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    Method of preparing N,N′-disubstituted-3,3′-dithiodipropionamide and method of preparing substituted 3-isothiazolone by using the same
    2.
    发明授权
    Method of preparing N,N′-disubstituted-3,3′-dithiodipropionamide and method of preparing substituted 3-isothiazolone by using the same 有权
    制备N，N'-二取代-3,3'-二硫代二丙酰胺的方法及其制备取代的3-异噻唑酮的方法

    公开(公告)号：US06479701B1

    公开(公告)日：2002-11-12

    申请号：US09937747

    申请日：2001-09-28

    申请人： Seung-Hwan Kim ,  Jeong-Ho Park ,  Jin-Man Kim ,  Soon-Jong Hahn ,  Ki-Seung Choi ,  Myung-Ho Cho

    发明人： Seung-Hwan Kim ,  Jeong-Ho Park ,  Jin-Man Kim ,  Soon-Jong Hahn ,  Ki-Seung Choi ,  Myung-Ho Cho

    IPC分类号： C07C23305

    CPC分类号： C07D275/03 ,  C07C319/20 ,  C07C319/24 ,  C07C323/60

    摘要： A method of preparing N,N-disubstituted-3,3′-dithiodipropionamide of formula (2) is provided. In the method, 3-mercaptopropionamide of formula (4) reacts with an aqueous solution of amine to prepare N-substituted-3-mercaptopropionamide of formula (3) and N-substituted-3-mercaptopropionamide reacts with an aqueous solution of hydrogen peroxide. In addition, a method of preparing substituted 3-isothiazolone is provided. In the method, the produced N,N-disubstituted-3,3′-dithiodipropionamide reacts with a halogenating agent, wherein X and Z are same or different and each selected from the group consisting of hydrogen or a lower alkyl group; Y is selected from the group consisting of hydrogen, an alkyl group of 1 to 18 carbon atoms, a cycloalkyl group of up to 10 carbon atoms, an aralkyl group of up to 10 carbon atoms, an aryl group of up to 10 carbon atoms, a halogen-, lower alkyl- or lower alkoxy-substituted aryl group, a cyano alkyl group, a carboalkoxyalkyl group, a haloalkyl group, an alkoxyalkyl group, an aryloxyalkyl group of up to 12 carbon atoms, an aralkoxyalkyl group of up to 12 carbon atoms, a dialkylaminoalkyl group, an alkylacyl group of up to 8 carbon atoms, a lower alkylsulfonyl group, an arylsulfonyl group of up to 10 carbon atoms, a cyano group and a carbamoyl group.

    摘要翻译： 提供制备式（2）的N，N-二取代-3,3'-二硫代二丙酰胺的方法。 在该方法中，式（4）的3-巯基丙酰胺与胺水溶液反应制备式（3）的N-取代-3-巯基丙酰胺，N-取代-3-巯基丙酰胺与过氧化氢水溶液反应。 此外，提供了制备取代的3-异噻唑酮的方法。 在该方法中，所制备的N，N-二取代-3,3'-二硫代二丙酰胺与卤化剂反应，其中X和Z相同或不同，各自选自氢或低级烷基; Y选自氢，1至18个碳原子的烷基，至多10个碳原子的环烷基，至多10个碳原子的芳烷基，至多10个碳原子的芳基， 卤素，低级烷基或低级烷氧基取代的芳基，氰基烷基，碳烷氧基烷基，卤代烷基，烷氧基烷基，至多12个碳原子的芳氧基烷基，至多12个碳原子的芳烷氧基烷基 原子，二烷基氨基烷基，至多8个碳原子的烷基酰基，低级烷基磺酰基，至多10个碳原子的芳基磺酰基，氰基和氨基甲酰基。

    Method of preparing N,N′-disubstituted-3,3′-dithiodipropionamide and method of preparing substituted 3-isothiazolone by using the same
    5.
    发明授权
    Method of preparing N,N′-disubstituted-3,3′-dithiodipropionamide and method of preparing substituted 3-isothiazolone by using the same 有权
    制备N，N'-二取代-3,3'-二硫代二丙酰胺的方法及其制备取代的3-异噻唑酮的方法

    公开(公告)号：US06506904B1

    公开(公告)日：2003-01-14

    申请号：US10152118

    申请日：2002-05-21

    申请人： Seung-Hwan Kim ,  Jeong-Ho Park ,  Jin-Man Kim ,  Soon-Jong Hahn ,  Ki-Seong Choi ,  Myung-Ho Cho

    发明人： Seung-Hwan Kim ,  Jeong-Ho Park ,  Jin-Man Kim ,  Soon-Jong Hahn ,  Ki-Seong Choi ,  Myung-Ho Cho

    IPC分类号： C07D27503

    CPC分类号： C07D275/03 ,  C07C319/20 ,  C07C319/24 ,  C07C323/60

    摘要： A method of preparing N,N-disubstituted 3,3′-dithiodipropionamide of formula (2) is provided. In the method, 3-mercaptopropi-onamide of formula (4) reacts with an aqueous solution of amine to prepare N-substituted-3-mercaptopropionamide of formula (3) and N-substituted-3-mercaptopropionamide reacts with an aqueous solution of hydrogen peroxide. In addition, a method of preparing substituted 3-isothiazolone is provided. In the method, the produced N,N-disubstituted-3,3′-dithiodipropionamide reacts with a halogenating agent, wherein X and Z are same or different and each selected from the group consisting of hydrogen or a lower alkyl group; Y is selected from the group consisting of hydrogen, an alkyl group of 1 to 18 carbon atoms, a cycloalkyl group of up to 10 carbon atoms, an aralkyl group of up to 10 carbon atoms, an alkyl group of up to 10 carbon atoms, a halogen-, lower alkyl- or lower alkoxy-substituted aryl group, cyano alkyl group, a carboalkoxyalkyl group, a haloalkyl group, an alkoxyalkyl group, an aryloxyalkyl group of up to 12 carbon atoms, an aralkoxyalkyl group of up to 12 carbon atoms, a dialkylaminoalkyl group, an alkylacyl group of up to 8 carbon atoms, a lower alkylsulfonyl group, an arylsulfonyl group of up to 10 carbon atoms, a cyano group and a carbamoyl group.

    摘要翻译： 提供了制备式（2）的N，N-二取代的3,3'-二硫代二丙酰胺的方法。 在该方法中，式（4）的3-巯基丙酰胺与胺水溶液反应制备式（3）的N-取代-3-巯基丙酰胺，N-取代-3-巯基丙酰胺与过氧化氢水溶液 。 此外，提供了制备取代的3-异噻唑酮的方法。 在该方法中，所制备的N，N-二取代-3,3'-二硫代二丙酰胺与卤化剂反应，其中X和Z相同或不同，各自选自氢或低级烷基; Y选自氢，1至18个碳原子的烷基，至多10个碳原子的环烷基，至多10个碳原子的芳烷基，至多10个碳原子的烷基， 卤素，低级烷基或低级烷氧基取代的芳基，氰基烷基，碳烷氧基烷基，卤代烷基，烷氧基烷基，至多12个碳原子的芳氧基烷基，至多12个碳原子的芳烷氧基烷基 ，二烷基氨基烷基，至多8个碳原子的烷基酰基，低级烷基磺酰基，至多10个碳原子的芳基磺酰基，氰基和氨基甲酰基。

    Bioreactor for sewage and wastewater treatment
    8.
    发明授权
    Bioreactor for sewage and wastewater treatment 有权
    污水和污水处理生物反应器

    公开(公告)号：US07329539B2

    公开(公告)日：2008-02-12

    申请号：US10343673

    申请日：2002-06-03

    申请人： Wan-Pyo Hong ,  Jin-Man Kim ,  Ki-Seung Choi ,  Hi-Weon Jung ,  Soon-Jong Hahn ,  Jong-Taek Kim

    发明人： Wan-Pyo Hong ,  Jin-Man Kim ,  Ki-Seung Choi ,  Hi-Weon Jung ,  Soon-Jong Hahn ,  Jong-Taek Kim

    IPC分类号： C12M1/00 ,  C12M3/00 ,  C12M1/02 ,  C12M1/09 ,  C12M1/12

    CPC分类号： C02F3/1284 ,  C02F3/348 ,  C02F2209/02 ,  Y02W10/15

    摘要： The present invention relates to a bioreactor for sewage and wastewater treatment, which is capable of agitating and supplying oxygen simultaneously. A bioreactor of the present invention, comprises a culture drum in which microorganisms are cultured; a supplier for supplying a culture solution, and organic and inorganic media to the culture drum, the supplier including a supply tube connected to an upper side of the culture drum, and a pump connected to the supply tube for supplying the culture solution to the culture drum; an agitator for agitating the culture solution by spraying air into the culture solution in the culture drum, the air being supplied from an air blower; and a thermostatic controller for controlling a temperature of the culture solution and disinfecting the interior of the culture drum.

    摘要翻译： 本发明涉及一种用于污水和废水处理的生物反应器，其能够同时搅动和供应氧气。 本发明的生物反应器包括其中培养微生物的培养桶; 用于向培养鼓供应培养溶液的供应商和有机和无机介质，供应商包括连接到培养桶上侧的供应管，以及连接到供应管的泵，用于将培养溶液提供给培养物 鼓; 用于通过将空气喷入培养筒中的培养液中来搅拌培养液的搅拌器，从鼓风机供给的空气; 以及用于控制培养液温度并对培养筒内部进行消毒的恒温控制器。

    Antifouling paint composition
    9.
    发明授权
    Antifouling paint composition 失效
    防污漆组成

    公开(公告)号：US07108741B2

    公开(公告)日：2006-09-19

    申请号：US10529463

    申请日：2003-10-23

    申请人： Kyung-Wook Yang ,  Nam-Sik Park ,  Ki-Seung Choi ,  Soon-Jong Hahn ,  Jin-Man Kim ,  Wan-Pyo Hong

    发明人： Kyung-Wook Yang ,  Nam-Sik Park ,  Ki-Seung Choi ,  Soon-Jong Hahn ,  Jin-Man Kim ,  Wan-Pyo Hong

    IPC分类号： C09D5/16 ,  A01N33/00

    CPC分类号： C09D5/1637

    摘要： A novel antifouling paint composition is disclosed. The antifouling paint composition comprises a resin of 5 to 20 wt %, a solvent of 3 to 30 wt %; a polyhexamethyleneguanidine salt of the following chemical formula 1 of 0.05 to 20 wt %, a pigment of 1 to 50 wt %; and cuprous oxide of 22 to 75 wt % and/or zinc pyrithione of the following chemical formula 2 of 0.05 to 20 wt %; wherein in chemical formula 1, X can be the same or different, and at least one of X is an inorganic acid salt or an organic acid salt; R1 can be the same or different, and is a linear or branched alkyl group containing from 1 to 20 carbon atoms, a phenyl group, a chlorophenyl group, a bromophenyl group, an iodophenyl group, a benzyl group, a chlorobenzyl group, a bromobenzyl group, a iodobenzyl group, a phenethyl group, a naphthyl group or a hydrogen; and n is an integer of 1 or more.

    摘要翻译： 公开了一种新型防污涂料组合物。 防污涂料组合物包含5至20重量％的树脂，3至30重量％的溶剂; 以下化学式1的聚六亚甲基胍盐为0.05〜20重量％，颜料为1〜50重量％ 和22〜75重量％的氧化亚铜和/或以下化学式2的吡啶硫酮锌为0.05〜20重量％ 其中在化学式1中，X可以相同或不同，X中的至少一个是无机酸盐或有机酸盐; R 1可以相同或不同，为含有1〜20个碳原子的直链或支链烷基，苯基，氯苯基，溴苯基，碘苯基，苄基 基团，氯苄基，溴苄基，碘苄基，苯乙基，萘基或氢; n为1以上的整数。

    ANTIFOULING PAINT COMPOSITION
    10.
    发明申请
    ANTIFOULING PAINT COMPOSITION 失效
    防油漆组合物

    公开(公告)号：US20060137566A1

    公开(公告)日：2006-06-29

    申请号：US10529463

    申请日：2003-10-23

    申请人： Kyung-Wook Yang ,  Nam-Sik Park ,  Ki-Seung Choi ,  Soon-Jong Hahn ,  Jin-Man Kim ,  Wan-Pyo Hong

    发明人： Kyung-Wook Yang ,  Nam-Sik Park ,  Ki-Seung Choi ,  Soon-Jong Hahn ,  Jin-Man Kim ,  Wan-Pyo Hong

    IPC分类号： C09D5/14

    CPC分类号： C09D5/1637

    摘要： A novel antifouling paint composition is disclosed. The antifouling paint composition comprises a resin of 5 to 20 weight %; a solvent of 3 to 30 weight %; polyhexamethyleneguanidine salt of the following chemical formula 1 of 0.05 to 20 weight %; a pigment of 1 to 50 weight %; and cuprous oxide of 22 to 75 weight % and/or zinc pyrithione of the following chemical formula 2 of 0.05 to 20 weight %. [Chemical formula 1] [Chemical formula 2] In chemical formula 1, at least one of X is an inorganic acid salt or an organic acid salt; R1 is an alkyl group, a phenyl group, a benzyl group, a phenethyl group, a naphthyl group or hydrogen, and n is an integer of 1 or more.

    摘要翻译： 公开了一种新型防污涂料组合物。 防污漆组合物包含5〜20重量％的树脂; 3〜30重量％的溶剂; 以下化学式1的聚六亚甲基胍盐为0.05〜20重量％; 1〜50重量％的颜料; 和22〜75重量％的氧化亚铜和/或以下化学式2的吡啶硫酮锌为0.05〜20重量％。 [化学式1] [化学式2]在化学式1中，X中的至少一个是无机酸盐或有机酸盐; R1是烷基，苯基，苄基，苯乙基，萘基或氢，n是1以上的整数。