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    Mid-range vinylidene content, high viscosity polyisobutylene polymers
    1.
    发明授权
    Mid-range vinylidene content, high viscosity polyisobutylene polymers 有权
    中等偏亚乙烯含量，高粘度聚异丁烯聚合物

    公开(公告)号：US09309339B2

    公开(公告)日：2016-04-12

    申请号：US14346860

    申请日：2012-10-10

    Applicant: TPC Group LLC

    Inventor： Sohel K. Shaikh

    IPC: C08F10/10 ,  C08F110/10 ,  C08L23/22 ,  B01J19/18 ,  C08F210/10

    CPC classification number: C08F110/10 ,  B01J19/1837 ,  B01J19/1881 ,  B01J2219/00065 ,  B01J2219/00081 ,  B01J2219/00094 ,  B01J2219/00162 ,  B01J2219/0022 ,  B01J2219/00231 ,  C08F10/10 ,  C08F210/10 ,  C08L23/22 ,  Y02P20/582 ,  C08F2/00 ,  C08F2500/03 ,  C08F2500/17 ,  C08F4/14

    Abstract: A mid-range vinylidene content, high viscosity PIB polymer composition including PIB molecules, wherein a first portion of the PIB molecules have alpha position double bonds and a second portion of the PIB molecules have beta position double bonds, and the first and second portions together include at least 80 mole % of the PIB molecules of the composition. The first portion includes less than 75 mole % of the PIB molecules of the composition. Additionally, no more than 10 mole % of the PIB molecules of the composition have tetra-substituted double bonds, while the composition is further characterized by having a polydispersity of no more than 2.7 and in that the composition has a kinematic viscosity in the range of 3000 cSt to 5000 cSt, a number average molecular weight, Mn, in the range of 2800 Daltons to 4000 Daltons and a ratio of Mn:PDI of greater than 1100.

    Abstract translation: 包含PIB分子的中等范围亚乙烯含量的高粘度PIB聚合物组合物，其中PIB分子的第一部分具有α位双键，并且PIB分子的第二部分具有β位双键，并且第一和第二部分在一起 包括至少80摩尔％的组合物的PIB分子。 第一部分包括少于75摩尔％的组合物的PIB分子。 此外，组合物中不超过10摩尔％的PIB分子具有四取代的双键，而组合物的进一步特征在于多分散性不超过2.7，并且组合物的运动粘度范围为 3000cSt至5000cSt，数均分子量Mn在2800道尔顿至4000道尔顿范围内，Mn：PDI的比例大于1100。

    Polyisobutylene Prepared with Low Diluent Content Reaction Medium
    4.
    发明申请
    Polyisobutylene Prepared with Low Diluent Content Reaction Medium 有权
    用低稀释度反应介质制备聚异丁烯

    公开(公告)号：US20140256891A1

    公开(公告)日：2014-09-11

    申请号：US14347695

    申请日：2012-10-10

    Applicant: TPC Group LLC

    Inventor： Sohel K. Shaikh

    IPC: C08F110/10

    CPC classification number: C08F110/10 ,  Y02P20/582 ,  C08F2500/03 ,  C08F2500/17 ,  C08F2/00 ,  C08F2/01 ,  C08F4/14

    Abstract: A method of making a polyisobutylene polymer in a recirculating loop reactor with one or more reaction tubes in contact with a heat transfer medium includes: (a) providing a feed mixture consisting essentially of polymerizable monomer and catalyst to a residual reactor stream at a feed rate to form a reaction mixture, the reaction mixture containing less than 5% by weight diluent components; (b) recirculating the reaction mixture in the one or more reaction tubes of the loop reactor at a recirculation rate greater than the feed rate utilizing a recirculating pump operating at a pressure differential, delta P, corresponding to a recirculating flow; (c) polymerizing the reaction mixture in the one or more tubes of the loop reactor to convert the feed mixture to polyisobutylene polymer while cooling the one or more tubes of the loop reactor with the heat transfer medium; and (e) withdrawing polyisobutylene polymer from the loop reactor.

    Abstract translation: 在具有与传热介质接触的一个或多个反应管的再循环回路反应器中制备聚异丁烯聚合物的方法包括：（a）以进料速率将主要由可聚合单体和催化剂组成的进料混合物提供给残余反应器流 形成反应混合物，该反应混合物含有少于5重量％的稀释剂组分; （b）使用在对应于循环流动的压力差ΔP工作的循环泵将循环反应器的一个或多个反应管中的反应混合物以大于进料速率的循环速率循环; （c）在环流反应器的一个或多个管中聚合反应混合物以将进料混合物转化为聚异丁烯聚合物，同时用传热介质冷却环流反应器的一个或多个管; 和（e）从环管反应器中取出聚异丁烯聚合物。

    Mid-Range Vinylidene Content, High Viscosity Polyisobutylene Polymers
    5.
    发明申请
    Mid-Range Vinylidene Content, High Viscosity Polyisobutylene Polymers 有权
    中等偏亚乙烯含量，高粘度聚异丁烯聚合物

    公开(公告)号：US20140235810A1

    公开(公告)日：2014-08-21

    申请号：US14346860

    申请日：2012-10-10

    Applicant: TPC Group LLC

    Inventor： Sohel K. Shaikh

    IPC: C08F110/10

    CPC classification number: C08F110/10 ,  B01J19/1837 ,  B01J19/1881 ,  B01J2219/00065 ,  B01J2219/00081 ,  B01J2219/00094 ,  B01J2219/00162 ,  B01J2219/0022 ,  B01J2219/00231 ,  C08F10/10 ,  C08F210/10 ,  C08L23/22 ,  Y02P20/582 ,  C08F2/00 ,  C08F2500/03 ,  C08F2500/17 ,  C08F4/14

    Abstract: A mid-range vinylidene content, high viscosity PIB polymer composition including PIB molecules, wherein a first portion of the PIB molecules have alpha position double bonds and a second portion of the PIB molecules have beta position double bonds, and the first and second portions together include at least 80 mole % of the PIB molecules of the composition. The first portion includes less than 75 mole % of the PIB molecules of the composition. Additionally, no more than 10 mole % of the PIB molecules of the composition have tetra-substituted double bonds, while the composition is further characterized by having a polydispersity of no more than 2.7 and in that the composition has a kinematic viscosity in the range of 3000 cSt to 5000 cSt, a number average molecular weight, Mn, in the range of 2800 Daltons to 4000 Daltons and a ratio of Mn:PDI of greater than 1100.

    Abstract translation: 包含PIB分子的中等范围亚乙烯含量的高粘度PIB聚合物组合物，其中PIB分子的第一部分具有α位双键，并且PIB分子的第二部分具有β位双键，并且第一和第二部分在一起 包括至少80摩尔％的组合物的PIB分子。 第一部分包括少于75摩尔％的组合物的PIB分子。 此外，组合物中不超过10摩尔％的PIB分子具有四取代的双键，而组合物的进一步特征在于多分散性不超过2.7，并且组合物的运动粘度范围为 3000cSt至5000cSt，数均分子量Mn在2800道尔顿至4000道尔顿范围内，Mn：PDI的比例大于1100。

    Polyisobutylene prepared with low diluent content reaction medium
    8.
    发明授权
    Polyisobutylene prepared with low diluent content reaction medium 有权
    聚异丁烯用低稀释剂制备反应介质

    公开(公告)号：US09074026B2

    公开(公告)日：2015-07-07

    申请号：US14347695

    申请日：2012-10-10

    Applicant: TPC Group LLC

    Inventor： Sohel K. Shaikh

    IPC: C08F2/00 ,  C08F2/02 ,  C08F2/14 ,  C08F110/10

    CPC classification number: C08F110/10 ,  Y02P20/582 ,  C08F2500/03 ,  C08F2500/17 ,  C08F2/00 ,  C08F2/01 ,  C08F4/14

    Abstract: A method of making a polyisobutylene polymer in a recirculating loop reactor with one or more reaction tubes in contact with a heat transfer medium includes: (a) providing a feed mixture consisting essentially of polymerizable monomer and catalyst to a residual reactor stream at a feed rate to form a reaction mixture, the reaction mixture containing less than 5% by weight diluent components; (b) recirculating the reaction mixture in the one or more reaction tubes of the loop reactor at a recirculation rate greater than the feed rate utilizing a recirculating pump operating at a pressure differential, delta P, corresponding to a recirculating flow; (c) polymerizing the reaction mixture in the one or more tubes of the loop reactor to convert the feed mixture to polyisobutylene polymer while cooling the one or more tubes of the loop reactor with the heat transfer medium; and (e) withdrawing polyisobutylene polymer from the loop reactor.

    Abstract translation: 在具有与传热介质接触的一个或多个反应管的再循环回路反应器中制备聚异丁烯聚合物的方法包括：（a）以进料速率将主要由可聚合单体和催化剂组成的进料混合物提供给残余反应器流 形成反应混合物，该反应混合物含有少于5重量％的稀释剂组分; （b）使用在对应于循环流动的压力差ΔP工作的循环泵将循环反应器的一个或多个反应管中的反应混合物以大于进料速率的循环速率循环; （c）在环流反应器的一个或多个管中聚合反应混合物以将进料混合物转化为聚异丁烯聚合物，同时用传热介质冷却环流反应器的一个或多个管; 和（e）从环管反应器中取出聚异丁烯聚合物。

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