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1.发明授权公开(公告)号：US09079812B2
公开(公告)日：2015-07-14
申请号：US13646002
申请日：2012-10-05
发明人： Vincent Coupard , Natacha Touchais , Stephanie Fleurier , Helena Gonzalez Penas , Philip De Smedt , Walter Vermeiren , Cindy Adam , Delphine Minoux
IPC分类号： C07C1/24
CPC分类号： C07C1/24 , C07C2529/40 , Y02P30/48 , C07C11/04
摘要： A process for dehydration of an ethanol feedstock into ethylene, comprising the vaporization of said dilute hydrated ethanol feedstock in an exchanger, with heat exchange with the effluent that is obtained from a last reactor, with said mixture being introduced into said vaporization stage at a pressure that is lower than the pressure of the effluent that is obtained from the last reactor, the compression of the mixture that is vaporized in a compressor, the introduction of the vaporized and compressed mixture, into at least one adiabatic reactor that contains at least one dehydration catalyst.
摘要翻译： 一种将乙醇原料脱水成乙烯的方法，包括在交换器中蒸发所述稀水合乙醇原料，与最后一个反应器获得的流出物进行热交换，所述混合物在压力下被引入所述蒸发阶段 低于从最后一个反应器获得的流出物的压力，在压缩机中蒸发的混合物的压缩，将蒸发和压缩的混合物引入到至少一个绝热反应器中，该绝热反应器含有至少一个脱水 催化剂。
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2.发明申请公开(公告)号：US20150291485A1
公开(公告)日：2015-10-15
申请号：US14647174
申请日：2013-11-18
发明人： Vincent Coupard , Natacha Touchais , Thomas Plennevaux , Emilie Kobel , Stephanie Fleurier , Walter Vermeiren , Delphine Minoux , Philip De Smedt , Cindy Adam , Nikolai Nesterenko
CPC分类号： C07C1/24 , C07C29/76 , C07C41/09 , C07C2527/173 , C07C2529/40 , C07C2529/85 , C07C11/04 , C07C43/06 , C07C31/08
摘要： The invention relates to a process for dehydration of an ethanol feedstock into ethylene comprising at least the stages: a) A stage for pretreatment of the ethanol feedstock on an acidic solid, b) A stage for evaporation of said pretreated ethanol feedstock in a heat exchanger, c) A stage for superheating said evaporated feedstock in such a way as to bring it to an inlet temperature that is compatible with the temperature of a dehydration reaction, d) A stage for dehydration of said feedstock that is obtained from stage c) in at least one adiabatic reactor that contains at least one dehydration catalyst.
摘要翻译： 本发明涉及一种将乙醇原料脱水成乙烯的方法，至少包括以下阶段：a）用于在酸性固体上预处理乙醇原料的阶段，b）在热交换器中蒸发所述预处理的乙醇原料的阶段 c）用于使所述蒸发的原料过热以使其达到与脱水反应的温度相适应的入口温度的阶段，d）用于脱水所述原料的阶段，其从阶段c） 至少一个含有至少一种脱水催化剂的绝热反应器。
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3.发明授权公开(公告)号：US09650311B2
公开(公告)日：2017-05-16
申请号：US14760827
申请日：2014-01-10
发明人： Vincent Coupard , Thomas Plennevaux , Stephanie Fleurier , Walter Vermeiren , Delphine Minoux , Philip De Smedt , Cindy Adam , Nikolai Nesterenko
IPC分类号： C07C1/24
摘要： Process for the production of ethylene from an ethanol feedstock that comprises these stages: a) dehydration to produce at least ethylene and water effluents, b) partial condensation of said ethylene effluent, c) separating phases of said partially condensed ethylene effluent to produce gas and liquid effluents, d) compression of said gas effluent to produce compressed gas effluent, e) washing said compressed gas effluent by contact with the recycled washing water of stage h) to produce washed gas and waste water effluents, f) absorption of said washed gas effluent by contact with at least an absorbent solution to produce purified gas effluent, g) distilling said waste water effluent and, jointly, said water effluent from said dehydration stage to produce at least gas distillate, liquid distillate, purified water effluent, and distillation residue, h) recycling, as washing water, at least a portion of said purified water effluent upstream from the washing stage e).
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公开(公告)号：US09725376B2
公开(公告)日：2017-08-08
申请号：US14647174
申请日：2013-11-18
发明人： Vincent Coupard , Natacha Touchais , Thomas Plennevaux , Emilie Kobel , Stephanie Fleurier , Walter Vermeiren , Delphine Minoux , Philip De Smedt , Cindy Adam , Nikolai Nesterenko
CPC分类号： C07C1/24 , C07C29/76 , C07C41/09 , C07C2527/173 , C07C2529/40 , C07C2529/85 , C07C11/04 , C07C43/06 , C07C31/08
摘要： The invention relates to a process for dehydration of an ethanol feedstock into ethylene comprising at least the stages: a) A stage for pretreatment of the ethanol feedstock on an acidic solid, b) A stage for evaporation of said pretreated ethanol feedstock in a heat exchanger, c) A stage for superheating said evaporated feedstock in such a way as to bring it to an inlet temperature that is compatible with the temperature of a dehydration reaction, d) A stage for dehydration of said feedstock that is obtained from stage c) in at least one adiabatic reactor that contains at least one dehydration catalyst.
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公开(公告)号：US09663414B2
公开(公告)日：2017-05-30
申请号：US14646877
申请日：2013-11-18
发明人： Vincent Coupard , Natacha Touchais , Thomas Plennevaux , Emilie Kobel , Stephanie Fleurier , Walter Vermeiren , Delphine Minoux , Philip De Smedt , Cindy Adam , Nikolai Nesterenko
CPC分类号： C07C1/24 , C07C29/76 , C07C41/09 , C07C2527/173 , C07C2529/40 , C07C2529/85 , Y02P30/48 , C07C43/06 , C07C11/04 , C07C31/08
摘要： A process for dehydration of an ethanol feedstock to ethylene by: a) preheating ethanol feedstock by heat exchange with effluent from e), b) pretreating the ethanol feedstock to produce pretreated ethanol feedstock, c) vaporizing a vaporization feedstock containing pretreated ethanol feedstock and at least a portion of the flow of treated water recycled in an exchanger to produce a vaporized feedstock, d) compressing said vaporized feedstock to produce a compressed feedstock, e) dehydrating said compressed feedstock in at least one adiabatic reactor, f) separating the effluent from the last adiabatic reactor of e) into an effluent containing ethylene and an effluent containing water, g) purifying at least a portion of the effluent containing water from 0 and separating at least one flow of treated water and at least one flow of unconverted ethanol, h) recycling at least a portion of the flow of treated water from g) upstream of c).
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6.发明授权Process for the production of alcohols and/or solvents from lignocellulosic biomass with washing of the solid residue obtained after hydrolysis 有权通过洗涤水解后获得的固体残留物从木质纤维素生物质生产醇和/或溶剂的方法公开(公告)号：US09187770B2
公开(公告)日：2015-11-17
申请号：US14197619
申请日：2014-03-05
发明人： Caroline Aymard , Pierre Antoine Bouillon , Stephanie Fleurier , Sylvain Louret , Larissa Perotta , Eszter Toth
IPC分类号： C12P7/16 , C12P19/14 , C12P19/02 , C12P1/00 , C12N1/21 , C12M1/00 , A23K1/06 , A61K35/66 , A61P43/00 , C12P7/10 , C12P7/14 , C12P7/24 , C12P7/62 , C12P7/06 , C07H21/04
CPC分类号： C12P7/14 , C12P7/10 , C12P19/14 , C12P2201/00 , C12P2203/00 , Y02E50/16 , Y02E50/17
摘要： The process for the production of alcohol and/or solvent from a biomass feedstock comprises the stages for pretreatment (P) of the biomass feedstock, for enzymatic hydrolysis (H) of the pretreated substrate, and for fermenting the hydrolyzate (F).To reduce the size of the fermenters, at least a portion of the solid residue contained in the hydrolyzate is extracted (Ex1) in such a way as to obtain a stream of solid residue (9) comprising lignin and a hydrolyzate (8) that is low in solid residue. Then, the stream of solid residue is washed (L) with a liquid stream in such a way as to recover a sugar-enriched liquid stream (15). The sugar-enriched liquid stream (15) is recycled in the enzymatic hydrolysis stage (H) to be able to upgrade the sugars without providing dilution of the streams in the process.
摘要翻译： 从生物质原料生产醇和/或溶剂的方法包括生物质原料的预处理（P），预处理底物的酶水解（H）和发酵水解产物（F）的阶段。 为了减小发酵罐的尺寸，提取水解产物中含有的至少一部分固体残余物（Ex1），以获得包含木质素和水解产物（8）的固体残余物（9），即 固体残渣少。 然后，用液体流洗涤固体残余物流（L），以回收富含糖的液体流（15）。 富含糖的液体流（15）在酶水解阶段（H）中再循环，以便能够在不提供该过程中的流的稀释的情况下升级糖。
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公开(公告)号：US09605282B2
公开(公告)日：2017-03-28
申请号：US14772911
申请日：2014-02-06
发明人： Caroline Aymard , Pierre-Antoine Bouillon , Stephanie Fleurier , Sylvain Louret , Larissa Perotta , Eszter Toth
CPC分类号： C12P7/14 , C12P7/10 , C12P2201/00 , C12P2203/00 , Y02E50/16
摘要： The process for the production of alcohol and/or solvent from a biomass feedstock comprises the stages for pretreatment (P) of the biomass feedstock, for enzymatic hydrolysis (H1 and HF), and for fermenting the hydrolyzate (HF). To prevent solids from being sent and to facilitate operating the section for purifying the fermentation products, at least a portion of the solid material in the fermentation wine is extracted (Ex1) to obtain a stream of solid residue (11) comprising lignin and a fermentation wine (12) that is low in solid material. Then, the stream of solid residue is washed (L) with a liquid stream to recover a liquid stream that is enriched with fermentation products (16). The liquid stream that is enriched with fermentation products (16) is recycled in the enzymatic hydrolysis stage (H1) to recover any fermentation product and to increase the overall yield of the process.
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