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公开(公告)号：US10773480B2
公开(公告)日：2020-09-15
申请号：US16589279
申请日：2019-10-01
发明人： Kenneth E. Bertagnolli , Michael A. Vail , Jiang Qian , Jason K. Wiggins , Mark P. Chapman , Arnold D. Cooper , Debkumar Mukhopadhyay , Amy Leigh Rodriguez , Stephen Rudger Adams
摘要： Embodiments disclosed herein relate to cell assemblies for fabricating superhard materials (e.g., used in a high-pressure cubic press) and methods of using the same. The disclosed cell assemblies include a plurality of internal anvils, at least some of which are positioned internally relative to a cell pressure medium of the cell assembly. Such a configuration for the cell assemblies may enable one or more of intensifying cell pressure, reducing processing time, or reducing costs for fabricating such superhard materials.
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公开(公告)号：US20190211629A1
公开(公告)日：2019-07-11
申请号：US16358281
申请日：2019-03-19
发明人： Kenneth E. Bertagnolli , David P. Miess , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay
摘要： In an embodiment, a method of fabricating a polycrystalline diamond compact is disclosed. The method includes sintering a plurality of diamond particles in the presence of a metal-solvent catalyst to form a polycrystalline diamond body; leaching the polycrystalline diamond body to at least partially remove the metal-solvent catalyst therefrom, thereby forming an at least partially leached polycrystalline diamond body; and subjecting an assembly of the at least partially leached polycrystalline diamond body and a cemented carbide substrate to a high-pressure/high-temperature process at a pressure to infiltrate the at least partially leached polycrystalline diamond body with an infiltrant. The pressure of the high-pressure/high-temperature process is less than that employed in the act of sintering of the plurality of diamond particles.
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公开(公告)号：US10101263B1
公开(公告)日：2018-10-16
申请号：US14557154
申请日：2014-12-01
摘要： Embodiments of methods are disclosed for characterizing a tested superabrasive element, such as a polycrystalline diamond element. In an embodiment, a method of characterizing the relative strength of a superabrasive element is disclosed. A first superabrasive element and a second superabrasive element are positioned upper surface to upper surface, including an area of overlap between the upper surfaces. A load is applied while the first and second superabrasive elements are overlapped until failure of one or both of the first or second superabrasive elements fail. A relative strength is determined using at least the load during failure as a parameter.
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公开(公告)号：US09719307B1
公开(公告)日：2017-08-01
申请号：US14507638
申请日：2014-10-06
IPC分类号： E21B10/55 , E21B10/567 , E21B10/46 , B24D3/10 , C04B35/63 , C04B35/645
CPC分类号： E21B10/567 , B24D3/10 , B32B9/00 , C04B35/52 , C04B35/6303 , C04B35/645 , C04B2235/3201 , C04B2235/3203 , C04B2235/3206 , C04B2235/3208 , C04B2235/3213 , C04B2235/3225 , C04B2235/3234 , C04B2235/3256 , C04B2235/3272 , C04B2235/3274 , C04B2235/3427 , C04B2235/3821 , C04B2235/3843 , C04B2235/421 , C04B2235/427 , C04B2235/44 , C04B2235/442 , C04B2235/448 , E21B10/55 , Y10T407/27
摘要： A polycrystalline diamond compact useful for wear, cutting, drilling, drawing and like applications is provided with a first diamond region remote from the working surface which has a metallic catalyzing material and a second diamond region adjacent to or including the working surface containing a non-metallic catalyst and the method of making such a compact is provided. This compact is particularly useful in high temperature operations, such as hard rock drilling because of the improved thermal stability at the working surface.
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5.发明申请METHODS OF FABRICATING A POLYCRYSTALLINE DIAMOND COMPACT INCLUDING GASEOUS LEACHING OF A POLYCRYSTALLINE DIAMOND BODY 审中-公开一种制作多晶金刚石复合材料的方法，包括多晶金刚石体的气相浸出公开(公告)号：US20160263727A1
公开(公告)日：2016-09-15
申请号：US14493142
申请日：2014-09-22
IPC分类号： B24D3/10
CPC分类号： B24D3/10 , B24D3/06 , B24D18/00 , B24D99/005 , C09K3/1409
摘要： Embodiments of the invention relate to methods of fabricating polycrystalline diamond compacts (“PDCs”) and applications for such PDCs. In an embodiment, a method of fabricating a PDC includes providing a polycrystalline diamond (“PCD”) table in which a catalyst is disposed throughout, leaching the PCD table with a gaseous leaching agent to remove catalyst from the PCD table and bonding the at least partially leached PCD table to a substrate to form a PDC.
摘要翻译： 本发明的实施例涉及制造多晶金刚石压块（“PDC”）的方法以及用于这种PDC的应用。 在一个实施方案中，制备PDC的方法包括提供在其中设置催化剂的多晶金刚石（“PCD”）工作台，用PCD工作台浸出PCD工作台以从PCD工作台移除催化剂，并将至少 部分浸出的PCD表到基底以形成PDC。
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公开(公告)号：US20130205677A1
公开(公告)日：2013-08-15
申请号：US13789099
申请日：2013-03-07
发明人： Kenneth E. Bertagnolli , David P. Miess , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay
IPC分类号： B24D18/00
CPC分类号： E21B10/36 , B22F7/08 , B22F2998/00 , B24D18/00 , C22C26/00 , E21B10/5735 , F16C33/043 , F16C2352/00 , Y10T428/24612 , Y10T428/24996 , Y10T428/249967 , C22C29/08
摘要： In an embodiment, a method of fabricating a polycrystalline diamond compact is disclosed. The method includes sintering a plurality of diamond particles in the presence of a metal-solvent catalyst to form a polycrystalline diamond body; leaching the polycrystalline diamond body to at least partially remove the metal-solvent catalyst therefrom, thereby forming an at least partially leached polycrystalline diamond body; and subjecting an assembly of the at least partially leached polycrystalline diamond body and a cemented carbide substrate to a high-pressure/high-temperature process at a pressure to infiltrate the at least partially leached polycrystalline diamond body with an infiltrant. The pressure of the high-pressure/high-temperature process is less than that employed in the act of sintering of the plurality of diamond particles.
摘要翻译： 在一个实施例中，公开了一种制造多晶金刚石致密体的方法。 该方法包括在金属 - 溶剂催化剂的存在下烧结多个金刚石颗粒以形成多晶金刚石体; 浸出多晶金刚石体至少部分地从其中去除金属 - 溶剂催化剂，从而形成至少部分浸出的多晶金刚石体; 以及使所述至少部分浸出的多晶金刚石体和硬质合金基底的组件在压力下经受高压/高温过程，以浸润剂渗透至少部分浸出的多晶金刚石体。 高压/高温过程的压力小于在多个金刚石颗粒的烧结过程中使用的压力。
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公开(公告)号：US20210262295A1
公开(公告)日：2021-08-26
申请号：US17183478
申请日：2021-02-24
发明人： Kenneth E. Bertagnolli , David P. Miess , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay
IPC分类号： E21B10/567 , B22F7/08 , C22C26/00 , E21B10/573 , E21B10/46 , E21B10/55 , E21B10/36
摘要： In an embodiment, a method of fabricating a polycrystalline diamond compact is disclosed. The method includes sintering a plurality of diamond particles in the presence of a metal-solvent catalyst to form a polycrystalline diamond body; leaching the polycrystalline diamond body to at least partially remove the metal-solvent catalyst therefrom, thereby forming an at least partially leached polycrystalline diamond body; and subjecting an assembly of the at least partially leached polycrystalline diamond body and a cemented carbide substrate to a high-pressure/high-temperature process at a pressure to infiltrate the at least partially leached polycrystalline diamond body with an infiltrant. The pressure of the high-pressure/high-temperature process is less than that employed in the act of sintering of the plurality of diamond particles.
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8.发明授权公开(公告)号：US10520025B1
公开(公告)日：2019-12-31
申请号：US13761944
申请日：2013-02-07
摘要： Embodiments of the invention relate to bearing assemblies and associated cardiopulmonary bypass blood pumps in which the bearing assembly includes a stator and a rotor each including bearing surfaces oriented so as to be generally opposed to one another. The bearing surface may comprise a polycrystalline diamond material including a plurality of bonded diamond grains defining a plurality of interstitial regions therebetween, in which a non-metallic catalyst (e.g., a carbonate) and/or at least one derivative thereof is disposed interstitially between the bonded diamond grains.
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9.发明授权公开(公告)号：US10507565B2
公开(公告)日：2019-12-17
申请号：US15080379
申请日：2016-03-24
发明人： Kenneth E. Bertagnolli , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay , Brandon P. Linford
IPC分类号： B24D3/10 , E21B10/567 , F16C33/04 , C22C26/00 , F16C33/26 , B22F5/00 , F16C17/02 , F16C17/04
摘要： Embodiments of the invention relate to polycrystalline diamond compacts (“PDC”) exhibiting enhanced diamond-to-diamond bonding. In an embodiment, a PDC includes a polycrystalline diamond (“PCD”) table bonded to a substrate. At least a portion of the PCD table includes a plurality of diamond grains defining a plurality of interstitial regions. The plurality of interstitial regions includes a metal-solvent catalyst. The plurality of diamond grains exhibit an average grain size of about 30 μm or less. The plurality of diamond grains and the metal-solvent catalyst collectively exhibit an average electrical conductivity of less than about 1200 S/m. Other embodiments are directed to PCD, employing such PCD, methods of forming PCD and PDCs, and various applications for such PCD and PDCs in rotary drill bits, bearing apparatuses, and wire-drawing dies.
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公开(公告)号：US09597775B2
公开(公告)日：2017-03-21
申请号：US14520188
申请日：2014-10-21
发明人： Michael A. Vail
CPC分类号： B24D3/10 , B22F2998/10 , E21B10/567 , C22C26/00 , C23F1/00 , B22F3/14
摘要： Embodiments relate to methods of fabricating polycrystalline diamond compacts (“PDCs”) in which a removing agent includes at least one supercritical fluid component that is used to remove at least one interstitial constituent from at least a portion of a polycrystalline diamond (“PCD”) body and applications for such PDCs. Removing the at least one interstitial constituent using the removing agent including the at least one supercritical fluid component may provide more rapid and effective removal of the at least one interstitial constituent from a PCD body than conventional acid leaching. In an embodiment, a method of fabricating at least partially porous PCD body includes providing a PCD body in which at least one interstitial constituent is disposed throughout, and removing at least a portion of the at least one interstitial constituent from the PCD body with a removing agent including at least one supercritical fluid component.
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