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公开(公告)号：US07772435B2
公开(公告)日：2010-08-10
申请号：US11617416
申请日：2006-12-28
申请人： Thomas Link Guggenheim , Paul Edward Howson , Farid Fouad Khouri , Lioba Maria Kloppenburg , Matthew Hal Littlejohn , Jacob Lee Oberholtzer , Juan Rodriguez Ordonez , Suresh R. Sriram , David Winfield Woodruff
发明人： Thomas Link Guggenheim , Paul Edward Howson , Farid Fouad Khouri , Lioba Maria Kloppenburg , Matthew Hal Littlejohn , Jacob Lee Oberholtzer , Juan Rodriguez Ordonez , Suresh R. Sriram , David Winfield Woodruff
IPC分类号： C07C211/62 , C07C251/02 , C07D211/00 , C07D213/72
CPC分类号： C07C277/08 , C07D209/48 , C07D213/74 , C07C279/04
摘要： Disclosed herein is a method comprising: (a) adding an aqueous solution comprising a quaternary ammonium salt to an organic solvent in a vessel under an inert atmosphere, thereby forming a first mixture comprising the quaternary ammonium salt and the solvent; and (b) mixing the first mixture at a temperature and for a time sufficient to remove water and a portion of the solvent from the first mixture, wherein the mixing is performed in an inert atmosphere and the temperature is less than the decomposition temperature of the quaternary ammonium salt.
摘要翻译： 本文公开了一种方法，包括：（a）在惰性气氛下，将容纳季铵盐的水溶液在容器中加入到有机溶剂中，从而形成包含季铵盐和溶剂的第一混合物; 和（b）将第一混合物在足以从第一混合物中除去水和一部分溶剂的温度和时间下混合，其中混合在惰性气氛中进行，并且温度低于所述第一混合物的分解温度 季铵盐。
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公开(公告)号：US20080161576A1
公开(公告)日：2008-07-03
申请号：US11617416
申请日：2006-12-28
申请人： Thomas Link Guggenheim , Paul Edward Howson , Farid Fouad Khouri , Lioba Maria Kloppenburg , Matthew Hal Littlejohn , Jacob Lee Oberholtzer , Juan Rodriguez Ordonez , Suresh R. Sriram , David Winfield Woodruff
发明人： Thomas Link Guggenheim , Paul Edward Howson , Farid Fouad Khouri , Lioba Maria Kloppenburg , Matthew Hal Littlejohn , Jacob Lee Oberholtzer , Juan Rodriguez Ordonez , Suresh R. Sriram , David Winfield Woodruff
IPC分类号： C07C211/62 , C07C251/02 , C07D211/00 , C07D213/72
CPC分类号： C07C277/08 , C07D209/48 , C07D213/74 , C07C279/04
摘要： Disclosed herein is a method comprising: (a) adding an aqueous solution comprising a quaternary ammonium salt to an organic solvent in a vessel under an inert atmosphere, thereby forming a first mixture comprising the quaternary ammonium salt and the solvent; and (b) mixing the first mixture at a temperature and for a time sufficient to remove water and a portion of the solvent from the first mixture, wherein the mixing is performed in an inert atmosphere and the temperature is less than the decomposition temperature of the quaternary ammonium salt.
摘要翻译： 本文公开了一种方法，包括：（a）在惰性气氛下，将容纳季铵盐的水溶液在容器中加入到有机溶剂中，从而形成包含季铵盐和溶剂的第一混合物; 和（b）将第一混合物在足以从第一混合物中除去水和一部分溶剂的温度和时间下混合，其中混合在惰性气氛中进行，并且温度低于所述第一混合物的分解温度 季铵盐。
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公开(公告)号：US07115785B2
公开(公告)日：2006-10-03
申请号：US10647890
申请日：2003-08-25
申请人： Thomas Link Guggenheim , Daniel Joseph Brunelle , David Winfield Woodruff , Lee Harris Bergman , Norman Enoch Johnson , Matthew Hal Littlejohn , Farid Fouad Khouri
发明人： Thomas Link Guggenheim , Daniel Joseph Brunelle , David Winfield Woodruff , Lee Harris Bergman , Norman Enoch Johnson , Matthew Hal Littlejohn , Farid Fouad Khouri
CPC分类号： C07C37/70 , C07C37/66 , C07C39/235
摘要： Disclosed is a method for preparing an alkali metal salt of a hydroxy-substituted hydrocarbon which comprises the steps of (i) contacting in solvent media at least one hydroxy-substituted hydrocarbon with a base comprising an alkali metal cation; and (ii) devolatilizing the solvent media comprising alkali metal salt by adding or spraying the solvent media into a substantially water-immiscible organic solvent, said solvent being at a temperature greater than the boiling point of solvent media at the prevailing pressure. In one embodiment the solvent media comprises water, and optionally at least one water-soluble protic organic solvent.
摘要翻译： 公开了一种制备羟基取代烃的碱金属盐的方法，其包括以下步骤：（i）在溶剂介质中使至少一种羟基取代的烃与包含碱金属阳离子的碱接触; 和（ii）通过将溶剂介质加入或喷雾到基本上与水不混溶的有机溶剂中来使包含碱金属盐的溶剂介质脱挥发分，所述溶剂的温度大于溶剂介质在当前压力下的沸点。 在一个实施方案中，溶剂介质包含水和任选的至少一种水溶性质子有机溶剂。
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公开(公告)号：US07842188B2
公开(公告)日：2010-11-30
申请号：US11684882
申请日：2007-03-12
申请人： David Bruce Hall , Thomas Link Guggenheim , James Manio Silva , Farid Fouad Khouri , Matthew Hal Littlejohn , Balakrishnan Ganesan , Ashok Shankrappa Shyadligeri , Pradeep Jeevaji Nadkarni
发明人： David Bruce Hall , Thomas Link Guggenheim , James Manio Silva , Farid Fouad Khouri , Matthew Hal Littlejohn , Balakrishnan Ganesan , Ashok Shankrappa Shyadligeri , Pradeep Jeevaji Nadkarni
CPC分类号： C02F9/00 , B01D61/027 , C02F1/281 , C02F1/283 , C02F1/44 , C02F2101/38 , C07C277/06 , C07C279/04
摘要： Disclosed is a method for removing a neutral or an ionic guanidine compound from aqueous media optionally comprising an alkali metal halide, wherein the method is selected from the group consisting of (a) adsorption onto a carbonaceous adsorbent, (b) adsorption onto a clay adsorbent, (c) filtration through a nanofiltration membrane, and (d) removal of water and calcination.
摘要翻译： 公开了一种从任选地包含碱金属卤化物的水性介质中除去中性或离子胍化合物的方法，其中所述方法选自（a）吸附到含碳吸附剂上，（b）吸附到粘土吸附剂上 ，（c）通过纳滤膜过滤，和（d）去除水和煅烧。
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公开(公告)号：US5756843A
公开(公告)日：1998-05-26
申请号：US768871
申请日：1996-12-17
申请人： Jimmy Lynn Webb , Matthew Hal Littlejohn , Joseph John Caringi , Thomas Link Guggenheim , Robert Joseph Nick , Patrick Joseph McCloskey , Joseph Anthony King, Jr.
发明人： Jimmy Lynn Webb , Matthew Hal Littlejohn , Joseph John Caringi , Thomas Link Guggenheim , Robert Joseph Nick , Patrick Joseph McCloskey , Joseph Anthony King, Jr.
IPC分类号： B01J31/02 , C07C277/08 , C07C279/02 , C07C319/20 , C07C323/20 , C07F9/54 , C08G64/20 , C08G64/30 , C08G65/34 , C07C279/00 , C07C211/63
CPC分类号： C08G64/307 , B01J31/0239 , B01J31/0247 , B01J31/0251 , B01J31/0268 , C08G64/20 , B01J2231/14 , B01J2531/98
摘要： Quaternary salts having a double helix structure are prepared by the reaction of dihydroxyaromatic compound, preferably a bisphenol, with an alkali metal hydroxide and a quaternary salt, such as a tetraalkylammonium or hexaalkylguanidinium chloride. The quaternary salts and their alkaline hydrolysis products are useful as catalysts in various reactions, including imide formation from bisphenol salts and halo- or nitro-substituted phthalimides and redistribution and equilibration of polycarbonates.
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公开(公告)号：US5916997A
公开(公告)日：1999-06-29
申请号：US30076
申请日：1998-02-25
申请人： Jimmy Lynn Webb , Randall Lee Carter , Tiberiu Mircca Siclovan , Matthew Hal Littlejohn , James Edward Pickett
发明人： Jimmy Lynn Webb , Randall Lee Carter , Tiberiu Mircca Siclovan , Matthew Hal Littlejohn , James Edward Pickett
摘要： Disclosed are weatherable polyester soft block copolymer compositions comprising copolymers of resorcinol or alternatively phenol, aromatic dicarboxylic acid, and a aliphatic dicarboxylic acid based structural units. These polyester soft block copolymers comprise a substantial proportion of direct linkages between the resorcinol or alternatively the phenol, and the aromatic dicarboxylic acid based structural units, the balance of the linkages being between resorcinol and the aliphatic dicarboxylic acid based structural units.
摘要翻译： 公开了耐候性聚酯软嵌段共聚物组合物，其包含间苯二酚或可选的苯酚，芳族二羧酸和基于脂族二羧酸的结构单元的共聚物。 这些聚酯软嵌段共聚物包括在间苯二酚或可选择的苯酚和基于芳族二羧酸的结构单元之间的相当大比例的直接连接，其间的连接是在间苯二酚和基于脂族二羧酸的结构单元之间。
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公开(公告)号：US06784253B2
公开(公告)日：2004-08-31
申请号：US10200877
申请日：2002-07-23
申请人： Shripathy Vilasagar , Vern Lowry , Dane M. Ferraris , Ke Feng , Robert E. Colborn , Matthew Hal Littlejohn , David Francis Townsend
发明人： Shripathy Vilasagar , Vern Lowry , Dane M. Ferraris , Ke Feng , Robert E. Colborn , Matthew Hal Littlejohn , David Francis Townsend
IPC分类号： C08L5104
CPC分类号： C08F279/04 , C08F2/38 , C08F36/04
摘要： An emulsion polymerization process for the preparation of polybutadiene grafted with styrene and acrylonitrile monomers in a reaction system is provided. The resultant product has a low end content of unreacted residual monomers, low yellowness index, and improved impact strength. The diene rubber is prepared via a process wherein a chain transfer agent is added on a continuous basis to give a rubber substrate having a low crosslink density. In one embodiment of the invention, the process includes charging the reaction system with a pre-selected diene emulsion with a low crosslink density, adding a first portion of at least one of a styrene monomer and acrylonitrile monomer to the diene emulsion, adding to the reaction system, over a predetermined time, an initiator and a second portion of acrylonitrile and styrene monomer, and polymerizing the catalyzed reaction mixture of diene substrate, styrene and acrylonitrile to form ABS graft polymers. In another embodiment, a third monomer is added after the conversion rate of the monomers is greater than 98%.
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