Process for synthesis of N,N-disubstituted hydrazone
    1.
    发明授权
    Process for synthesis of N,N-disubstituted hydrazone 失效
    合成N,N-二取代腙的方法

    公开(公告)号:US4990625A

    公开(公告)日:1991-02-05

    申请号:US445930

    申请日:1989-12-05

    摘要: A process for synthesizing an N,N-disubstituted hydrazone comprises carrying out nitrozation by adding an aqueous solution of sodium nitrite to a solution having one part by weight of an N,N-disubstituted amine dissolved in 3 to 30 parts by weight of an organic acid, then reducing the nitrozated product to an N,N-disubstituted hydrazine by adding a reducing agent to the mixture containing the nitrozated product, and thereafter adding to the mixture containing the N,N-disubstituted hydrazine a carbonyl compound of the formula: ##STR1## wherein A represents an aromatic hydrocarbon group or an aromatic heterocyclic group which may have a substituent, B represents a hydrogen atom, an alkyl group, an aryl group or an aromatic heterocyclic group, which may have a substituent, thereby performing condensation of the N,N-disubstituted hydrazine with the carbonyl compound.

    摘要翻译: 合成N,N-二取代腙的方法包括通过将亚硝酸钠水溶液加入到溶解有3重量份的N,N-二取代胺的溶液中进行硝化,所述N,N-二取代胺溶解在3-30重量份的有机 然后通过向含有硝基化产物的混合物中加入还原剂将硝化产物还原成N,N-二取代的肼,然后向含有N,N-二取代肼的混合物中加入下式的羰基化合物: 其中A表示可以具有取代基的芳香族烃基或芳香族杂环基,B表示可以具有取代基的氢原子,烷基,芳基或芳香族杂环基,由此进行 N,N-二取代肼与羰基化合物。

    Recording medium and process employing a photosensitive organic film
    2.
    发明授权
    Recording medium and process employing a photosensitive organic film 失效
    记录介质和采用光敏有机膜的工艺

    公开(公告)号:US4501808A

    公开(公告)日:1985-02-26

    申请号:US526533

    申请日:1983-08-25

    摘要: An organic film comprising at least one compound of the following formulae (1)-(5): ##STR1## wherein R.sub.11 and R.sub.13 each represent substituted or unsubstituted aryl, R.sub.12 represents substituted or unsubstituted arylene, and A.sup..crclbar. represents an anionic residue; ##STR2## wherein R.sub.21, R.sub.22, and R.sub.24 each represent substituted or unsubstituted aryl, R.sub.23 represents substituted or unsubstituted arylene, and A.sup..crclbar. represents an anionic residue; ##STR3## wherein R.sub.31, R.sub.33, and R.sub.35 each represent substituted or unsubstituted aryl, R.sub.32 and R.sub.34 each represent substituted or unsubstituted arylene, and A.sup..crclbar. represents an anionic residue; ##STR4## wherein R.sub.41 represents alkyl, substituted or unsubstituted phenyl, or substituted or unsubstituted styryl, R.sub.42 represents substituted or unsubstituted arylene, R.sub.43 represents substituted or unsubstituted aryl, and A.sup..crclbar. represents an anionic residue; and ##STR5## wherein R.sub.51 represents alkoxy, R.sub.52 represents alkyl, R.sub.53 represents substituted or unsubstituted arylene, R.sub.54 represents substituted or unsubstituted aryl, A.sup..crclbar. represents an anionic residue, and n represents an integer of 1 or 2.

    摘要翻译: 包含至少一种下式(1) - (5)的化合物的有机膜:其中R11和R13各自表示取代或未取代的芳基,R12表示取代或未取代的亚芳基,A( - )表示 阴离子残基; (2)其中R21,R22和R24各自表示取代或未取代的芳基,R23表示取代或未取代的亚芳基,A( - )表示阴离子残基; (3)其中R 31,R 33和R 35各自表示取代或未取代的芳基,R 32和R 34各自表示取代或未取代的亚芳基,A( - )表示阴离子残基; (4)其中R41表示烷基,取代或未取代的苯基或取代或未取代的苯乙烯基,R42表示取代或未取代的亚芳基,R43表示取代或未取代的芳基,A( - )表示阴离子残基; (5)其中R51表示烷氧基,R52表示烷基,R53表示取代或未取代的亚芳基,R54表示取代或未取代的芳基,A( - )表示阴离子残基,n表示1或2的整数。

    Roller for fixing and image fixing apparatus using roller for fixing
    6.
    发明授权
    Roller for fixing and image fixing apparatus using roller for fixing 有权
    用于固定的辊和用于固定的辊的图像定影装置

    公开(公告)号:US08208844B2

    公开(公告)日:2012-06-26

    申请号:US12437913

    申请日:2009-05-08

    IPC分类号: G03G15/20

    摘要: A fixing roller of an image fixing apparatus has an elastic layer on a core metal and has a thermal conductive fluororubber latex layer containing a mixture of fluororubber, fluororesin and thermal conductive fillers more outer side than the elastic. An intermediate layer made of silicone rubber having higher thermal conductivity than the thermal conductive fluororubber latex layer is provided between the thermal conductive fluororubber latex layer and the elastic layer, and the intermediate layer is configured so that an elastic parameter Y(=H×T) satisfies a relational expression: Y≧4200 where H (degree) is Asker-C hardness of the silicone rubber having higher thermal conductivity (500 g load) and T (μm) is a thickness of the silicone rubber having higher thermal conductivity.

    摘要翻译: 图像定影装置的定影辊在芯金属上具有弹性层,并且具有包含比弹性体更外侧的氟橡胶,氟树脂和导热填料的混合物的导热氟橡胶胶乳层。 在导热性氟橡胶胶乳层和弹性层之间设置由热导率高于导热性氟橡胶胶乳层的硅橡胶制成的中间层,中间层构成为弹性参数Y(= H×T) 满足关系式:Y≥4200其中H(度)是具有较高导热性(500g负载)的硅橡胶的Asker-C硬度,T(μm)是具有较高导热率的硅橡胶的厚度。

    Coloring compound and recording material using the same
    7.
    发明授权
    Coloring compound and recording material using the same 有权
    着色化合物和使用其的记录材料

    公开(公告)号:US07598012B2

    公开(公告)日:2009-10-06

    申请号:US10548372

    申请日:2004-05-14

    IPC分类号: C07D211/46 G03G9/09

    CPC分类号: C09B11/22

    摘要: Disclosed herein are a coloring compound represented by the general formula: A-L1-X-L2-B  (1) wherein A is a coloring moiety, B is a stabilizing moiety having fading-preventing ability, L1 and L2 are linkers for linking A, X and B by covalent bonding and denote, independently of each other, any group of —O—,—CO—, —OCO—, —NR1— (in which R1 is a group selected from hydrogen, alkyl, aryl and aralkyl groups), —NHCO—, —NHCOO—, —NHCONH—, —NHCSNH—, —SO—, —SO2—, —SO2NH—, —S—, —SS— and —CH2—, with the proviso that L1 and L2 are not —CH2— at the same time, and X is a spacer moiety and denotes any group of an alkylene group having 1 to 10 carbon atoms, an alkenylene group having 2 to 10 carbon atoms, an alkynylene group having 2 to 10 carbon atoms, an alkoxyalkylene group having 1 to 10 carbon atoms, a cycloalkylene group having 5 to 7 carbon atoms, an arylene group having 6 to 10 carbon atoms and a pyranose type saccharide having 1 to 7 saccharide units, and a recording material using the coloring compound as a coloring material.

    摘要翻译: 本文公开的是由以下通式表示的着色化合物:<?in-line-formula description =“In-line Formulas”end =“lead”?> A-L1-X-L2-B(1) line-formula description =“In-line Formulas”end =“tail”?>其中A是着色部分,B是具有防褪色能力的稳定部分,L1和L2是通过共价键连接A,X和B的接头 键合并且彼此独立地表示-O - , - CO-,-OCO-,-NR1-(其中R 1是选自氢,烷基,芳基和芳烷基的基团),-NHCO-, -NHCOO - , - NHCONH-, - NHCSN - , - SO - , - SO 2 - , - SO 2 NH-, - S - , - S - 和-CH 2 - ,条件是在该位置上L1和L2不是-CH2- X是间隔部分,表示碳原子数1〜10的亚烷基,碳原子数2〜10的亚烯基,碳原子数2〜10的亚炔基,碳原子数1〜10的烷氧基亚烷基 10个碳原子,具有5至7个碳原子的亚环烷基,亚芳基具有6个 至10个碳原子的吡喃糖型糖和具有1至7个糖单元的吡喃糖型糖,以及使用着色化合物作为着色材料的记录材料。