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公开(公告)号：US4180466A
公开(公告)日：1979-12-25
申请号：US489216
申请日：1974-07-17
申请人： Thomas D. Newingham , Alexander D. Recchuite , John Q. Griffith, III , Marcus W. Haseltine, Jr.
发明人： Thomas D. Newingham , Alexander D. Recchuite , John Q. Griffith, III , Marcus W. Haseltine, Jr.
IPC分类号： C07F9/02 , C10M135/02 , C10M169/04 , C10M171/00 , C10M1/38 , C07G17/00
CPC分类号： C10M171/002 , C07F9/02 , C10M135/02 , C10M169/044 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10M2203/06 , C10M2203/065 , C10M2203/10 , C10M2203/1006 , C10M2203/102 , C10M2203/1025 , C10M2203/104 , C10M2203/1045 , C10M2203/106 , C10M2203/1065 , C10M2203/108 , C10M2203/1085 , C10M2205/00 , C10M2205/02 , C10M2205/0206 , C10M2205/024 , C10M2205/026 , C10M2205/028 , C10M2205/04 , C10M2207/024 , C10M2211/02 , C10M2219/02 , C10M2219/022 , C10M2219/024 , C10M2219/046 , C10M2221/041 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2223/045 , C10M2223/065 , C10M2223/12 , C10M2225/04 , C10M2225/041 , C10N2210/02 , C10N2240/00 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： An improved method of lubrication of a controlled-slip differential comprises using a lubricant comprising major amounts of a hydrocarbon base stock and friction improving amounts of synthetic sulfurized oil consisting essentially of a cosulfurized blend of a triglyceride and a C.sub.2 -C.sub.128 monoolefin. The hydrocarbon base stock can have a kinematic viscosity at 210.degree. F. in the range of 1.5 to 200.0 cs. and contain paraffinic (by VGC) petroleum oil or a blend of at least one C.sub.13 -C.sub.29 naphthene and from 0.1 to 20 parts by weight, based on said naphthene of at least one member from at least one of the following groups (a), (b), (c) and (d):(a) a synthetic liquid C.sub.3 -C.sub.8 olefin homopolymer, copolymer or terpolymer;(b) a member from group (a) above which is at least partially hydrogenated;(c) a severely hydrorefined naphthenic mineral oil lube containing less than 1 percent of gel aromatic hydrocarbons; and(d) a severely hydrorefined paraffinic mineral oil lube containing less than 1 percent of gel aromatic hydrocarbons.
摘要翻译： 一种改进的控制滑差差润滑方法包括使用包含主要量的烃基原料的润滑剂和基本上由甘油三酯和C2-C128单烯烃的共硫化共混物组成的合成硫化油的摩擦改进量。 烃基料可以在210°F的运动粘度范围为1.5至200.0cs。 并且含有链烷烃（通过VGC）石油油或至少一种C13-C29环烷烃的共混物和0.1至20重量份，基于所述环烷烃至少一种成员，所述组分至少一种（a）， （b），（c）和（d）：（a）合成液体C3-C8烯烃均聚物，共聚物或三元共聚物; （b）上述（a）组成员至少部分氢化; （c）含有少于1％凝胶芳烃的严重加氢精制环烷矿物油润滑油; 和（d）含有少于1％凝胶芳烃的严重加氢精制石蜡矿物油润滑剂。
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公开(公告)号：US4009117A
公开(公告)日：1977-02-22
申请号：US628853
申请日：1975-11-05
CPC分类号： B01F5/20 , B01F3/0811 , B01F3/0869 , B01F5/10
摘要： A simplified procedure for making a water-in-oil emulsion involving passing the water and oil through an open face centrifugal pump, passing the pump effluent through a nozzle, and repeating these two steps until an emulsion is formed.
摘要翻译： 一种制造油包水乳液的简化程序，包括使水和油通过开口离心泵，使泵流出物通过喷嘴，并重复这两个步骤，直至形成乳液。
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公开(公告)号：US4456540A
公开(公告)日：1984-06-26
申请号：US319528
申请日：1981-11-09
IPC分类号： C07F9/02 , C10M171/00 , C10M1/38 , C10M3/32
CPC分类号： C07F9/02 , C10M1/08 , C10M171/002 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10M2203/06 , C10M2203/10 , C10M2203/102 , C10M2203/104 , C10M2203/106 , C10M2203/108 , C10M2205/00 , C10M2205/02 , C10M2205/024 , C10M2205/026 , C10M2205/028 , C10M2205/04 , C10M2207/024 , C10M2211/02 , C10M2219/02 , C10M2219/022 , C10M2219/024 , C10M2219/046 , C10M2221/041 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2223/045 , C10M2223/065 , C10M2223/12 , C10N2210/02 , C10N2240/00 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： Process of sulfurizing a blend of 90 to 50 and preferably 88 to 70 parts by volume of triglyceride such as lard oil and 10 to 50 and preferably 12 to 30 parts by volume of an ethylenically unsaturated hydrocarbon containing 2 to 24 carbon atoms. The sulfurization is carried out using elemental sulfur. Simultaneous sulfurization and chlorination may be effected by reacting with sulfur monochloride. Phosphosulfurization may also be carried out by addition of small amounts of a phosphorus sulfide to the sulfurized blend followed by heating at 180.degree. F. to 250.degree. F. for from 30 minutes to 10 hours to effect phosphosulfurization. The sulfurization or phosphosulfurization involves reacting at from 330.degree. F. to 445.degree. F. for 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours to remove hydrogen sulfide. The simultaneous sulfurization and chlorination reaction is carried out at from 90.degree. F. to 280.degree. F. for from 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours. The sulfurized oils contain from 7.5 to 25 weight percent sulfur as based on the blend of olefin and triglyceride.
摘要翻译： 将90至50体积％，优选88至70体积份的甘油三酯如猪油和10至50体积％，优选12至30体积份含有2至24个碳原子的烯键式不饱和烃的共混物硫化的方法。 硫化使用元素硫进行。 同时硫化和氯化可以通过与一氯化硫反应来实现。 磷硫化也可以通过向硫化混合物中加入少量硫化磷，然后在180°F加热至250°F进行30分钟至10小时进行磷硫化。 硫化或磷硫化包括在330°F至445°F下反应20分钟至10小时，然后用125°F至250°F的气体吹扫30分钟至20小时以除去硫化氢 。 同步硫化和氯化反应在90°F至280°F进行20分钟至10小时，随后用125°F至250°F的气体吹扫30分钟至20小时 。 基于烯烃和甘油三酯的共混物，硫化油含有7.5至25重量％的硫。
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公开(公告)号：US4481140A
公开(公告)日：1984-11-06
申请号：US220399
申请日：1972-01-24
IPC分类号： C07F9/02 , C07G99/00 , C10M135/02 , C10M159/12 , C10M171/00 , C09B49/00 , C10M1/38 , C10M3/32
CPC分类号： C07G17/002 , C07F9/02 , C10M135/02 , C10M159/123 , C10M171/002 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10M2203/06 , C10M2203/065 , C10M2203/10 , C10M2203/1006 , C10M2203/102 , C10M2203/1025 , C10M2203/104 , C10M2203/1045 , C10M2203/106 , C10M2203/1065 , C10M2203/108 , C10M2203/1085 , C10M2205/00 , C10M2205/02 , C10M2205/0206 , C10M2205/024 , C10M2205/026 , C10M2205/028 , C10M2205/04 , C10M2207/024 , C10M2211/02 , C10M2219/02 , C10M2219/022 , C10M2219/024 , C10M2219/046 , C10M2221/041 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2223/045 , C10M2223/065 , C10M2223/12 , C10M2225/04 , C10M2225/041 , C10N2210/02 , C10N2240/00 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： Process of sulfurizing a blend of 90 to 50 and preferably 88 to 70 parts by volume of triglyceride such as lard oil and 10 to 50 and preferably 12 to 30 parts by volume of an ethylenically unsaturated hydrocarbon containing 2 to 24 carbon atoms. The sulfurization is carried out using elemental sulfur. Simultaneous sulfurization and chlorination may be effected by reacting with sulfur monochloride. Phosphosulfurization may also be carried out by addition of small amounts of a phosphorus sulfide to the sulfurized blend followed by heating at 180.degree. F. to 250.degree. F. for from 30 minutes to 10 hours to effect phosphosulfurization. The sulfurization or phosphosulfurization involves reacting at from 330.degree. F. to 445.degree. F. for 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours to remove hydrogen sulfide. The simultaneous sulfuriztion and chlorination reaction is carried out from 90.degree. F. to 280.degree. F. for from 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours. The sulfurized oils contain from 7.5 to 25 weight percent sulfur as based on the blend of olefin and triglyceride.
摘要翻译： 将90至50体积％，优选88至70体积份的甘油三酯如猪油和10至50体积％，优选12至30体积份含有2至24个碳原子的烯键式不饱和烃的共混物硫化的方法。 硫化使用元素硫进行。 同时硫化和氯化可以通过与一氯化硫反应来实现。 磷硫化也可以通过向硫化混合物中加入少量硫化磷，然后在180°F加热至250°F进行30分钟至10小时进行磷硫化。 硫化或磷硫化包括在330°F至445°F下反应20分钟至10小时，然后用125°F至250°F的气体吹扫30分钟至20小时以除去硫化氢 。 同时硫化和氯化反应在90°F至280°F进行20分钟至10小时，然后用125°F至250°F的气体吹扫30分钟至20小时。 基于烯烃和甘油三酯的共混物，硫化油含有7.5至25重量％的硫。
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公开(公告)号：US4321153A
公开(公告)日：1982-03-23
申请号：US49864
申请日：1979-06-18
IPC分类号： C07F9/02 , C07G99/00 , C10M135/02 , C10M171/00 , C10M1/38 , C10M3/32
CPC分类号： C07G17/002 , C07F9/02 , C10M135/02 , C10M171/002 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10M2203/06 , C10M2203/10 , C10M2203/102 , C10M2203/104 , C10M2203/106 , C10M2203/108 , C10M2205/00 , C10M2205/02 , C10M2205/024 , C10M2205/026 , C10M2205/028 , C10M2205/04 , C10M2207/024 , C10M2211/02 , C10M2219/02 , C10M2219/022 , C10M2219/024 , C10M2219/046 , C10M2221/041 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2223/045 , C10M2223/065 , C10M2223/12 , C10N2210/02 , C10N2240/00 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： Process of sulfurizing a blend of 90 to 50 and preferably 88 to 70 parts by volume of triglyceride such as lard oil and 10 to 50 and preferably 12 to 30 parts by volume of an ethylenically unsaturated hydrocarbon containing 2 to 24 carbon atoms. The sulfurization is carried out using elemental sulfur. Simultaneous sulfurization and chlorination may be effected by reacting with sulfur monochloride. Phosphosulfurization may also be carried out by addition of small amounts of a phosphorus sulfide to the sulfurized blend followed by heating at 180.degree. F. to 250.degree. F. for from 30 minutes to 10 hours to effect phosphosulfurization. The sulfurization or phosphosulfurization involves reacting at from 330.degree. F. to 445.degree. F. for 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours to remove hydrogen sulfide. The simultaneous sulfurization and chlorination reaction is carried out at from 90.degree. F. to 280.degree. F. for from 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours. The sulfurized oils contain from 7.5 to 25 weight percent sulfur as based on the blend of olefin and triglyceride.
摘要翻译： 将90至50体积％，优选88至70体积份的甘油三酯如猪油和10至50体积％，优选12至30体积份含有2至24个碳原子的烯键式不饱和烃的共混物硫化的方法。 硫化使用元素硫进行。 同时硫化和氯化可以通过与一氯化硫反应来实现。 磷硫化也可以通过向硫化混合物中加入少量硫化磷，然后在180°F加热至250°F进行30分钟至10小时进行磷硫化。 硫化或磷硫化包括在330°F至445°F下反应20分钟至10小时，然后用125°F至250°F的气体吹扫30分钟至20小时以除去硫化氢 。 同步硫化和氯化反应在90°F至280°F进行20分钟至10小时，随后用125°F至250°F的气体吹扫30分钟至20小时 。 基于烯烃和甘油三酯的共混物，硫化油含有7.5至25重量％的硫。
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6.发明授权
公开(公告)号：US4166796A
公开(公告)日：1979-09-04
申请号：US905909
申请日：1978-05-15
IPC分类号： C07F9/02 , C07G99/00 , C10M135/02 , C10M171/00 , C10M1/38 , C07G17/00 , C09B49/00 , C10M5/22
CPC分类号： C07G17/002 , C07F9/02 , C10M135/02 , C10M171/002 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10M2203/06 , C10M2203/10 , C10M2203/102 , C10M2203/104 , C10M2203/106 , C10M2203/108 , C10M2205/00 , C10M2205/02 , C10M2205/024 , C10M2205/026 , C10M2205/028 , C10M2205/04 , C10M2207/024 , C10M2211/02 , C10M2219/02 , C10M2219/022 , C10M2219/024 , C10M2219/046 , C10M2221/041 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2223/045 , C10M2223/065 , C10M2223/12 , C10N2210/02 , C10N2240/00 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： Process of sulfurizing a blend of 90 to 50 and preferably 88 to 70 parts by volume of triglyceride such as lard oil and 10 to 50 and preferably 12 to 30 parts by volume of an ethylenically unsaturated hydrocarbon contaning 2 to 24 carbon atoms. The sulfurization is carried out using elemental sulfur. Simultaneous sulfurization and chlorination may be effected by reacting with sulfur monochloride. Phosphosulfurization may also be carried out by addition of small amounts of a phosphorus sulfide to the sulfurized blend followed by heating at 180.degree. F. to 250.degree. F. for from 30 minutes to 10 hours to effect phosphosulfurization. The sulfurization or phosphosulfurization involves reacting at from 330.degree. F. to 445.degree. F. for 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours to remove hydrogen sulfide. The simultaneous sulfurization and chlorination reaction is carried out at from 90.degree. F. to 280.degree. F. for from 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours. The sulfurized oils contain from 7.5 to 25 weight percent sulfur as based on the blend of olefin and triglyceride.
摘要翻译： 将90至50体积％，优选88至70体积份的甘油三酯如猪油和10至50份，优选12至30份体积的含有2至24个碳原子的烯属不饱和烃的共混物硫化的方法。 硫化使用元素硫进行。 同时硫化和氯化可以通过与一氯化硫反应来实现。 磷硫化也可以通过向硫化混合物中加入少量硫化磷，然后在180°F加热至250°F进行30分钟至10小时进行磷硫化。 硫化或磷硫化包括在330°F至445°F下反应20分钟至10小时，然后用125°F至250°F的气体吹扫30分钟至20小时以除去硫化氢 。 同步硫化和氯化反应在90°F至280°F进行20分钟至10小时，随后用125°F至250°F的气体吹扫30分钟至20小时 。 基于烯烃和甘油三酯的共混物，硫化油含有7.5至25重量％的硫。
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公开(公告)号：US4487705A
公开(公告)日：1984-12-11
申请号：US397473
申请日：1973-09-14
IPC分类号： C07F9/02 , C07G99/00 , C10M135/02 , C10M159/12 , C10M171/00 , C10M1/48 , C10M1/38
CPC分类号： C07G17/002 , C07F9/02 , C10M135/02 , C10M159/123 , C10M171/002 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10M2203/06 , C10M2203/065 , C10M2203/10 , C10M2203/1006 , C10M2203/102 , C10M2203/1025 , C10M2203/104 , C10M2203/1045 , C10M2203/106 , C10M2203/1065 , C10M2203/108 , C10M2203/1085 , C10M2205/00 , C10M2205/02 , C10M2205/0206 , C10M2205/024 , C10M2205/026 , C10M2205/028 , C10M2205/04 , C10M2207/024 , C10M2211/02 , C10M2219/02 , C10M2219/022 , C10M2219/024 , C10M2219/046 , C10M2221/041 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2223/045 , C10M2223/065 , C10M2223/12 , C10M2225/04 , C10M2225/041 , C10N2210/02 , C10N2240/00 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： Process of sulfurizing a blend of 90 to 50 and preferably 88 to 70 parts by volume of triglyceride such as lard oil and 10 to 50 and preferably 12 to 30 parts by volume of an ethylenically unsaturated hydrocarbon containing 2 to 24 carbon atoms. The sulfurization is carried out using elemental sulfur. Simultaneous sulfurization and chlorination may be effected by reacting with sulfur monochloride. Phosphosulfurization may also be carried out by addition of small amounts of a phosphorus sulfide to the sulfurized blend followed by heating at 180.degree. F. to 250.degree. F. for from 30 minutes to 10 hours to effect phosphosulfurization. The sulfurization or phosphosulfurization involves reacting at from 330.degree. F. to 445.degree. F. for 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours to remove hydrogen sulfide. The simultaneous sulfurization and chlorination reaction is carried out at from 90.degree. F. to 280.degree. F. for from 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours. The sulfurized oils contain from 7.5 to 25 weight percent sulfur as based on the blend of olefin and triglyceride.
摘要翻译： 将90至50体积％，优选88至70体积份的甘油三酯如猪油和10至50体积％，优选12至30体积份含有2至24个碳原子的烯键式不饱和烃的共混物硫化的方法。 硫化使用元素硫进行。 同时硫化和氯化可以通过与一氯化硫反应来实现。 磷硫化也可以通过向硫化混合物中加入少量硫化磷，然后在180°F加热至250°F进行30分钟至10小时进行磷硫化。 硫化或磷硫化包括在330°F至445°F下反应20分钟至10小时，然后用125°F至250°F的气体吹扫30分钟至20小时以除去硫化氢 。 同步硫化和氯化反应在90°F至280°F进行20分钟至10小时，随后用125°F至250°F的气体吹扫30分钟至20小时 。 基于烯烃和甘油三酯的共混物，硫化油含有7.5至25重量％的硫。
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公开(公告)号：US4166797A
公开(公告)日：1979-09-04
申请号：US905910
申请日：1978-05-15
IPC分类号： C10M135/02 , C10M1/38 , C10M3/32 , C10M5/22 , C10M7/36
CPC分类号： C10M135/02 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10M2203/06 , C10M2203/10 , C10M2203/102 , C10M2203/104 , C10M2203/106 , C10M2203/108 , C10M2205/00 , C10M2205/02 , C10M2205/024 , C10M2205/026 , C10M2205/028 , C10M2205/04 , C10M2207/024 , C10M2211/02 , C10M2219/02 , C10M2219/022 , C10M2219/024 , C10M2219/046 , C10M2221/041 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2223/045 , C10M2223/065 , C10M2223/12 , C10N2210/02 , C10N2240/00 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： Process of sulfurizing a blend of 90 to 50 and preferably 88 to 70 parts by volume of triglyceride such as lard oil and 10 to 50 and preferably 12 to 30 parts by volume of an ethylenically unsaturated hydrocarbon containing 2 to 24 carbon atoms. The sulfurization is carried out using elemental sulfur. Simultaneous sulfurization and chlorination may be effected by reacting with sulfur monochloride. Phosphosulfurization may also be carried out by addition of small amounts of a phosphorus sulfide to the sulfurized blend followed by heating at 180.degree. F. to 250.degree. F. for from 30 minutes to 10 hours to effect phosphosulfurization. The sulfurization or phosphosulfurization involves reacting at from 350.degree. F. to 445.degree. F. for 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours to remove hydrogen sulfide. The simultaneous sulfurization and chlorination reaction is carried out at from 90.degree. F. to 280.degree. F. for from 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. for 30 minutes to 20 hours. The sulfurized oils contain from 7.5 to 25 weight percent sulfur as based on the blend of olefin and triglyceride.
摘要翻译： 将90至50体积％，优选88至70体积份的甘油三酯如猪油和10至50体积％，优选12至30体积份含有2至24个碳原子的烯键式不饱和烃的共混物硫化的方法。 硫化使用元素硫进行。 同时硫化和氯化可以通过与一氯化硫反应来实现。 磷硫化也可以通过向硫化混合物中加入少量硫化磷，然后在180°F加热至250°F进行30分钟至10小时进行磷硫化。 硫化或磷硫化包括在350°F至445°F下反应20分钟至10小时，然后用125°F至250°F的气体吹扫30分钟至20小时以除去硫化氢 。 同步硫化和氯化反应在90°F至280°F进行20分钟至10小时，随后在125°F吹入气体30分钟至20小时。 基于烯烃和甘油三酯的共混物，硫化油含有7.5至25重量％的硫。
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公开(公告)号：US4166795A
公开(公告)日：1979-09-04
申请号：US137556
申请日：1971-04-26
IPC分类号： C07F9/02 , C10M135/02 , C10M159/12 , C10M171/00 , C10M1/38 , C07G17/00 , C10M3/32
CPC分类号： C10M171/002 , C07F9/02 , C10M135/02 , C10M159/12 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10M2203/06 , C10M2203/10 , C10M2203/102 , C10M2203/104 , C10M2203/106 , C10M2203/108 , C10M2205/00 , C10M2205/02 , C10M2205/024 , C10M2205/026 , C10M2205/028 , C10M2205/04 , C10M2211/02 , C10M2219/02 , C10M2219/022 , C10M2219/024 , C10M2219/046 , C10M2221/041 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2223/045 , C10M2223/065 , C10M2223/12 , C10N2210/02 , C10N2240/00 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： A synthetic sulfurized oil, useful as an additive to lubricants, and especially as a replacement for sulfurized sperm oil, is produced by reaction of sulfur, lard oil and polyisobutylene oligimers containing at least one pair of maximally crowded geminal methyl groups (e.g. "tetraisobutylene"). Preferably, sufficient sulfur to obtain a final sulfurized product containing in the range of about 5-25 weight percent sulfur is reacted with a mixture comprising about 30-90 parts by weight of lard oil and 70-10 parts of the polyisobutylene. Minor amounts (e.g. up to about 15 weight percent) of other unsaturated hydrocarbons (e.g. "C.sub.18 olefin") can also be present in the mixture.
摘要翻译： 可用作润滑剂添加剂，特别是作为硫化精油的替代品的合成硫化油是通过硫，猪油和含有至少一对最大拥挤的孪生甲基（例如“四异丁烯”）的聚异丁烯聚合物的反应产生的， ）。 优选地，获得包含约5-25重量％硫的最终硫化产物的足够的硫与包含约30-90重量份的猪油和70-10份聚异丁烯的混合物反应。 混合物中也可存在少量（例如至多约15重量％）的其它不饱和烃（例如“C18烯烃”）。
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