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    Stretched multilayer polypropylene film
    2.
    发明授权
    Stretched multilayer polypropylene film 失效
    拉伸多层聚丙烯薄膜

    公开(公告)号：US4584239A

    公开(公告)日：1986-04-22

    申请号：US753846

    申请日：1985-07-11

    申请人： Masahiro Kakugo ,  Yoshiharu Fukui ,  Kizuku Wakatsuki ,  Seiichiro Ima ,  Junichi Kimura

    发明人： Masahiro Kakugo ,  Yoshiharu Fukui ,  Kizuku Wakatsuki ,  Seiichiro Ima ,  Junichi Kimura

    IPC分类号： B32B27/00 ,  B32B27/32 ,  C09J7/02 ,  C09J123/08 ,  C09J123/14

    CPC分类号： C09J7/0242 ,  B32B27/32 ,  C09J123/0815 ,  C09J123/142 ,  Y10S428/91 ,  Y10T428/2826

    摘要： A stretched multilayer polypropylene film is described, comprising a stretched crystalline polypropylene layer and a layer of a composition (Composition B) laminated on at least one side of said polypropylene layer, wherein the composition B comprises a homo- or copolymer composed mainly of ethylene, propylene or butene-1 and having a melting point of 150.degree. C. or less, and a vinylcycloalkane polymer in an amount of 0.05 wt ppm to 10 wt % calculated as a vinylcycloalkane unit. This multilayer film is greatly improved in optical properties such as excellent see-through properties without deteriorating its good heat sealability. Thus it is very useful for wrapping.

    摘要翻译： 描述了拉伸的多层聚丙烯薄膜，其包含拉伸的结晶聚丙烯层和层压在所述聚丙烯层的至少一侧上的组合物层（组合物B），其中组合物B包含主要由乙烯组成的均聚物或共聚物， 丙烯或丁烯-1，熔点为150℃以下，乙烯基环烷烃聚合物的量为0.05重量％〜10重量％，以乙烯基环烷烃单元计算。 这种多层膜在透光性方面优异的光学特性大大提高，而不会使其良好的热封性劣化。 因此，它是非常有用的包装。

    Process for producing propylene block copolymers
    4.
    发明授权
    Process for producing propylene block copolymers 失效
    制备丙烯嵌段共聚物的方法

    公开(公告)号：US4433110A

    公开(公告)日：1984-02-21

    申请号：US255005

    申请日：1981-04-17

    申请人： Kazuo Baba ,  Shyozo Kawamata ,  Yoshiharu Fukui ,  Seiichiro Ima ,  Tatsuya Miyatake

    发明人： Kazuo Baba ,  Shyozo Kawamata ,  Yoshiharu Fukui ,  Seiichiro Ima ,  Tatsuya Miyatake

    IPC分类号： C08F297/08

    CPC分类号： C08F297/08 ,  Y10S526/916

    摘要： A propylene block copolymer produced by polymerizing propylene, ethylene and an .alpha.-olefin having 4 to 8 carbon atoms in two stages with a Zieglar-Natta catalyst by a process which comprises (A) supplying propylene and ethylene in the first stage and propylene and the .alpha.-olefin in the second stage, or (B) supplying propylene and the .alpha.-olefin in the first stage and propylene and ethylene in the second stage, to the polymerization system, wherein the amounts of propylene and ethylene supplied in the first stage of (A) or in the second stage of (B) are 90 to 99 wt % and 10 to 1 wt % based on the total amount of propylene and ethylene supplied in the first stage of (A) or in the second stage of (B), respectively, the amounts of propylene and the .alpha.-olefin supplied in the second stage of (A) or in the first stage of (B) are 60 to 98 wt % and 40 to 2 wt % based on the total amount of propylene and the .alpha.-olefin supplied in the second stage of (A) or in the first stage of (B), respectively, and the amounts of copolymers formed in the first and second stages are 20 to 90 wt % and 80 to 10 wt % based on the final block copolymer, respectively.

    摘要翻译： 通过包括（A）在第一阶段中供应丙烯和乙烯的方法，用齐格列 - 纳塔催化剂将丙烯，乙烯和具有4至8个碳原子的碳原子的α-烯烃分两步制备的丙烯嵌段共聚物，其中丙烯和 第二阶段中的α-烯烃或（B）将第一阶段中的丙烯和α-烯烃和第二阶段中的丙烯和乙烯供应到聚合体系中，其中在第一阶段中供应的丙烯和乙烯的量 （A）或（B）的第二阶段中（A）或（B）的第二阶段中的丙烯和乙烯的总量为90〜99重量％，10〜1重量％ ）在（A）或第（B）的第一阶段中供应的丙烯和α-烯烃的量分别为基于丙烯总量的60至98重量％和40至2重量％ 和在（A）或第一阶段的第二阶段中提供的α-烯烃 （B），第一和第二阶段中形成的共聚物的量分别为最终嵌段共聚物的20〜90重量％和80〜10重量％。

    Process for producing olefin polymers
    7.
    发明授权
    Process for producing olefin polymers 失效
    生产烯烃聚合物的方法

    公开(公告)号：US4364851A

    公开(公告)日：1982-12-21

    申请号：US113668

    申请日：1980-01-21

    申请人： Akinobu Shiga ,  Yoshiharu Fukui ,  Toshio Sasaki ,  Masahisa Okawa ,  Hideaki Matsu-Ura ,  Yasuharu Yamada

    发明人： Akinobu Shiga ,  Yoshiharu Fukui ,  Toshio Sasaki ,  Masahisa Okawa ,  Hideaki Matsu-Ura ,  Yasuharu Yamada

    IPC分类号： C08F4/00 ,  C08F4/60 ,  C08F4/64 ,  C08F10/00

    CPC分类号： C08F10/00

    摘要： A process for producing an olefin polymer by polymerizing an olefin with a catalyst system comprising an organoaluminum compound and a supported catalyst component prepared by using as the carrier a solid product obtained by the reaction of an organomagnesium compound with an aluminum halide compound and/or a silicon halide compound, by heating a liquid ether complex of titanium trichloride in the presence of said carrier, and further reacting the resulting titanium trichloride-containing solid product with titanium tetrachloride. By this process, the olefin polymer having a broad molecular weight distribution suitable for flow molding or extrusion molding is produced.

    摘要翻译： 一种烯烃聚合物的制造方法，其特征在于，将烯烃与含有有机铝化合物和负载型催化剂体系的催化剂体系进行聚合，所述催化剂体系通过使用有机镁化合物与卤化铝化合物和/或 通过在所述载体的存在下加热三氯化钛的液体醚络合物，并进一步使得到的含三氯化钛的固体产物与四氯化钛反应来制备卤化硅化合物。 通过该方法，生产适用于流动成型或挤出成型的具有宽分子量分布的烯烃聚合物。

    Catalysts for the polymerization of olefins
    9.
    发明授权
    Catalysts for the polymerization of olefins 失效
    用于烯烃聚合的催化剂

    公开(公告)号：US4183824A

    公开(公告)日：1980-01-15

    申请号：US885249

    申请日：1978-03-10

    申请人： Akinobu Shiga ,  Yoshiharu Fukui ,  Kazuhiro Matsumura ,  Toshio Sasaki ,  Masahisa Okawa

    发明人： Akinobu Shiga ,  Yoshiharu Fukui ,  Kazuhiro Matsumura ,  Toshio Sasaki ,  Masahisa Okawa

    IPC分类号： C08F4/64 ,  C08F10/00

    CPC分类号： C08F10/00

    摘要： A method for preparing a solid catalyst comprising reacting a titanium trichloride composition with a mixture of(1) an ether compound and carbon atom and represented by the general formula (IV): ##STR1## wherein R.sup.5, R.sup.6 and R.sup.7, which may be the same or different, each has up to 18 carbon atoms and represents an aliphatic hydrocarbon group, which may be straight chain, branched chain or cyclic, or an aromatic hydrocarbon group, with at least one of R.sup.5, R.sup.6 and R.sup.7 being an aromatic hydrocarbon group, with at least one of R.sup.5, R.sup.6 and R.sup.7 being an aromatic hydrocarbon group, the amount of the hydrocarbon compound being about 0.01 to about 10 moles per mole of titanium trichloride in the titanium trichloride composition; and/or(2) (b) an organic sulfur compound represented by the general formulas (VI) and (VIII):R.sup.9 --S--S--R.sup.10 (V)HS--(CH.sub.2).sub.d --SH (VI)wherein each of R.sup.9 and R.sup.10 has up to 18 carbon atoms and represents an aliphatic hydrocarbon group, which may be straight chain, branched chain or cyclic, or an aromatic hydrocarbon group, where R.sup.9 and R.sup.10 may be the same or different; and d is an integer of 2 to 8, the amounts of the organic sulfur compounds represented by the formulas of (VI) and (VII) being about 0.05 to about 1.0 mole and about 0.001 to about 0.2 mole per mole of titanium trichloride in the titanium trichloride composition, respectively.The catalyst, in combination with organoaluminum compounds as activators, being useful to polymerize olefins for the efficient production of highly crystalline olefin polymers.

    摘要翻译： 一种制备固体催化剂的方法，包括使三氯化钛组合物与（1）醚化合物和碳原子并由通式（IV）表示的混合物反应：其中R5，R6和R7，其中R5，R6和R7， 可以相同或不同，各自具有多达18个碳原子，并且表示脂族烃基，其可以是直链，支链或环状或芳族烃基，其中R 5，R 6和R 7中的至少一个为 芳族烃基，其中R 5，R 6和R 7中的至少一个是芳族烃基，在三氯化钛组合物中，烃化合物的量为每摩尔三氯化钛约0.01至约10摩尔; 和/或（2）（b）由通式（VI）和（VIII）表示的有机硫化合物：R9-SS-R10（V）HS-（CH2）d-SH（VI）其中R9和 R 10具有多达18个碳原子，并且表示脂肪族烃基，其可以是直链，支链或环状或芳族烃基，其中R 9和R 10可以相同或不同; d为2-8的整数，由式（VI）和（VII）表示的有机硫化合物的量为每摩尔三氯化钛约0.05至约1.0摩尔和约0.001至约0.2摩尔 三氯化钛组成。 催化剂与有机铝化合物作为活化剂的组合可用于聚合烯烃以有效生产高度结晶的烯烃聚合物。

    Inorganic filler containing polyolefin composition
    10.
    发明授权
    Inorganic filler containing polyolefin composition 失效

    公开(公告)号：US5086100A

    公开(公告)日：1992-02-04

    申请号：US606936

    申请日：1990-10-31

    申请人： Yoshiharu Fukui ,  Kazuhisa Kuroda

    发明人： Yoshiharu Fukui ,  Kazuhisa Kuroda

    IPC分类号： C08K5/1575 ,  C08K5/20

    CPC分类号： C08K5/1575 ,  C08K5/20

    摘要： An inorganic filler-containing polyolefin composition which comprises100 parts by weight of a polyolefin,1-100 parts by weight of an inorganic filler.0.01-1.0 part by weight of a phenolic antioxidant represented by the general formula (I) shown below, andat least one compound selected from the group consisting of the compounds represented by the general formulas (II) to (IV) shown below, and optionally 0.01-1.0 part by weight of a sulfur antioxidant and/or 0.01-2.0 parts by weight of a light stabilizer. ##STR1## wherein R.sub.1 represents an alkyl group of 1-3 carbon atoms,R.sub.2 --CO--NH--(CH.sub.2).sub.n --HN--CO--R.sub.2 (II) wherein R.sub.2 represents an alkyl group or an alkenyl group of 5-21 carbon atoms, and n is an integer of 1 to 6.R.sub.3 --CONH.sub.2 (III) wherein R.sub.3 represents an alkyl group or an alkenyl group of 5-21 carbon atoms. ##STR2## wherein R.sub.4 represents and alkyl group, an alkenyl group or an acyl group (R'--CO) of 8-18 carbon atoms, m and n are integers which meet m+n-2 to 10, R' represents an aliphatic carbon chain which may be saturated or unsaturated, and R.sub.5 represents an alkyl group or an alkenyl group of 7-17 carbon atoms.Excellent thermal-oxidation stability and/or light stability are obtained.