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    Process for Continous Production of Carbon Fibres
    3.
    发明申请
    Process for Continous Production of Carbon Fibres 审中-公开
    碳纤维连续生产工艺

    公开(公告)号：US20090277772A1

    公开(公告)日：2009-11-12

    申请号：US12226325

    申请日：2007-03-31

    申请人： Mathias Kaiser ,  Lukas Alberts ,  Frank Henning ,  Rudolf Emmerich ,  Christian Hunyar ,  Klaus-Dieter Nauenburg ,  Ralf Dreher ,  Peter Elsner ,  Bernd Wohlmann

    发明人： Mathias Kaiser ,  Lukas Alberts ,  Frank Henning ,  Rudolf Emmerich ,  Christian Hunyar ,  Klaus-Dieter Nauenburg ,  Ralf Dreher ,  Peter Elsner ,  Bernd Wohlmann

    IPC分类号： B01J19/12

    CPC分类号： D01F9/328 ,  D01F9/14 ,  D01F9/225

    摘要： A process for continuous production of carbon fibres whereby stabilised precursor fibres are carbonised and graphitised with the help of high-frequency electromagnetic waves, characterised in that the stabilised precursor fibres are continuously conveyed, as the inner conductor of a coaxial conductor consisting of an outer and an inner conductor, through the coaxial conductor and a treatment zone; that the stabilised precursor fibres are irradiated in the treatment zone with high-frequency electromagnetic waves that are absorbed by the precursor fibres, which are thereby heated and converted into carbon fibres; and that the stabilised precursor fibres or carbon fibres are conveyed under an inert gas atmosphere through the coaxial conductor and the treatment zone.

    摘要翻译： 一种用于连续生产碳纤维的方法，其中借助于高频电磁波将稳定的前体纤维碳化并石墨化，其特征在于，稳定化的前体纤维作为同轴导体的内部导体被连续输送，该同轴导体由外部和 内导体，通过同轴导体和处理区; 在处理区中将稳定化的前体纤维照射到被前体纤维吸收的高频电磁波，由此被加热并转化为碳纤维; 并且通过同轴导体和处理区在惰性气体气氛下输送稳定化的前体纤维或碳纤维。

    THERMOPLASTIC LIGNIN FOR PRODUCING CARBON FIBERS
    5.
    发明申请
    THERMOPLASTIC LIGNIN FOR PRODUCING CARBON FIBERS 审中-公开
    用于生产碳纤维的热塑性树脂

    公开(公告)号：US20130183227A1

    公开(公告)日：2013-07-18

    申请号：US13823987

    申请日：2011-09-08

    申请人： Bernd Wohlmann ,  Michael Wolki ,  Silke Stusgen

    发明人： Bernd Wohlmann ,  Michael Wolki ,  Silke Stusgen

    IPC分类号： C07G1/00

    CPC分类号： C07G1/00 ,  C08H6/00 ,  D01F9/17

    摘要： A fusible lignin has a gas transition temperature in the range between 90 and 160° C. determined using differential scanning calorimetry (DSC), a molar mass distribution with a dispersivity of less than 28, determined using gel permeation chromatography (GPC), an ash content of less than 1 wt. %, and a proportion of volatile components of a maximum of 1 wt. %. Also provided is a precursor fiber based on the fusible lignin, as well as a method for the production thereof Also provided is a method for producing a carbon fiber from the precursor fiber.

    摘要翻译： 熔融木质素的气体转变温度在90至160℃的范围内，使用差示扫描量热法（DSC）测定，使用凝胶渗透色谱（GPC）测定的分散度小于28的摩尔质量分数，灰分 含量小于1重量％ ％，挥发性成分的比例最大为1重量％。 ％。 还提供了基于可熔性木质素的前体纤维，以及其生产方法。还提供了从前体纤维制备碳纤维的方法。

    HOLLOW CARBON FIBRES AND PROCESS FOR THEIR PRODUCTION
    6.
    发明申请
    HOLLOW CARBON FIBRES AND PROCESS FOR THEIR PRODUCTION 审中-公开
    中空碳纤维及其生产工艺

    公开(公告)号：US20110104489A1

    公开(公告)日：2011-05-05

    申请号：US12674995

    申请日：2008-09-17

    申请人： Michael Wolki ,  Bernd Wohlmann ,  Mathias Kaiser ,  Rudolf Emmerich ,  Frank Henning

    发明人： Michael Wolki ,  Bernd Wohlmann ,  Mathias Kaiser ,  Rudolf Emmerich ,  Frank Henning

    IPC分类号： D02G3/02 ,  C01B31/02 ,  D02G3/22

    CPC分类号： B01D71/021 ,  B01D67/0067 ,  B01D69/08 ,  B01D69/081 ,  B01D2323/42 ,  B01D2325/40 ,  D01D5/24 ,  D01F9/225 ,  Y10T428/2918

    摘要： A process for the production of hollow carbon fibres by the treatment of a stabilised carbon fibre precursor in an application device using high-frequency electromagnetic waves. The application device includes structure supplying the electromagnetic waves to a outcoupling region and a hollow outer conductor terminating in the outcoupling region. For the treatment, a field of the high-frequency electromagnetic waves is generated and a field strength in the range from 15 to 40 kV/m is set in the outcoupling region of the application device. The stabilised carbon fibre precursor is conveyed continuously as an inner conductor through the hollow outer conductor, thereby forming a coaxial conductor having an outer and an inner conductor, and through the subsequent outcoupling region. An inert gas atmosphere is created in the coaxial conductor and in the outcoupling region by passing through an inert gas.

    摘要翻译： 一种通过在使用高频电磁波的应用装置中处理稳定的碳纤维前体来生产中空碳纤维的方法。 应用装置包括将电磁波提供给输出耦合区域和终止于输出耦合区域的中空外部导体的结构。 为了处理，产生高频电磁波的场，并且在应用装置的输出耦合区域中设定在15至40kV / m范围内的场强。 稳定的碳纤维前体作为内导体通过中空外导体连续输送，从而形成具有外导体和内导体的同轴导体，并通过随后的外耦合区域。 在同轴导体和外耦合区域中通过惰性气体产生惰性气体气氛。

    Fiber preform made from reinforcing fiber bundles and comprising unidirectional fiber tapes, and composite component
    8.
    发明授权
    Fiber preform made from reinforcing fiber bundles and comprising unidirectional fiber tapes, and composite component 有权
    由增强纤维束制成并包括单向纤维带和复合部件的纤维预制件

    公开(公告)号：US08840988B2

    公开(公告)日：2014-09-23

    申请号：US13988216

    申请日：2011-11-11

    申请人： Bernd Wohlmann ,  Markus Schneider ,  Andreas Woginger ,  Frank Oberwahrenbrock

    发明人： Bernd Wohlmann ,  Markus Schneider ,  Andreas Woginger ,  Frank Oberwahrenbrock

    IPC分类号： B32B27/04 ,  B29C70/88 ,  B29C70/08 ,  B29B11/16 ,  D04H13/00 ,  B29K707/04

    CPC分类号： D04H13/00 ,  B29B11/16 ,  B29C70/081 ,  B29C70/887 ,  B29K2707/04 ,  Y10T428/249921 ,  Y10T428/249924 ,  Y10T428/24994 ,  Y10T428/249947

    摘要： A fiber preform for producing fiber composite structures, a wall thereof including a first zone made from reinforcing fiber bundles having a first resin composition and a second zone made from at least one fiber tape comprising at least one unidirectionally directed reinforcing yarn strand having a second resin composition. The reinforcing fiber bundles in the first zone are oriented in different spatial directions to each other when viewed in a direction parallel to the extension of the thickness. Each reinforcing fiber has a length of from 3 to 50 mm, and contains the first resin composition in a concentration of from 1 to 10 wt % of the fiber weight. The wall of the fiber preform has a proportion of reinforcing fibers of more than 35 vol %, and the second zone forms a discrete region when viewed in a direction perpendicular to the thickness extension of the wall.

    摘要翻译： 一种用于生产纤维复合结构的纤维预制件，其壁包括由具有第一树脂组合物的增强纤维束制成的第一区和由至少一个纤维带制成的第二区，所述纤维带包括至少一个单向指向的增强纱线，其具有第二树脂 组成。 当从与厚度的延伸平行的方向观察时，第一区域中的增强纤维束彼此在不同的空间方向上取向。 每个增强纤维的长度为3至50mm，并且含有浓度为纤维重量的1至10重量％的第一树脂组合物。 纤维预制件的壁具有大于35体积％的增强纤维的比例，当从垂直于壁的厚度延伸的方向观察时，第二区形成离散区域。

    FLEXIBLE REINFORCING FIBER YARN PRE-IMPREGNATED WITH RESIN
    9.
    发明申请
    FLEXIBLE REINFORCING FIBER YARN PRE-IMPREGNATED WITH RESIN 审中-公开
    柔性增强纤维纱预先用树脂印迹

    公开(公告)号：US20140205831A1

    公开(公告)日：2014-07-24

    申请号：US14235564

    申请日：2012-07-20

    申请人： Markus Schneider ,  Silke Stüsgen ,  Silke Witzel ,  Bernd Wohlmann

    发明人： Markus Schneider ,  Silke Stüsgen ,  Silke Witzel ,  Bernd Wohlmann

    IPC分类号： D06M15/55

    CPC分类号： D06M15/55 ,  C08J5/06 ,  C08J5/24 ,  C08J2363/02 ,  Y10T428/249921 ,  Y10T428/2927 ,  Y10T428/2938

    摘要： A pre-impregnated yarn having a bundle made of reinforcing fiber filaments impregnated with a first resin composition infiltrated into the pre-impregnated yarn and at least partially connected via the first resin composition. The first resin composition contains at least two bisphenol A epichlorohydrin resins H1 and H2 in a weight ratio H1:H2 of 1.1 to 1.4, and an aromatic polyhydroxy ether P1. The pre-impregnated yarn has a second resin composition on the bundle outer side in the form of adhesive particles or drops. The second resin composition is solid at ambient temperatures and has a melting temperature in the range from 80 to 150° C. The bundle interior and at least 50% of the surface of the bundle outer side are free of the second resin composition.

    摘要翻译： 一种预浸渍纱线，其具有由增强纤维丝制成的束，浸渍有浸渍到预浸渍纱线中并且经由第一树脂组合物至少部分连接的第一树脂组合物。 第一种树脂组合物含有至少两种重量比H1:H2为1.1〜1.4的双酚A表氯醇树脂H1和H2，以及芳族多羟基醚P1。 预浸渍纱线在捆外侧具有粘合剂颗粒或滴剂形式的第二树脂组合物。 第二树脂组合物在环境温度下是固体，并且具有在80至150℃范围内的熔融温度。束内部和束外侧表面的至少50％不含第二树脂组合物。

    STABILIZATION OF POLYACRYLONITRILE PRECURSOR YARNS
    10.
    发明申请
    STABILIZATION OF POLYACRYLONITRILE PRECURSOR YARNS 审中-公开
    聚丙烯腈前驱纱线的稳定性

    公开(公告)号：US20120137446A1

    公开(公告)日：2012-06-07

    申请号：US13390635

    申请日：2010-08-31

    申请人： Bernd Wohlmann ,  Michael Wolki ,  Christian Hunyar ,  Rudolf Emmerich ,  Mathias Kaiser ,  Matthias Graf ,  Lukas Alberts ,  Klaus-Dieter Nauenburg

    发明人： Bernd Wohlmann ,  Michael Wolki ,  Christian Hunyar ,  Rudolf Emmerich ,  Mathias Kaiser ,  Matthias Graf ,  Lukas Alberts ,  Klaus-Dieter Nauenburg

    IPC分类号： C08J7/12

    CPC分类号： D06M10/04 ,  D01F9/225 ,  D06M10/06 ,  D06M2101/28

    摘要： A method for stabilizing yarns made from polyacrylonitrile using chemical stabilization reactions, including: generating a field of high-frequency electromagnetic waves in an application space of an applicator, which has areas with minimum electric field strength and areas with maximum electric field strength, the maximum electric field strength in the application space being in a range from 3 to 150 kV/m; continuously supplying a precursor yarn based on a polyacrylonitrile polymer into the application space, and conveying the precursor yarn through the application space and through the field of the high-frequency electromagnetic waves; introducing a process gas into the application space and conveying the process gas through the application space with a flow rate of at least 0.1 m/s relative to the precursor yarn being conveyed through the application space, wherein a temperature of the process gas is in a range between 150 and 300° C., so that it is above a critical minimum temperature Tcrit and below a maximum temperature Tmax.

    摘要翻译： 一种用于使用化学稳定反应稳定由聚丙烯腈制成的纱线的方法，包括：在施加器的施加空间中产生高频电磁场，其具有最小电场强度和最大电场强度的区域，最大值 应用空间的电场强度在3〜150kV / m的范围内; 将基于聚丙烯腈聚合物的前体纱线连续地供给到涂布空间中，并通过涂布空间和高频电磁波的领域输送前体纱线; 将工艺气体引入所述应用空间中，并且以相对于通过所述施加空间传送的所述前体纱线的流速为至少0.1m / s的速度将所述工艺气体输送通过所述施加空间，其中所述处理气体的温度为 范围在150和300℃之间，使得其高于临界最低温度Tcrit并低于最大温度Tmax。