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公开(公告)号：US20230150091A1
公开(公告)日：2023-05-18
申请号：US18097398
申请日：2023-01-16
Applicant: US Synthetic Corporation
Inventor： Julie Ann Kidd , Heather Marie Schaefer , Jason K. Wiggins , Cody Frisby
IPC: B24D3/10 , E21B10/42 , E21B10/567 , B24D99/00
CPC classification number: B24D3/10 , B24D99/005 , E21B10/42 , E21B10/567
Abstract: Embodiments relate to polycrystalline diamond compacts (“PDCs”), methods of fabricating PDCs, and applications for such PDCs. In an embodiment, a method includes providing an at least partially leached polycrystalline diamond (“PCD”) body. A residual amount of acid may remain in and/or on the at least partially leached PCD body. The method further includes removing and/or neutralizing at least some of the residual amount of acid from the at least partially leached PCD body and/or a substrate to which the at least partially leached PCD body is attached.
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公开(公告)号：US20210262295A1
公开(公告)日：2021-08-26
申请号：US17183478
申请日：2021-02-24
Applicant: US SYNTHETIC CORPORATION
Inventor： Kenneth E. Bertagnolli , David P. Miess , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay
IPC: E21B10/567 , B22F7/08 , C22C26/00 , E21B10/573 , E21B10/46 , E21B10/55 , E21B10/36
Abstract: In an embodiment, a method of fabricating a polycrystalline diamond compact is disclosed. The method includes sintering a plurality of diamond particles in the presence of a metal-solvent catalyst to form a polycrystalline diamond body; leaching the polycrystalline diamond body to at least partially remove the metal-solvent catalyst therefrom, thereby forming an at least partially leached polycrystalline diamond body; and subjecting an assembly of the at least partially leached polycrystalline diamond body and a cemented carbide substrate to a high-pressure/high-temperature process at a pressure to infiltrate the at least partially leached polycrystalline diamond body with an infiltrant. The pressure of the high-pressure/high-temperature process is less than that employed in the act of sintering of the plurality of diamond particles.
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3.发明授权公开(公告)号：US10507565B2
公开(公告)日：2019-12-17
申请号：US15080379
申请日：2016-03-24
Applicant: US SYNTHETIC CORPORATION
Inventor： Kenneth E. Bertagnolli , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay , Brandon P. Linford
Abstract: Embodiments of the invention relate to polycrystalline diamond compacts (“PDC”) exhibiting enhanced diamond-to-diamond bonding. In an embodiment, a PDC includes a polycrystalline diamond (“PCD”) table bonded to a substrate. At least a portion of the PCD table includes a plurality of diamond grains defining a plurality of interstitial regions. The plurality of interstitial regions includes a metal-solvent catalyst. The plurality of diamond grains exhibit an average grain size of about 30 μm or less. The plurality of diamond grains and the metal-solvent catalyst collectively exhibit an average electrical conductivity of less than about 1200 S/m. Other embodiments are directed to PCD, employing such PCD, methods of forming PCD and PDCs, and various applications for such PCD and PDCs in rotary drill bits, bearing apparatuses, and wire-drawing dies.
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公开(公告)号：US20240410232A1
公开(公告)日：2024-12-12
申请号：US18662563
申请日：2024-05-13
Applicant: US SYNTHETIC CORPORATION
Inventor： Kenneth E. Bertagnolli , David P. Miess , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay
IPC: E21B10/567 , B22F7/08 , B24D18/00 , C22C26/00 , E21B10/36 , E21B10/46 , E21B10/55 , E21B10/573 , F16C17/02 , F16C17/04 , F16C17/10 , F16C33/04 , F16C33/26
Abstract: In an embodiment, a method of fabricating a polycrystalline diamond compact is disclosed. The method includes sintering a plurality of diamond particles in the presence of a metal-solvent catalyst to form a polycrystalline diamond body; leaching the polycrystalline diamond body to at least partially remove the metal-solvent catalyst therefrom, thereby forming an at least partially leached polycrystalline diamond body; and subjecting an assembly of the at least partially leached polycrystalline diamond body and a cemented carbide substrate to a high-pressure/high-temperature process at a pressure to infiltrate the at least partially leached polycrystalline diamond body with an infiltrant. The pressure of the high-pressure/high-temperature process is less than that employed in the act of sintering of the plurality of diamond particles.
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公开(公告)号：US10773480B2
公开(公告)日：2020-09-15
申请号：US16589279
申请日：2019-10-01
Applicant: US SYNTHETIC CORPORATION
Inventor： Kenneth E. Bertagnolli , Michael A. Vail , Jiang Qian , Jason K. Wiggins , Mark P. Chapman , Arnold D. Cooper , Debkumar Mukhopadhyay , Amy Leigh Rodriguez , Stephen Rudger Adams
Abstract: Embodiments disclosed herein relate to cell assemblies for fabricating superhard materials (e.g., used in a high-pressure cubic press) and methods of using the same. The disclosed cell assemblies include a plurality of internal anvils, at least some of which are positioned internally relative to a cell pressure medium of the cell assembly. Such a configuration for the cell assemblies may enable one or more of intensifying cell pressure, reducing processing time, or reducing costs for fabricating such superhard materials.
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Patent Agency Ranking
公开(公告)号：US20190211629A1
公开(公告)日：2019-07-11
申请号：US16358281
申请日：2019-03-19
Applicant: US SYNTHETIC CORPORATION
Inventor： Kenneth E. Bertagnolli , David P. Miess , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay
Abstract: In an embodiment, a method of fabricating a polycrystalline diamond compact is disclosed. The method includes sintering a plurality of diamond particles in the presence of a metal-solvent catalyst to form a polycrystalline diamond body; leaching the polycrystalline diamond body to at least partially remove the metal-solvent catalyst therefrom, thereby forming an at least partially leached polycrystalline diamond body; and subjecting an assembly of the at least partially leached polycrystalline diamond body and a cemented carbide substrate to a high-pressure/high-temperature process at a pressure to infiltrate the at least partially leached polycrystalline diamond body with an infiltrant. The pressure of the high-pressure/high-temperature process is less than that employed in the act of sintering of the plurality of diamond particles.
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公开(公告)号：US10101263B1
公开(公告)日：2018-10-16
申请号：US14557154
申请日：2014-12-01
Applicant: US SYNTHETIC CORPORATION
Inventor： Michael A. Vail , Kenneth E. Bertagnolli , Jason K. Wiggins
Abstract: Embodiments of methods are disclosed for characterizing a tested superabrasive element, such as a polycrystalline diamond element. In an embodiment, a method of characterizing the relative strength of a superabrasive element is disclosed. A first superabrasive element and a second superabrasive element are positioned upper surface to upper surface, including an area of overlap between the upper surfaces. A load is applied while the first and second superabrasive elements are overlapped until failure of one or both of the first or second superabrasive elements fail. A relative strength is determined using at least the load during failure as a parameter.
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公开(公告)号：US20130205677A1
公开(公告)日：2013-08-15
申请号：US13789099
申请日：2013-03-07
Applicant: US Synthetic Corporation
Inventor： Kenneth E. Bertagnolli , David P. Miess , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay
IPC: B24D18/00
CPC classification number: E21B10/36 , B22F7/08 , B22F2998/00 , B24D18/00 , C22C26/00 , E21B10/5735 , F16C33/043 , F16C2352/00 , Y10T428/24612 , Y10T428/24996 , Y10T428/249967 , C22C29/08
Abstract: In an embodiment, a method of fabricating a polycrystalline diamond compact is disclosed. The method includes sintering a plurality of diamond particles in the presence of a metal-solvent catalyst to form a polycrystalline diamond body; leaching the polycrystalline diamond body to at least partially remove the metal-solvent catalyst therefrom, thereby forming an at least partially leached polycrystalline diamond body; and subjecting an assembly of the at least partially leached polycrystalline diamond body and a cemented carbide substrate to a high-pressure/high-temperature process at a pressure to infiltrate the at least partially leached polycrystalline diamond body with an infiltrant. The pressure of the high-pressure/high-temperature process is less than that employed in the act of sintering of the plurality of diamond particles.
Abstract translation: 在一个实施例中，公开了一种制造多晶金刚石致密体的方法。 该方法包括在金属 - 溶剂催化剂的存在下烧结多个金刚石颗粒以形成多晶金刚石体; 浸出多晶金刚石体至少部分地从其中去除金属 - 溶剂催化剂，从而形成至少部分浸出的多晶金刚石体; 以及使所述至少部分浸出的多晶金刚石体和硬质合金基底的组件在压力下经受高压/高温过程，以浸润剂渗透至少部分浸出的多晶金刚石体。 高压/高温过程的压力小于在多个金刚石颗粒的烧结过程中使用的压力。
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公开(公告)号：US11738315B2
公开(公告)日：2023-08-29
申请号：US17479553
申请日：2021-09-20
Applicant: US Synthetic Corporation
Inventor： Julie Ann Kidd , Heather Marie Schaefer , Chengkun Xu , Jason K. Wiggins , Matthew Brown , Cody Frisby
IPC: B01J3/06 , E21B10/56 , E21B10/567 , B24D18/00 , C01B32/28
CPC classification number: B01J3/062 , B24D18/00 , B24D18/0009 , B24D18/0027 , C01B32/28 , E21B10/56 , E21B10/567 , B01J2203/062
Abstract: In an embodiment, a polycrystalline diamond table includes a plurality of bonded diamond grains and a plurality of interstitial regions defined by the plurality of bonded diamond grains. The polycrystalline diamond table may be at least partially leached such that at least a portion of at least one interstitial constituent has been removed from at least a portion of the plurality of interstitial regions by exposure to a leaching agent. The leaching agent may include a mixture having a ratio of weight % hydrofluoric acid to weight % nitric acid of about 1.0 to about 2.4, and water in a concentration of about 50 weight % to about 85 weight %. Various other materials, articles, and methods are also disclosed.
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公开(公告)号：US10549402B1
公开(公告)日：2020-02-04
申请号：US14876516
申请日：2015-10-06
Applicant: US SYNTHETIC CORPORATION
Inventor： Julie Ann Kidd , Heather Marie Schaefer , Jason K. Wiggins , Cody Frisby
IPC: B24D3/10 , B24D99/00 , E21B10/42 , E21B10/567
Abstract: Embodiments relate to polycrystalline diamond compacts (“PDCs”), methods of fabricating PDCs, and applications for such PDCs. In an embodiment, a method includes providing an at least partially leached polycrystalline diamond (“PCD”) body. A residual amount of acid may remain in and/or on the at least partially leached PCD body. The method further includes removing and/or neutralizing at least some of the residual amount of acid from the at least partially leached PCD body and/or a substrate to which the at least partially leached PCD body is attached.
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