Method of preparing N,N′-disubstituted-3,3′-dithiodipropionamide and method of preparing substituted 3-isothiazolone by using the same
    1.
    发明授权
    Method of preparing N,N′-disubstituted-3,3′-dithiodipropionamide and method of preparing substituted 3-isothiazolone by using the same 有权
    制备N,N'-二取代-3,3'-二硫代二丙酰胺的方法及其制备取代的3-异噻唑酮的方法

    公开(公告)号:US06506904B1

    公开(公告)日:2003-01-14

    申请号:US10152118

    申请日:2002-05-21

    IPC分类号: C07D27503

    摘要: A method of preparing N,N-disubstituted 3,3′-dithiodipropionamide of formula (2) is provided. In the method, 3-mercaptopropi-onamide of formula (4) reacts with an aqueous solution of amine to prepare N-substituted-3-mercaptopropionamide of formula (3) and N-substituted-3-mercaptopropionamide reacts with an aqueous solution of hydrogen peroxide. In addition, a method of preparing substituted 3-isothiazolone is provided. In the method, the produced N,N-disubstituted-3,3′-dithiodipropionamide reacts with a halogenating agent, wherein X and Z are same or different and each selected from the group consisting of hydrogen or a lower alkyl group; Y is selected from the group consisting of hydrogen, an alkyl group of 1 to 18 carbon atoms, a cycloalkyl group of up to 10 carbon atoms, an aralkyl group of up to 10 carbon atoms, an alkyl group of up to 10 carbon atoms, a halogen-, lower alkyl- or lower alkoxy-substituted aryl group, cyano alkyl group, a carboalkoxyalkyl group, a haloalkyl group, an alkoxyalkyl group, an aryloxyalkyl group of up to 12 carbon atoms, an aralkoxyalkyl group of up to 12 carbon atoms, a dialkylaminoalkyl group, an alkylacyl group of up to 8 carbon atoms, a lower alkylsulfonyl group, an arylsulfonyl group of up to 10 carbon atoms, a cyano group and a carbamoyl group.

    摘要翻译: 提供了制备式(2)的N,N-二取代的3,3'-二硫代二丙酰胺的方法。 在该方法中,式(4)的3-巯基丙酰胺与胺水溶液反应制备式(3)的N-取代-3-巯基丙酰胺,N-取代-3-巯基丙酰胺与过氧化氢水溶液 。 此外,提供了制备取代的3-异噻唑酮的方法。 在该方法中,所制备的N,N-二取代-3,3'-二硫代二丙酰胺与卤化剂反应,其中X和Z相同或不同,各自选自氢或低级烷基; Y选自氢,1至18个碳原子的烷基,至多10个碳原子的环烷基,至多10个碳原子的芳烷基,至多10个碳原子的烷基, 卤素,低级烷基或低级烷氧基取代的芳基,氰基烷基,碳烷氧基烷基,卤代烷基,烷氧基烷基,至多12个碳原子的芳氧基烷基,至多12个碳原子的芳烷氧基烷基 ,二烷基氨基烷基,至多8个碳原子的烷基酰基,低级烷基磺酰基,至多10个碳原子的芳基磺酰基,氰基和氨基甲酰基。

    Method of preparing N,N′-disubstituted-3,3′-dithiodipropionamide and method of preparing substituted 3-isothiazolone by using the same
    2.
    发明授权
    Method of preparing N,N′-disubstituted-3,3′-dithiodipropionamide and method of preparing substituted 3-isothiazolone by using the same 有权
    制备N,N'-二取代-3,3'-二硫代二丙酰胺的方法及其制备取代的3-异噻唑酮的方法

    公开(公告)号:US06479701B1

    公开(公告)日:2002-11-12

    申请号:US09937747

    申请日:2001-09-28

    IPC分类号: C07C23305

    摘要: A method of preparing N,N-disubstituted-3,3′-dithiodipropionamide of formula (2) is provided. In the method, 3-mercaptopropionamide of formula (4) reacts with an aqueous solution of amine to prepare N-substituted-3-mercaptopropionamide of formula (3) and N-substituted-3-mercaptopropionamide reacts with an aqueous solution of hydrogen peroxide. In addition, a method of preparing substituted 3-isothiazolone is provided. In the method, the produced N,N-disubstituted-3,3′-dithiodipropionamide reacts with a halogenating agent, wherein X and Z are same or different and each selected from the group consisting of hydrogen or a lower alkyl group; Y is selected from the group consisting of hydrogen, an alkyl group of 1 to 18 carbon atoms, a cycloalkyl group of up to 10 carbon atoms, an aralkyl group of up to 10 carbon atoms, an aryl group of up to 10 carbon atoms, a halogen-, lower alkyl- or lower alkoxy-substituted aryl group, a cyano alkyl group, a carboalkoxyalkyl group, a haloalkyl group, an alkoxyalkyl group, an aryloxyalkyl group of up to 12 carbon atoms, an aralkoxyalkyl group of up to 12 carbon atoms, a dialkylaminoalkyl group, an alkylacyl group of up to 8 carbon atoms, a lower alkylsulfonyl group, an arylsulfonyl group of up to 10 carbon atoms, a cyano group and a carbamoyl group.

    摘要翻译: 提供制备式(2)的N,N-二取代-3,3'-二硫代二丙酰胺的方法。 在该方法中,式(4)的3-巯基丙酰胺与胺水溶液反应制备式(3)的N-取代-3-巯基丙酰胺,N-取代-3-巯基丙酰胺与过氧化氢水溶液反应。 此外,提供了制备取代的3-异噻唑酮的方法。 在该方法中,所制备的N,N-二取代-3,3'-二硫代二丙酰胺与卤化剂反应,其中X和Z相同或不同,各自选自氢或低级烷基; Y选自氢,1至18个碳原子的烷基,至多10个碳原子的环烷基,至多10个碳原子的芳烷基,至多10个碳原子的芳基, 卤素,低级烷基或低级烷氧基取代的芳基,氰基烷基,碳烷氧基烷基,卤代烷基,烷氧基烷基,至多12个碳原子的芳氧基烷基,至多12个碳原子的芳烷氧基烷基 原子,二烷基氨基烷基,至多8个碳原子的烷基酰基,低级烷基磺酰基,至多10个碳原子的芳基磺酰基,氰基和氨基甲酰基。

    Method For Preparing Asymmetric Linear Carbonate
    7.
    发明申请
    Method For Preparing Asymmetric Linear Carbonate 审中-公开
    制备不对称线性碳酸盐的方法

    公开(公告)号:US20070276151A1

    公开(公告)日:2007-11-29

    申请号:US11667413

    申请日:2005-10-19

    IPC分类号: C07C69/96

    CPC分类号: C07C68/06 C07C68/08 C07C69/96

    摘要: A method for preparing asymmetric linear carbonate useful as an electrolyte for lithium secondary battery is disclosed. The method comprises the steps of: removing methyl acetate by a distillation while carrying out a transesterification of dimethyl carbonate with acetate compound in the presence of a basic catalyst; and separating the asymmetric linear carbonate from the transesterification product.

    摘要翻译: 公开了一种制备用作锂二次电池用电解质的不对称线性碳酸酯的方法。 该方法包括以下步骤:通过蒸馏除去甲酸甲酯,同时在碱性催化剂存在下进行碳酸二甲酯与乙酸酯化合物的酯交换反应; 并将不对称直链碳酸酯与酯交换产物分离。

    Apparatus and method for scheduling using beam scanning in beamformed wireless communication system
    8.
    发明授权
    Apparatus and method for scheduling using beam scanning in beamformed wireless communication system 有权
    在波束形成的无线通信系统中使用波束扫描进行调度的装置和方法

    公开(公告)号:US09154967B2

    公开(公告)日:2015-10-06

    申请号:US13592749

    申请日:2012-08-23

    IPC分类号: H04W16/28 H04W72/04

    CPC分类号: H04W16/28 H04W72/046

    摘要: An apparatus and a method for beam selection and inter-beam scheduling using beam scanning in a beamformed wireless communication system are provided. A method for transmitting a signal in a transmitting stage includes transmitting a reference signal through at least one transmission beam, receiving channel information of at least one transmission beam from a receiving stage, selecting a first transmission beam for sending a signal to the receiving stage, by considering the channel information of the at least one transmission beam provided from the receiving stage, and performing inter-beam scheduling for the receiving stage by considering ID information of the first transmission beam.

    摘要翻译: 提供了一种用于在波束形成的无线通信系统中使用波束扫描的波束选择和波束间调度的装置和方法。 用于在发送级发送信号的方法包括通过至少一个发送波束发送参考信号,从接收级接收至少一个发送波束的信道信息,选择用于向接收台发送信号的第一发送波束, 通过考虑从接收级提供的至少一个发送波束的信道信息,并且通过考虑第一发送波束的ID信息,对接收级进行波束间调度。

    Copper phthalocyanine compounds and near-infrared absorption filter using the same
    9.
    发明授权
    Copper phthalocyanine compounds and near-infrared absorption filter using the same 有权
    铜酞菁化合物和使用其的近红外吸收滤光片

    公开(公告)号:US08691978B2

    公开(公告)日:2014-04-08

    申请号:US13142719

    申请日:2009-11-05

    IPC分类号: C09B47/04

    CPC分类号: C07D487/22

    摘要: A novel copper phthalocyanine compound with low absorptivity in the visible light region and high absorptivity in the near-infrared light region, and a near-infrared absorption filter using the same are disclosed. The near-infrared absorption copper phthalocyanine compound is represented by the following Formula 1, wherein, A2, A3, A6, A7, A10, A11, A14 and A15 are independently OR1, SR2 or a halogen atom, wherein at least four thereof are OR1; A1, A4, A5, A8, A9, A12, A13 and A16 are independently OR1, SR2, NR3R4 or a halogen atom, wherein at least two thereof are NR3R4, and at least four thereof are OR1; R1, R2, R3 and R4 are independently an alkyl group of 1 to 10 carbon atoms, an aryl group of 6 to 10 carbon atoms, or an aralkyl group of 7 to 15 carbon atoms.

    摘要翻译: 公开了一种在可见光区域具有低吸收率和近红外光区域的高吸收率的新型铜酞菁化合物,以及使用该铜酞菁化合物的近红外吸收滤光片。 近红外吸收铜酞菁化合物由下式1表示,其中,A2,A3,A6,A7,A10,A11,A14和A15独立地为OR1,SR2或卤原子,其中至少四个为OR1 ; A1,A4,A5,A8,A9,A12,A13和A16独立地为OR1,SR2,NR3R4或卤素原子,其中至少两个为NR3R4,其中至少四个为OR1; R 1,R 2,R 3和R 4独立地为1至10个碳原子的烷基,6至10个碳原子的芳基或7至15个碳原子的芳烷基。

    APPARATUS AND METHOD FOR SUPPORTING MULTI-ANTENNA TRANSMISSION IN BEAMFORMED WIRELESS COMMUNICATION SYSTEM
    10.
    发明申请
    APPARATUS AND METHOD FOR SUPPORTING MULTI-ANTENNA TRANSMISSION IN BEAMFORMED WIRELESS COMMUNICATION SYSTEM 有权
    支持无线通信系统中多天线传输的装置和方法

    公开(公告)号:US20130045690A1

    公开(公告)日:2013-02-21

    申请号:US13587739

    申请日:2012-08-16

    IPC分类号: H04B7/06

    摘要: An apparatus and method for supporting diversity in a beamformed wireless communication system. A method for transmitting a signal in a transmit end includes determining Receive (Rx) beamforming capability information of a receive end, receiving channel information on at least one Transmit (Tx) beam pattern from the receive end, determining at least one Tx beam pattern for transmitting a signal to the receive end, in consideration of Rx beamforming support information of the receive end and the channel information on the at least one Tx beam pattern, and transmitting a signal to the receive end using the at least one Tx beam pattern for transmitting the signal to the receive end.

    摘要翻译: 一种用于支持波束形成的无线通信系统中的分集的装置和方法。 用于在发送端发送信号的方法包括确定接收端的接收(Rx)波束成形能力信息,从接收端接收关于至少一个发射(Tx)波束图案的信道信息,确定至少一个Tx波束模式, 考虑到接收端的Rx波束形成支持信息和关于至少一个Tx波束图案的信道信息,将信号发送到接收端,并且使用至少一个Tx波束模式将信号发射到接收端,用于发射 信号到接收端。