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1.发明授权Method for the production of perfluoroalkyl phosphines and the use thereof as perfluoroalkylating reactants 失效制备全氟烷基膦的方法及其作为全氟烷基化反应物的用途公开(公告)号：US07208626B2
公开(公告)日：2007-04-24
申请号：US10511554
申请日：2003-03-17
申请人： Urs Welz-Biermann , Nikolai Ignatyev , Michael Weiden , Michael Schmidt , Udo Heider , Alexej Miller , Helge Willner , Peter Sartori
发明人： Urs Welz-Biermann , Nikolai Ignatyev , Michael Weiden , Michael Schmidt , Udo Heider , Alexej Miller , Helge Willner , Peter Sartori
IPC分类号： C07F9/02
摘要： The invention relates to a method for producing perfluoroalkyl phosphines, comprising at least one step in which at least one fluoro(perfluoroalkyl)phosphorane is reacted with at least one hydride ion donator, and the use of tris(perfluoroalkyl)phos-phines as perfluoroalkylating reactants.
摘要翻译： 本发明涉及一种制备全氟烷基膦的方法，其包括至少一个步骤，其中至少一个氟（全氟烷基）正膦与至少一个氢化物离子供体反应，并且使用三（全氟烷基）磷 - 作为全氟烷基化反应物 。
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2.发明申请PROCESS FOR THE PREPARATION OF PERFLUOROALKYLPHOSPHINES AND THE USE THEREOF AS PERFLUOROALKYLATING REAGENTS 失效制备全氟烷基磷酸酯的方法及其作为全氟化合物试剂的用途公开(公告)号：US20070191637A1
公开(公告)日：2007-08-16
申请号：US11738985
申请日：2007-04-23
申请人： Urs Welz-Biermann , Nikolai Ignatyev , Michael Weiden , Michael Schmidt , Udo Heider , Alexej Miller , Helge Willner , Peter Sartori
发明人： Urs Welz-Biermann , Nikolai Ignatyev , Michael Weiden , Michael Schmidt , Udo Heider , Alexej Miller , Helge Willner , Peter Sartori
IPC分类号： C07F9/02
摘要： The present invention relates to a process for the preparation of perfluoroalkylphosphines comprising at least the reaction of at least one fluoro(perfluoroalkyl)phosphorane with at least one hydride ion donor, and to the use of tris(perfluoroalkyl)phosphines as perfluoroalkylating reagents.
摘要翻译： 本发明涉及制备全氟烷基膦的方法，该方法至少包括至少一种氟（全氟烷基）正膦与至少一种氢化物离子给体的反应，以及使用三（全氟烷基）膦作为全氟烷基化试剂。
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3.发明授权Process for the preparation of perfluoroalkylphosphines and the use thereof as perfluoroalkylating reagents 失效制备全氟烷基膦的方法及其作为全氟烷基化试剂的用途公开(公告)号：US07632969B2
公开(公告)日：2009-12-15
申请号：US11738985
申请日：2007-04-23
申请人： Urs Welz-Biermann , Nikolai Ignatyev , Michael Weiden , Michael Schmidt , Udo Heider , Alexej Miller , Helge Willner , Peter Sartori
发明人： Urs Welz-Biermann , Nikolai Ignatyev , Michael Weiden , Michael Schmidt , Udo Heider , Alexej Miller , Helge Willner , Peter Sartori
IPC分类号： C07C9/02
摘要： The present invention relates to a process for the preparation of perfluoroalkylphosphines comprising at least the reaction of at least one fluoro(perfluoroalkyl)phosphorane with at least one hydride ion donor, and to the use of tris(perfluoroalkyl)phosphines as perfluoroalkylating reagents.
摘要翻译： 本发明涉及制备全氟烷基膦的方法，该方法至少包括至少一种氟（全氟烷基）正膦与至少一种氢化物离子给体的反应，以及使用三（全氟烷基）膦作为全氟烷基化试剂。
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4.发明申请Method for perfluoroalkylation by means of tris (perfluoroalkyl) phosphine oxides 审中-公开通过三（全氟烷基）氧化膦进行全氟烷基化的方法公开(公告)号：US20050119513A1
公开(公告)日：2005-06-02
申请号：US10511156
申请日：2003-03-17
申请人： Nikolai Ignatyev , Urs Welz-Biermann , Michael Schmidt , Michael Weiden , Udo Heider , Helge Willner , Peter Sartori , Alexej Miller
发明人： Nikolai Ignatyev , Urs Welz-Biermann , Michael Schmidt , Michael Weiden , Udo Heider , Helge Willner , Peter Sartori , Alexej Miller
CPC分类号： C07F5/02 , C07C29/38 , C07F9/5304 , C07C33/46
摘要： The invention relates to a method for perfluoroalkylation by means of tris(perfluoroalkyl)phosphine oxides.
摘要翻译： 本发明涉及通过三（全氟烷基）氧化膦进行全氟烷基化的方法。
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5.发明授权Process for the preparation of bis(perfluoroalkyl)phosphinic acids and salts thereof 有权制备双（全氟烷基）次膦酸及其盐的方法公开(公告)号：US07202379B2
公开(公告)日：2007-04-10
申请号：US10511157
申请日：2003-03-17
申请人： Urs Welz-Biermann , Nikolai Ignatyev , Michael Weiden , Udo Heider , Andri Kucheryna , Helge Willner , Peter Sartori
发明人： Urs Welz-Biermann , Nikolai Ignatyev , Michael Weiden , Udo Heider , Andri Kucheryna , Helge Willner , Peter Sartori
IPC分类号： C07F9/22
CPC分类号： B01F17/0064 , B01J31/0231 , B01J31/0284 , B01J31/0288 , B01J31/0289 , B01J31/0291 , B01J2531/98 , C07C211/63 , C07D231/12 , C07D233/54 , C07D233/56 , C07D249/08 , C07F9/301 , C07F9/5456
摘要： The present invention relates to a process for the preparation of bis(perfluoroalkyl)phosphinic acids comprising at least the reaction of at least one difluorotris(perfluoroalkyl)phosphorane or at least one trifluorobis(perfluoroalkyl)phosphorane with hydrogen fluoride in a suitable reaction medium, and heating of the resultant reaction mixture. The invention also relates to salts of bis(perfluoroalkyl)phosphinic acids and to the use thereof.
摘要翻译： 本发明涉及一种制备双（全氟烷基）次膦酸的方法，至少包含至少一种二氟三（全氟烷基）正膦或至少一个三氟双（全氟烷基）正膦与氟化氢在合适的反应介质中的反应，以及 加热所得反应混合物。 本发明还涉及双（全氟烷基）次膦酸的盐及其用途。
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6.发明授权Method for the production of monohydro-perfluoroalkanes, bis(perfluoroalkyl)phosphinates and perfluoroalkylphosphonates 有权制备单氢 - 全氟烷烃，双（全氟烷基）次膦酸酯和全氟烷基膦酸酯的方法公开(公告)号：US07145004B2
公开(公告)日：2006-12-05
申请号：US10511171
申请日：2003-03-17
申请人： Nikolai Ignatyev , Michael Weiden , Urs Welz-Biermann , Udo Heider , Peter Sartori , Andriy Kucheryna , Helge Willner
发明人： Nikolai Ignatyev , Michael Weiden , Urs Welz-Biermann , Udo Heider , Peter Sartori , Andriy Kucheryna , Helge Willner
IPC分类号： C07D237/00 , C97D237/02
CPC分类号： B01F17/0064 , B01J31/0231 , B01J31/0284 , B01J31/0288 , B01J31/0289 , B01J31/0291 , B01J2531/98 , C07C17/361 , C07C17/38 , C07C211/63 , C07D231/12 , C07D233/54 , C07D233/56 , C07D249/08 , C07F9/301 , C07F9/3808 , C07F9/5407 , C07C19/08
摘要： The present invention relates to a process for the preparation of monohydroperfluoroalkanes, bis(perfluoroalkyl)phosphinates and perfluoroalkylphosphonates which comprises at least the treatment of at least one perfluoroalkylphosphorane with at least one base in a suitable reaction medium.
摘要翻译： 本发明涉及制备单氢全氟烷烃，双（全氟烷基）次膦酸酯和全氟烷基膦酸酯的方法，该方法至少包括在合适的反应介质中用至少一种碱处理至少一种全氟烷基磷烷。
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7.发明申请Process for the preparation of bis(perfluoroalkyl)phosphinic acids and salts thereof 有权制备双（全氟烷基）次膦酸及其盐的方法公开(公告)号：US20050256334A1
公开(公告)日：2005-11-17
申请号：US10511157
申请日：2003-03-17
申请人： Urs Welz-Biermann , Nikolai Ignatyev , Michael Weiden , Udo Heider , Andriy Kucheryna , Helge Willner , Peter Sartori
发明人： Urs Welz-Biermann , Nikolai Ignatyev , Michael Weiden , Udo Heider , Andriy Kucheryna , Helge Willner , Peter Sartori
IPC分类号： B01F17/00 , B01F17/14 , B01J31/02 , C07C211/07 , C07C211/12 , C07C211/63 , C07D233/54 , C07D233/58 , C07D521/00 , C07F9/30 , C07F9/34 , C07F9/54 , C07F9/22
CPC分类号： B01F17/0064 , B01J31/0231 , B01J31/0284 , B01J31/0288 , B01J31/0289 , B01J31/0291 , B01J2531/98 , C07C211/63 , C07D231/12 , C07D233/54 , C07D233/56 , C07D249/08 , C07F9/301 , C07F9/5456
摘要： The present invention relates to a process for the preparation of bis(perfluoroalkyl)phosphinic acids comprising at least the reaction of at least one difluorotris(perfluoroalkyl)phosphorane or at least one trifluorobis(perfluoroalkyl)phosphorane with hydrogen fluoride in a suitable reaction medium, and heating of the resultant reaction mixture. The invention also relates to salts of bis(perfluoroalkyl)phosphinic acids and to the use thereof.
摘要翻译： 本发明涉及一种制备双（全氟烷基）次膦酸的方法，至少包含至少一种二氟三（全氟烷基）正膦或至少一个三氟双（全氟烷基）正膦与氟化氢在合适的反应介质中的反应，以及 加热所得反应混合物。 本发明还涉及双（全氟烷基）次膦酸的盐及其用途。
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8.发明申请Method for the production of monohydro-perfluoroalkanes, bis (perfluoroalkyl) phosphinates and perfluoroalkylphosphonates 有权制备单氢 - 全氟烷烃，双（全氟烷基）次膦酸酯和全氟烷基膦酸酯的方法公开(公告)号：US20050222411A1
公开(公告)日：2005-10-06
申请号：US10511171
申请日：2003-03-17
申请人： Nikolai Ignatyev , Michael Weiden , Urs Welz-Biermann , Udo Heider , Peter Sartori , Andriy Kucheryna , Helge Willner
发明人： Nikolai Ignatyev , Michael Weiden , Urs Welz-Biermann , Udo Heider , Peter Sartori , Andriy Kucheryna , Helge Willner
IPC分类号： B01F17/00 , B01J31/02 , C07C17/361 , C07C17/38 , C07C19/08 , C07C211/63 , C07D233/54 , C07D233/58 , C07D521/00 , C07F9/30 , C07F9/38 , C07F9/54 , C09K3/00 , C07F9/28
CPC分类号： B01F17/0064 , B01J31/0231 , B01J31/0284 , B01J31/0288 , B01J31/0289 , B01J31/0291 , B01J2531/98 , C07C17/361 , C07C17/38 , C07C211/63 , C07D231/12 , C07D233/54 , C07D233/56 , C07D249/08 , C07F9/301 , C07F9/3808 , C07F9/5407 , C07C19/08
摘要： The present invention relates to a process for the preparation of monohydroperfluoroalkanes, bis(perfluoroalkyl)phosphinates and perfluoroalkylphosphonates which comprises at least the treatment of at least one perfluoroalkylphosphorane with at least one base in a suitable reaction medium.
摘要翻译： 本发明涉及一种制备单氢全氟烷烃，双（全氟烷基）次膦酸酯和全氟烷基膦酸酯的方法，其至少包括在合适的反应介质中用至少一种碱处理至少一种全氟烷基磷烷。
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公开(公告)号：US07094328B2
公开(公告)日：2006-08-22
申请号：US10481786
申请日：2002-06-11
申请人： Nikolai Ignatyev , Michael Schmidt , Andreas Kühner , Volker Hilarius , Udo Heider , Andriy Kucheryna , Peter Sartori , Helge Willner
发明人： Nikolai Ignatyev , Michael Schmidt , Andreas Kühner , Volker Hilarius , Udo Heider , Andriy Kucheryna , Peter Sartori , Helge Willner
IPC分类号： C25B3/08
CPC分类号： B01J31/0288 , B01J31/0278 , B01J2531/985 , C07F9/28 , H01M10/052 , H01M10/0568
摘要： The present invention relates to acids of the general formula [I], [RyPF6-y]−H+ [I], where y=1, 2 or 3, and in which the ligands R may be identical or different and R is a perfluorinated C1-8-alkyl or aryl group or R is a partially fluorinated C1-8-alkyl or aryl group, in which some of the F or H may have been substituted by chlorine. The present invention furthermore relates to a process for the preparation of the acids according to the invention, to salts comprising a cation and the anion of the acid according to the invention, and to a process for the preparation of the salts. The invention furthermore relates to the use of the acids and salts according to the invention.
摘要翻译： 本发明涉及通式[I]的酸，其中R 1，R 2，R 3， 其中y = 1,2或3，其中配体R可以相同或不同，R是全氟化的C 1-8 - 烷基或芳基或R 是部分氟化的C 1-8 - 烷基或芳基，其中一些F或H可能被氯取代。 本发明还涉及根据本发明的酸的制备方法，包括阳离子和根据本发明的酸的阴离子的盐，以及制备盐的方法。 本发明还涉及根据本发明的酸和盐的用途。
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![Ionic liquids having [n(cf3)2]-anions](/abs-image/US/2006/04/13/US20060079691A1/abs.jpg.150x150.jpg)
公开(公告)号：US20060079691A1
公开(公告)日：2006-04-13
申请号：US10538847
申请日：2003-11-17
IPC分类号： C07F9/28
CPC分类号： C07D213/20 , C07D231/12 , C07D233/54 , C07D233/56 , C07D249/08 , C07D277/62 , C07D295/03
摘要： The present invention relates to salts comprising bis(trifluoromethyl)imide anions and saturated, partially or fully unsaturated, heterocyclic cations, to a process for the preparation thereof, and to the use thereof as ionic liquids.
摘要翻译： 本发明涉及包含双（三氟甲基）酰亚胺阴离子和饱和的，部分或完全不饱和的杂环阳离子的盐，其制备方法及其作为离子液体的用途。
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