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公开(公告)号：US4687757A
公开(公告)日：1987-08-18
申请号：US843489
申请日：1986-03-24
摘要： A composition of matter comprising alumina, at least one compound of titanium and at least one compound of molybdenum is prepared either by the steps of impregnating an alumina support material with an aqueous solution of at least one titanium compound, drying, impregnating the Ti-impregnated material with an aqueous solution of at least one molybdenum compound, drying and calcining; or by the steps of impregnating an alumina support material with an aqueous solution of at least one titanium compound and at least one molybdenum compound, drying and calcining. The compositions of matter of this invention are useful as catalysts for hydrotreating substantially liquid hydrocarbon-containing feed streams (particularly heavy oils) which also contain compounds of nickel, vanadium and sulfur.
摘要翻译： 包含氧化铝，至少一种钛化合物和至少一种钼化合物的物质组合物可以通过以下步骤制备：用至少一种钛化合物的水溶液浸渍氧化铝载体材料，干燥，浸渍Ti浸渍 材料与至少一种钼化合物的水溶液，干燥和煅烧; 或通过用至少一种钛化合物和至少一种钼化合物的水溶液浸渍氧化铝载体材料的步骤，干燥和煅烧。 本发明的物质组合物可用作加氢处理基本上液体含烃的进料流（特别是重油）的催化剂，其还含有镍，钒和硫化合物。
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公开(公告)号：US4588706A
公开(公告)日：1986-05-13
申请号：US748112
申请日：1985-06-24
申请人： Simon G. Kukes , Stephen L. Parrott
发明人： Simon G. Kukes , Stephen L. Parrott
IPC分类号： B01J27/188 , C10G45/08 , B01J27/19
CPC分类号： B01J27/188 , C10G45/08
摘要： A catalyst composition is prepared by dissolving a suitable oxygen containing compound of a Group VIB metal (preferably Mo), a suitable compound of a Group VIII metal (preferably Ni) and phosphorous acid in water, mixing this solution with an alumina containing support material, and calcining this mixture. This catalyst composition is used primarily for hydrotreating of hydrocarbon feed stream, which contain nitrogen and sulfur impurities, particularly heavy cycle oils.
摘要翻译： 通过将VIB族金属（优选Mo），适合的VIII族金属（优选Ni）和亚磷酸的合适的化合物溶解在水中来制备催化剂组合物，将该溶液与含氧化铝的载体材料混合， 并煅烧该混合物。 该催化剂组合物主要用于加氢处理含有氮和硫杂质的烃进料流，特别是重循环油。
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公开(公告)号：US4724069A
公开(公告)日：1988-02-09
申请号：US896916
申请日：1986-08-15
IPC分类号： C07F15/02 , B01J23/88 , B01J23/94 , C07F15/06 , C10G45/02 , C10G45/12 , C10G45/00 , C10G45/06
CPC分类号： C10G45/02
摘要： An additive comprising a metal naphthenate selected from the group consisting of cobalt naphthenate and iron naphthenate is mixed with a hydrocarbon-containing feed stream. The hydrocarbon-containing feed stream containing the additive is then contacted in a hydrofining process with a catalyst composition comprising a support selected from the group consisting of alumina, silica and silica-alumina and a promoter comprising at least one metal selected from Group VIB, Group VIIB and Group VIII of the Periodic Table. The introduction of the inventive additive may be commenced when the catalyst is new, partially deactivated or spent with a beneficial result occuring in each case.
摘要翻译： 将包含选自环烷酸钴和环烷酸铁的环烷酸金属的添加剂与含烃进料流混合。 然后将含有添加剂的含烃进料物流在加氢精制过程中与包含选自氧化铝，二氧化硅和二氧化硅 - 氧化铝的载体的催化剂组合物和包含至少一种选自组VIB的金属的组合物 VIIB和第八期。 本发明添加剂的引入可以在催化剂是新的，部分失活的或在每种情况下产生有益结果的情况下消耗或开始。
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公开(公告)号：US4652361A
公开(公告)日：1987-03-24
申请号：US878558
申请日：1986-06-26
申请人： Simon G. Kukes , Stephen L. Parrott
发明人： Simon G. Kukes , Stephen L. Parrott
CPC分类号： B01J21/066 , B01J23/00 , B01J23/10 , C10G45/04
摘要： A composition of matter consisting essentially of alumina and at least one compound (preferably oxide) of yttrium and/or zirconium is provided and is employed as a catalyst in the hydrotreating of a substantially liquid hydrocarbon containing feed stream (particularly a heavy oil) which also contains compounds of nickel, vanadium and sulfur. The preferred preparation of the catalyst compositions of this invention comprises at least one impregnating step using a solution containing at least one aluminum compound, which is at least partially converted to aluminum oxide in a subsequent calcining step.
摘要翻译： 提供了基本上由氧化铝和至少一种钇和/或锆化合物（优选氧化物）组成的物质组合物，并且用作加氢处理基本上液体的含烃进料流（特别是重油）中的催化剂， 含有镍，钒和硫的化合物。 本发明的催化剂组合物的优选制备方法包括使用至少一种铝化合物的溶液进行至少一次浸渍步骤，该化合物在随后的煅烧步骤中至少部分转化为氧化铝。
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公开(公告)号：US4585751A
公开(公告)日：1986-04-29
申请号：US748113
申请日：1985-06-24
IPC分类号： B01J23/885 , B01J27/19 , C10G45/04
CPC分类号： C10G45/04 , B01J23/885 , B01J27/19
摘要： A catalyst composition is prepared by dissolving a suitable molybdenum and oxygen containing compound (preferably MoO.sub.3), a suitable divalent copper and/or manganese compound and a suitable phosphorus and oxygen containing compound (preferably H.sub.3 PO.sub.4) in water, mixing this solution with an alumina-containing support material, and calcining this mixture. This catalyst composition is used primarily for hydrotreating of hydrocarbon feed streams, which contain sulfur, vanadium and nickel impurities, particularly heavy oils.
摘要翻译： 通过将合适的含钼和氧的化合物（优选MoO 3），合适的二价铜和/或锰化合物和合适的含磷和氧的化合物（优选H 3 PO 4）溶解在水中来制备催化剂组合物，将该溶液与氧化铝 - 含有载体材料，并煅烧该混合物。 该催化剂组合物主要用于加氢处理含有硫，钒和镍杂质，特别是重油的烃进料流。
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公开(公告)号：US4565800A
公开(公告)日：1986-01-21
申请号：US748110
申请日：1985-06-24
IPC分类号： B01J23/847 , C10G45/06 , B01J23/22
CPC分类号： C10G45/06 , B01J23/8472
摘要： A catalyst composition is prepared by dissolving a suitable vanadium and oxygen containing compound, a suitable nickel (II) compound and ammonia in water, mixing this solution with an alumina containing support material, and calcining this mixture. This catalyst composition is used primarily for hydrotreating of hydrocarbon feed stream, which contain nickel, vanadium and sulfur impurities, particularly heavy oils.
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公开(公告)号：US4775652A
公开(公告)日：1988-10-04
申请号：US135904
申请日：1987-12-21
CPC分类号： C10G45/16
摘要： An additive comprising a mixture of at least one decomposable molybdenum compound selected from the group consisting of molybdenum dithiophosphates and molybdenum dithiocarbamates and at least one decomposable nickel compound selected from the group consisting of nickel dithiophosphates and nickel dithiocarbamates is mixed with a hydrocarbon-containing feed stream. The hydrocarbon-containing feed stream containing the additive is then contacted in a hydrofining process with a catalyst composition comprising a support selected from the group consisting of alumina, silica and silica-alumina and a promoter comprising at least one metal selected from Group VIB, Group VIIB and Group VIII of the Periodic Table. The introduction of the inventive additive may be commenced when the catalyst is new, partially deactivated or spent with a beneficial result occuring in each case.
摘要翻译： 包含选自二硫代磷酸钼和二硫代氨基甲酸钼的至少一种可分解的钼化合物和至少一种选自二硫代磷酸镍和二硫代氨基甲酸镍的可分解的镍化合物的混合物的添加剂与含烃进料流 。 然后将含有添加剂的含烃进料物流在加氢精制过程中与包含选自氧化铝，二氧化硅和二氧化硅 - 氧化铝的载体的催化剂组合物和包含至少一种选自组VIB的金属的组合物 VIIB和第八期。 本发明添加剂的引入可以在催化剂是新的，部分失活的或在每种情况下产生有益结果的情况下消耗或开始。
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公开(公告)号：US4687568A
公开(公告)日：1987-08-18
申请号：US909347
申请日：1986-09-19
申请人： Simon G. Kukes , Stephen L. Parrott
发明人： Simon G. Kukes , Stephen L. Parrott
IPC分类号： B01J23/755 , B01J27/185 , C10G45/06 , C10G45/00
CPC分类号： B01J23/755 , B01J27/1853 , C10G45/06
摘要： A process for hydrotreating substantially liquid hydrocarbon-containing feed streams (particularly heavy oils) which also contain compounds of nickel, vanadium and sulfur employing a catalyst composition comprising alumina, at least one compound of nickel, at least one compound of zirconium and at least one compound containing phosphorus and oxygen is prepared by a process comprising the steps of impregnating an alumina-containing support material with an aqueous solution containing at least one nickel compound and at least one zirconium compound, drying, impregnating the Ni/Zr-impregnated material with an aqueous solution containing at least one P-O compound, drying and calcining.
摘要翻译： 一种使用含有氧化铝，至少一种镍化合物，至少一种锆化合物和至少一种化合物的催化剂组合物，其还含有镍，钒和硫化合物的基本上液体含烃的进料流（特别是重油）的加氢处理方法 通过包括以下步骤的方法制备含磷和氧的方法，所述方法包括用含有至少一种镍化合物和至少一种锆化合物的水溶液浸渍含氧化铝的载体材料，干燥，浸渍含有Ni / Zr的材料 含有至少一种PO化合物的水溶液，干燥和煅烧。
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9.发明授权
公开(公告)号：US4681869A
公开(公告)日：1987-07-21
申请号：US781082
申请日：1985-09-27
申请人： Simon G. Kukes , Stephen L. Parrott
发明人： Simon G. Kukes , Stephen L. Parrott
CPC分类号： B01J21/066 , B01J23/00 , B01J23/10 , C10G45/04
摘要： A composition of matter consisting essentially of alumina and at least one compound (preferably oxide) of yttrium and/or zirconium is provided and is employed as a catalyst in the hydrotreating of a substantially liquid hydrocarbon containing feed stream (particularly a heavy oil) which also contains compounds of nickel, vanadium and sulfur. The preferred preparation of the catalyst compositions of this invention comprises at least one impregnating step using a solution containing at least one aluminum compound, which is at least partially converted to aluminum oxide in a subsequent calcining step.
摘要翻译： 提供了基本上由氧化铝和至少一种钇和/或锆化合物（优选氧化物）组成的物质组合物，并且用作加氢处理基本上液体的含烃进料流（特别是重油）中的催化剂， 含有镍，钒和硫的化合物。 本发明的催化剂组合物的优选制备方法包括使用至少一种铝化合物的溶液进行至少一次浸渍步骤，该化合物在随后的煅烧步骤中至少部分转化为氧化铝。
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公开(公告)号：US4596654A
公开(公告)日：1986-06-24
申请号：US781816
申请日：1985-09-30
IPC分类号： B01J23/847 , C10G45/06 , C10G45/00
CPC分类号： B01J23/8472 , C10G45/06
摘要： A catalyst composition is prepared by dissolving a suitable vanadium and oxygen containing compound, a suitable nickel (II) compound and ammonia in water, mixing this solution with an alumina containing support material, and calcining this mixture. This catalyst composition is used primarily for hydrotreating of hydrocarbon feed stream, which contain nickel, vanadium and sulfur impurities, particularly heavy oils.
摘要翻译： 通过将合适的含钒和含氧化合物，合适的镍（II）化合物和氨在水中溶解，将该溶液与含氧化铝的载体材料混合并煅烧该混合物来制备催化剂组合物。 该催化剂组合物主要用于加氢处理含有镍，钒和硫杂质，特别是重油的烃进料流。
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