aeration tank (13) to a bioreactor (17) and cultivating a microorganism existing in the aerated material by adding a culture having a relatively long preservation time and a large number of effective microorganisms.
摘要:
A method for preparing asymmetric linear carbonate useful as an electrolyte for lithium secondary battery is disclosed. The method comprises the steps of: removing methyl acetate by a distillation while carrying out a transesterification of dimethyl carbonate with acetate compound in the presence of a basic catalyst; and separating the asymmetric linear carbonate from the transesterification product.
摘要:
An apparatus and a method for beam selection and inter-beam scheduling using beam scanning in a beamformed wireless communication system are provided. A method for transmitting a signal in a transmitting stage includes transmitting a reference signal through at least one transmission beam, receiving channel information of at least one transmission beam from a receiving stage, selecting a first transmission beam for sending a signal to the receiving stage, by considering the channel information of the at least one transmission beam provided from the receiving stage, and performing inter-beam scheduling for the receiving stage by considering ID information of the first transmission beam.
摘要:
A novel copper phthalocyanine compound with low absorptivity in the visible light region and high absorptivity in the near-infrared light region, and a near-infrared absorption filter using the same are disclosed. The near-infrared absorption copper phthalocyanine compound is represented by the following Formula 1, wherein, A2, A3, A6, A7, A10, A11, A14 and A15 are independently OR1, SR2 or a halogen atom, wherein at least four thereof are OR1; A1, A4, A5, A8, A9, A12, A13 and A16 are independently OR1, SR2, NR3R4 or a halogen atom, wherein at least two thereof are NR3R4, and at least four thereof are OR1; R1, R2, R3 and R4 are independently an alkyl group of 1 to 10 carbon atoms, an aryl group of 6 to 10 carbon atoms, or an aralkyl group of 7 to 15 carbon atoms.
摘要翻译:公开了一种在可见光区域具有低吸收率和近红外光区域的高吸收率的新型铜酞菁化合物,以及使用该铜酞菁化合物的近红外吸收滤光片。 近红外吸收铜酞菁化合物由下式1表示,其中,A2,A3,A6,A7,A10,A11,A14和A15独立地为OR1,SR2或卤原子,其中至少四个为OR1 ; A1,A4,A5,A8,A9,A12,A13和A16独立地为OR1,SR2,NR3R4或卤素原子,其中至少两个为NR3R4,其中至少四个为OR1; R 1,R 2,R 3和R 4独立地为1至10个碳原子的烷基,6至10个碳原子的芳基或7至15个碳原子的芳烷基。
摘要:
An apparatus and method for supporting diversity in a beamformed wireless communication system. A method for transmitting a signal in a transmit end includes determining Receive (Rx) beamforming capability information of a receive end, receiving channel information on at least one Transmit (Tx) beam pattern from the receive end, determining at least one Tx beam pattern for transmitting a signal to the receive end, in consideration of Rx beamforming support information of the receive end and the channel information on the at least one Tx beam pattern, and transmitting a signal to the receive end using the at least one Tx beam pattern for transmitting the signal to the receive end.