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    METHOD FOR PRODUCING FATTY ACID ALKYL ESTERS AND/OR GLYCERIN
    3.
    发明申请
    METHOD FOR PRODUCING FATTY ACID ALKYL ESTERS AND/OR GLYCERIN 审中-公开
    生产脂肪酸乙酯和/或甘氨酸的方法

    公开(公告)号：US20090069586A1

    公开(公告)日：2009-03-12

    申请号：US11816754

    申请日：2006-02-20

    申请人： Tomoharu Oku ,  Toshimitsu Moriguchi ,  Takeo Akatsuka ,  Masanori Nonoguchi

    发明人： Tomoharu Oku ,  Toshimitsu Moriguchi ,  Takeo Akatsuka ,  Masanori Nonoguchi

    IPC分类号： C11C1/02 ,  C07C31/22 ,  C01G23/04 ,  C01G25/02 ,  C01B33/00

    CPC分类号： B01J23/002 ,  B01J21/063 ,  B01J21/066 ,  B01J23/06 ,  B01J23/34 ,  B01J23/8472 ,  B01J35/002 ,  B01J37/08 ,  B01J2523/00 ,  C07C67/03 ,  C11C3/003 ,  C07C69/52 ,  C07C69/24 ,  B01J2523/31 ,  B01J2523/47 ,  B01J2523/41 ,  B01J2523/72 ,  B01J2523/847 ,  B01J2523/48 ,  B01J2523/842 ,  B01J2523/27 ,  B01J2523/845 ,  B01J2523/55

    摘要： To provide: a production method using a catalyst which can substantially suppress leaching of active metal components and exhibit high activity for both reactions of transesterification of glycerides and esterification of free fatty acids each contained in a fat or oil; and the catalyst. A method for producing fatty acid alkyl esters and/or glycerin comprising a step of bringing a fat or oil into contact with an alcohol in the presence of a catalyst, wherein the catalyst is at least one catalyst selected from the group consisting of the following (I) to (V): (I) a metal oxide having an ilmenite structure and/or a slyrankite structure; (II) an oxide containing a metallic element belonging to the Group 12 and a metallic element belonging to the Group 4; (III) a mixed oxide containing a metallic element belonging to the Group 12 and a tetravalent transition metallic element; (IV) a metal oxide containing zirconium and at least one metallic element selected from the group consisting of metallic elements belonging to the Groups 4, 5 and 8; and (V) a metal oxide containing anatase type titanium oxide and/or rutile type titanium oxide, and the metal oxide containing a sulfur component of 700 ppm or less.

    摘要翻译： 提供：使用能够基本上抑制活性金属成分的浸出的催化剂的制造方法，并且对于甘油酯的酯交换反应和脂肪或油中各自含有游离脂肪酸的酯化反应均表现出高活性; 和催化剂。 一种生产脂肪酸烷基酯和/或甘油的方法，包括在催化剂存在下使脂肪或油与醇接触的步骤，其中所述催化剂是选自下列的至少一种催化剂（ I）至（V）：（I）具有钛铁矿结构和/或硅藻土结构的金属氧化物; （II）含有属于第12族的金属元素的氧化物和属于第4族的金属元素; （III）含有属于第12族的金属元素和四价过渡金属元素的混合氧化物; （IV）含有锆的金属氧化物和选自属于第4,5,8族的金属元素的至少一种金属元素; 和（V）含有锐钛矿型氧化钛和/或金红石型氧化钛的金属氧化物，以及含有700ppm以下的硫成分的金属氧化物。

    Method of production of fatty acid alkyl esters and/or glycerine and fatty acid alkyl ester-containing composition
    4.
    发明申请
    Method of production of fatty acid alkyl esters and/or glycerine and fatty acid alkyl ester-containing composition 失效
    脂肪酸烷基酯和/或甘油和含脂肪酸烷基酯的组合物的生产方法

    公开(公告)号：US20070167642A1

    公开(公告)日：2007-07-19

    申请号：US10569979

    申请日：2004-08-30

    申请人： Tomoharu Oku ,  Masanori Nonoguchi ,  Toshimitsu Moriguchi

    发明人： Tomoharu Oku ,  Masanori Nonoguchi ,  Toshimitsu Moriguchi

    IPC分类号： C07C51/43

    CPC分类号： B01J23/22 ,  B01J21/063 ,  B01J21/066 ,  B01J23/20 ,  B01J23/8472 ,  B01J35/002 ,  C11C3/003 ,  Y02E50/13

    摘要： The method of producing fatty acid alkyl esters and/or glycerine of the present invention is a method of producing high-purity fatty acid alkyl esters and/or glycerine advantageously from the energy viewpoint while reducing the energy consumption of the production, and the products can be used in various fields of application, for example in biodiesel fuels, foods, cosmetics and pharmaceuticals. The above-mentioned method of producing fatty acid alkyl esters and/or glycerine by reacting a fat or oil with an alcohol using an insoluble solid catalyst in a reaction apparatus comprising at least one reactor, comprises (a) a step of obtaining low-boiling components removed liquid by removing low-boiling components or fraction from an effluent liquid of a reactor and (b) a step of separating the fatty acid alkyl esters and glycerine from the low-boiling components removed liquid, wherein an eluted active metal component of the insoluble solid catalyst in the effluent liquid of a reactor amounts to a level not higher than 1,000 ppm.

    摘要翻译： 本发明的脂肪酸烷基酯和/或甘油的制造方法是从能源角度有利地生产高纯度脂肪酸烷基酯和/或甘油的方法，同时降低生产的能量消耗，并且产品可以 可用于各种应用领域，例如生物柴油燃料，食品，化妆品和药品。 上述通过在包含至少一个反应器的反应装置中使用不溶性固体催化剂使脂肪或油与醇反应制备脂肪酸烷基酯和/或甘油的方法包括（a）获得低沸点 组分通过从反应器的流出液中除去低沸点组分或部分来除去液体，和（b）从低沸点组分除去的液体中分离脂肪酸烷基酯和甘油的步骤，其中洗脱的活性金属组分 反应器流出液中不溶性固体催化剂的含量不高于1,000ppm。

    Method of production of fatty acid alkyl esters and/or glycerine and fatty acid alkyl ester-containing composition
    5.
    发明授权
    Method of production of fatty acid alkyl esters and/or glycerine and fatty acid alkyl ester-containing composition 失效
    脂肪酸烷基酯和/或甘油和脂肪酸烷基酯组合物的生产方法

    公开(公告)号：US07605281B2

    公开(公告)日：2009-10-20

    申请号：US10569979

    申请日：2004-08-30

    申请人： Tomoharu Oku ,  Masanori Nonoguchi ,  Toshimitsu Moriguchi

    发明人： Tomoharu Oku ,  Masanori Nonoguchi ,  Toshimitsu Moriguchi

    IPC分类号： C11C3/00

    CPC分类号： B01J23/22 ,  B01J21/063 ,  B01J21/066 ,  B01J23/20 ,  B01J23/8472 ,  B01J35/002 ,  C11C3/003 ,  Y02E50/13

    摘要： The method of producing fatty acid alkyl esters and/or glycerine of the present invention is a method of producing high-purity fatty acid alkyl esters and/or glycerine advantageously from the energy viewpoint while reducing the energy consumption of the production, and the products can be used in various fields of application, for example in biodiesel fuels, foods, cosmetics and pharmaceuticals.The above-mentioned method of producing fatty acid alkyl esters and/or glycerine by reacting a fat or oil with an alcohol using an insoluble solid catalyst in a reaction apparatus comprising at least one reactor, comprises (a) a step of obtaining low-boiling components removed liquid by removing low-boiling components or fraction from an effluent liquid of a reactor and (b) a step of separating the fatty acid alkyl esters and glycerine from the low-boiling components removed liquid, wherein an eluted active metal component of the insoluble solid catalyst in the effluent liquid of a reactor amounts to a level not higher than 1,000 ppm.

    摘要翻译： 本发明的脂肪酸烷基酯和/或甘油的制造方法是从能源角度有利地生产高纯度脂肪酸烷基酯和/或甘油的方法，同时降低生产的能量消耗，并且产品可以 可用于各种应用领域，例如生物柴油燃料，食品，化妆品和药品。 上述通过在包含至少一个反应器的反应装置中使用不溶性固体催化剂使脂肪或油与醇反应制备脂肪酸烷基酯和/或甘油的方法包括（a）获得低沸点 组分通过从反应器的流出液中除去低沸点组分或部分来除去液体，和（b）从低沸点组分除去的液体中分离脂肪酸烷基酯和甘油的步骤，其中洗脱的活性金属组分 反应器流出液中不溶性固体催化剂的含量不高于1,000ppm。

    Method for producing fluoroaryl metal compound
    6.
    发明授权
    Method for producing fluoroaryl metal compound 失效
    氟芳基金属化合物的制备方法

    公开(公告)号：US06465668B2

    公开(公告)日：2002-10-15

    申请号：US09993892

    申请日：2001-11-27

    申请人： Ikuyo Ikeno ,  Hitoshi Mitsui ,  Toshiya Iida ,  Toshimitsu Moriguchi

    发明人： Ikuyo Ikeno ,  Hitoshi Mitsui ,  Toshiya Iida ,  Toshimitsu Moriguchi

    IPC分类号： C07F722

    CPC分类号： C07F7/2208

    摘要： A method for easily and inexpensively producing and purifying a fluoroaryl metal compound such as bis(pentafluorophenyl)dialkyltin which is less colored and has no impurities is provided. Hydrocarbon magnesium halide is reacted with fluoroaryl halide in a solvent including an ether solvent so as to obtain fluoroaryl magnesium halide, which is then reacted with an organic metal compound so as to produce a fluoroaryl metal compound. Tin is more preferable as a metal atom included in the organic metal compound. As for the ether solvent, chain ether solvents are preferable, more specifically, diisopropyl ether, dibutyl ether, and t-butylmethyl ether are more preferable. Besides, it is preferable that magnesium halide, which is a by-product of the fluoroaryl metal compound, is precipitated and removed, or treated with an acid.

    摘要翻译： 提供了一种容易且廉价地生产和纯化氟代芳基金属化合物如双（五氟苯基）二烷基锡的方法，所述二（五氟苯基）二烷基锡颜色较少，没有杂质。 碳氢化镁卤化物与氟芳基卤化物在包括醚溶剂的溶剂中反应，得到氟化芳基卤化镁，然后与有机金属化合物反应，生成氟芳基金属化合物。 作为有机金属化合物中的金属原子，更优选锡。 对于醚类溶剂，优选链状醚溶剂，更优选二异丙基醚，二丁基醚和叔丁基甲基醚。 此外，优选将作为氟代芳基金属化合物的副产物的卤化镁沉淀除去，或用酸处理。

    PROCESS FOR PRODUCING ACROLEIN
    7.
    发明申请
    PROCESS FOR PRODUCING ACROLEIN 失效
    生产ACROLEIN的方法

    公开(公告)号：US20100113838A1

    公开(公告)日：2010-05-06

    申请号：US12451498

    申请日：2008-05-15

    申请人： Yoshitaka Arita ,  Tsukasa Takahashi ,  Masaki Okada ,  Toshimitsu Moriguchi

    发明人： Yoshitaka Arita ,  Tsukasa Takahashi ,  Masaki Okada ,  Toshimitsu Moriguchi

    IPC分类号： C07C45/00 ,  B01J27/18

    CPC分类号： B01J37/036 ,  B01J27/1804 ,  B01J27/285 ,  B01J37/03 ,  C07C45/52 ,  Y02P20/584 ,  C07C47/22

    摘要： There is provided a process for producing acrolein, which makes it possible to obtain acrolein in high yield by dehydration of glycerin. Glycerin is allowed to coexist with a catalyst containing a rare earth metal salt crystal of phosphoric acid, thereby dehydrating the glycerin, wherein the crystal is obtained by calcining a solid which is formed by allowing a liquid containing water and a hydroxide of the rare earth metal and/or a dehydration condensate of the hydroxide to contain phosphate ions.

    摘要翻译： 提供了制备丙烯醛的方法，其可以通过甘油脱水以高产率获得丙烯醛。 甘油与含有磷酸稀土金属盐晶体的催化剂共存，从而使甘油脱水，其中通过煅烧通过使含有水的液体和稀土金属的氢氧化物形成的固体而获得的结晶 和/或氢氧化物的脱水缩合物以含有磷酸根离子。

    Method for purifying fluoroaryl borane derivative and bis (fluoraryl) borane derivative
    8.
    发明授权
    Method for purifying fluoroaryl borane derivative and bis (fluoraryl) borane derivative 失效
    氟芳基硼烷衍生物和双（氟芳基）硼烷衍生物的纯化方法

    公开(公告)号：US06818785B2

    公开(公告)日：2004-11-16

    申请号：US10220635

    申请日：2002-09-04

    申请人： Ikuyo Ikeno ,  Hitoshi Mitsui ,  Toshiya Iida ,  Toshimitsu Moriguchi

    发明人： Ikuyo Ikeno ,  Hitoshi Mitsui ,  Toshiya Iida ,  Toshimitsu Moriguchi

    IPC分类号： C07F504

    CPC分类号： C07F5/027

    摘要： After a fluoroaryl borane derivative is precipitated from a solution containing the fluoroaryl borane derivative, a bis (fluoroaryl) borane derivative, and a hydrocarbon solvent and is subjected to first filtration so that the fluoroaryl borane derivative is isolated, a filtrate that has been obtained by the first filtration is cooled and the bis (fluoroaryl) borane derivative is separated and is subjected to second filtration so that the bis (fluoroaryl) borane derivative is isolated. In a case where the solution contains fluorobenzene, the solution is concentrated, so that the fluorobenzene is removed. Thus, it is possible to provide the high-purity fluoroaryl borane derivative and bis (fluoroaryl) borane derivative having no impurity with ease and at a low cost.

    摘要翻译： 氟化芳基硼烷衍生物从含有氟代芳基硼烷衍生物，双（氟化芳基）硼烷衍生物和烃溶剂的溶液中沉淀出来，并进行第一次过滤以分离出氟化芳基硼烷衍生物，得到的滤液由 将第一次过滤冷却并分离双（氟化芳基）硼烷衍生物，并进行第二次过滤，从而分离双（氟化芳基）硼烷衍生物。 在溶液含有氟苯的情况下，将溶液浓缩，以除去氟苯。 因此，可以容易且低成本地提供不含杂质的高纯度氟代芳基硼烷衍生物和双（氟代芳基）硼烷衍生物。

    Process for producing acrolein
    10.
    发明授权
    Process for producing acrolein 失效
    制备丙烯醛的方法

    公开(公告)号：US07847131B2

    公开(公告)日：2010-12-07

    申请号：US12451498

    申请日：2008-05-15

    申请人： Yoshitaka Arita ,  Tsukasa Takahashi ,  Masaki Okada ,  Toshimitsu Moriguchi

    发明人： Yoshitaka Arita ,  Tsukasa Takahashi ,  Masaki Okada ,  Toshimitsu Moriguchi

    IPC分类号： C07C45/52

    CPC分类号： B01J37/036 ,  B01J27/1804 ,  B01J27/285 ,  B01J37/03 ,  C07C45/52 ,  Y02P20/584 ,  C07C47/22

    摘要： There is provided a process for producing acrolein, which makes it possible to obtain acrolein in high yield by dehydration of glycerin. Glycerin is allowed to coexist with a catalyst containing a rare earth metal salt crystal of phosphoric acid, thereby dehydrating the glycerin, wherein the crystal is obtained by calcining a solid which is formed by allowing a liquid containing water and a hydroxide of the rare earth metal and/or a dehydration condensate of the hydroxide to contain phosphate ions.

    摘要翻译： 提供了制备丙烯醛的方法，其可以通过甘油脱水以高产率获得丙烯醛。 甘油与含有磷酸稀土金属盐晶体的催化剂共存，从而使甘油脱水，其中通过煅烧通过使含有水的液体和稀土金属的氢氧化物形成的固体而获得的结晶 和/或氢氧化物的脱水缩合物以含有磷酸根离子。