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公开(公告)号：US06469147B2
公开(公告)日：2002-10-22
申请号：US09780218
申请日：2001-02-09
IPC分类号： C09B4100
CPC分类号： C09B41/008 , B01J19/0093 , B01J2219/00873 , B01J2219/00889 , B01J2219/0095 , B01J2219/00957 , B01J2219/00959 , B01J2219/00961 , B01J2219/00966 , Y10S534/04
摘要： Azo colorants are prepared by conducting the diazotization of aromatic or hetaromatic amines or the azo coupling reaction or the diazotization and the azo coupling reaction in a microreactor.
摘要翻译： 偶氮着色剂是通过在微反应器中进行芳族或异丁胺或偶氮偶合反应或重氮化偶氮偶联反应的重氮化而制备的。
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公开(公告)号：US06548647B2
公开(公告)日：2003-04-15
申请号：US09972102
申请日：2001-10-05
申请人： Erwin Dietz , Joachim Weber , Dieter Schnaitmann , Christian Wille , Leonhard Unverdorben , Klaus Saitmacher , Jörg Jung , Kristina Schiffer
发明人： Erwin Dietz , Joachim Weber , Dieter Schnaitmann , Christian Wille , Leonhard Unverdorben , Klaus Saitmacher , Jörg Jung , Kristina Schiffer
IPC分类号： C09B4100
CPC分类号： C09B41/006
摘要： The invention provides a process for preparing azo colorants which comprises spraying one or more coupling components individually or in a mixture and one or more compatible diazonium salts individually or in a mixture, in their solution or suspension form through nozzles to a point of conjoint collision in a reactor chamber enclosed by a housing in a microjet reactor, a gas or an evaporating liquid being passed into the reactor chamber through an opening in the housing for the purpose of maintaining a gas atmosphere in the reactor chamber, and the resulting product solution or suspension and the gas or the evaporated liquid being removed from the reactor through a further opening in the housing by means of overpressure on the gas entry side or underpressure on the product and gas exit side.
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公开(公告)号：US06616859B1
公开(公告)日：2003-09-09
申请号：US09879747
申请日：2001-06-11
IPC分类号： C09K300
CPC分类号： B01J19/0093 , B01J2219/00835 , B01J2219/00873 , B01J2219/00889 , B01J2219/00984 , C07C29/70 , C07C31/30
摘要： A process for preparing alcoholic solutions of alkali metal alkoxides. The process includes reacting an alkali metal with an alcohol in a microreactor wherein the microreactor provides laminer flow.
摘要翻译： 一种制备碱金属醇盐的醇溶液的方法。 该方法包括在微反应器中使碱金属与醇反应，其中微反应器提供层流器流。
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公开(公告)号：US20060228640A1
公开(公告)日：2006-10-12
申请号：US11450228
申请日：2006-06-09
CPC分类号： C09D5/035 , B01J19/0093 , C09B41/006 , C09D11/0235 , C09D11/037 , C09D11/32 , C09D11/322 , C09D11/34 , C09D11/36 , G03G9/091
摘要： The invention is directed to an electrophotographic toner or developer, powder coating, ink jet ink or an electronic media having an azo colorant prepared by conducting the diazotization of aromatic or hetaromatic amines or the azo coupling reaction or the diazotization and the azo coupling reaction in a microreactor.
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公开(公告)号：US20060142588A1
公开(公告)日：2006-06-29
申请号：US10544076
申请日：2003-12-13
申请人： Uwe Nickel , Detlef Wehle , Leonhard Unverdorben , Klaus Forstinger , Hieng Kim
发明人： Uwe Nickel , Detlef Wehle , Leonhard Unverdorben , Klaus Forstinger , Hieng Kim
IPC分类号： C07D235/22 , C07C69/76 , C07C309/29
CPC分类号： C07D235/26 , C07C67/46 , C07C231/04 , C07C303/22 , C07C303/32 , C07C69/72 , C07C309/51
摘要： The invention relates to a method for the production of β-keto-carboxylic acid derivatives of formula (I) or the salts thereof, where X═NR′, O or S, R, R′, R1-R4 independently ═H, alkyl, alkenyl, aryl or heteroaryl, by reaction of a diketene of formula (II) with a compound comprising an active hydrogen of formula ROH, NHRR′ or RSH, characterised in that the reaction is continuously carried out in a microreactor.
摘要翻译： 本发明涉及制备式（I）的β-酮 - 羧酸衍生物或其盐的方法，其中X-NR'，O或S，R，R'，R 1 通过式（II）的二烯酮与包含式ROH，NHRR'或RSH的活性氢的化合物的反应，独立地是-H，烷基，烯基，芳基或杂芳基，-R 因为反应在微反应器中连续进行。
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6.发明授权Preparation of azo colorants in microreactors and their use in electrophotographic toners and developers, powder coatings, ink jet inks and electronic medias 失效在微反应器中制备偶氮着色剂及其在电子照相调色剂和显影剂，粉末涂料，喷墨油墨和电子介质中的用途公开(公告)号：US07309389B2
公开(公告)日：2007-12-18
申请号：US11450228
申请日：2006-06-09
IPC分类号： C09D11/00
CPC分类号： C09D5/035 , B01J19/0093 , C09B41/006 , C09D11/0235 , C09D11/037 , C09D11/32 , C09D11/322 , C09D11/34 , C09D11/36 , G03G9/091
摘要： The invention is directed to an electrophotographic toner or developer, powder coating, ink jet ink or an electronic media having an azo colorant prepared by conducting the diazotization of aromatic or hetaromatic amines or the azo coupling reaction or the diazotization and the azo coupling reaction in a microreactor.
摘要翻译： 本发明涉及一种电子照相调色剂或显影剂，粉末涂料，喷墨油墨或具有通过芳香族或异丁基胺的重氮化或偶氮偶联反应或重氮化和偶氮偶联反应制备的偶氮着色剂的电子介质 微反应器
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公开(公告)号：US07135266B2
公开(公告)日：2006-11-14
申请号：US10238365
申请日：2002-09-10
IPC分类号： G03G9/087
CPC分类号： C09D5/035 , B01J19/0093 , C09B41/006 , C09D11/0235 , C09D11/037 , C09D11/32 , C09D11/322 , C09D11/34 , C09D11/36 , G03G9/091
摘要： The invention is directed to an electrophotographic toner or developer, powder coating, ink jet ink or an electronic media having an azo colorant prepared by conducting the diazotization of aromatic or hetaromatic amines or the azo coupling reaction or the diazotization and the azo coupling reaction in a microreactor.
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公开(公告)号：US06723138B2
公开(公告)日：2004-04-20
申请号：US10383025
申请日：2003-03-06
IPC分类号： C09B5700
CPC分类号： B01J19/0093 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00828 , B01J2219/00831 , B01J2219/00833 , B01J2219/00873 , B01J2219/00889 , B01J2219/0095 , C09B57/004 , C09B67/00 , F28F2260/02 , Y10T428/24562
摘要： A process for preparing diketopyrrolopyrrole pigments comprises conducting the elementary steps of pigment synthesis (reaction and hydrolysis) in a miniaturized continuous reactor.
摘要翻译： 制备二酮吡咯并吡咯颜料的方法包括在小型连续反应器中进行颜料合成（反应和水解）的基本步骤。
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公开(公告)号：US06566519B2
公开(公告)日：2003-05-20
申请号：US09874689
申请日：2001-06-05
IPC分类号： C07D48702
CPC分类号： B01J19/0093 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00828 , B01J2219/00831 , B01J2219/00833 , B01J2219/00873 , B01J2219/00889 , B01J2219/0095 , C09B57/004 , C09B67/00 , F28F2260/02 , Y10T428/24562
摘要： A process for preparing diketopyrrolopyrrole pigments comprises conducting the elementary steps of pigment synthesis (reaction and hydrolysis) in a miniaturized continuous reactor.
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公开(公告)号：US06436182B1
公开(公告)日：2002-08-20
申请号：US09612470
申请日：2000-07-07
申请人： Leonhard Unverdorben , Uwe Nickel , Andreas Harz , Gunnar Tilch
发明人： Leonhard Unverdorben , Uwe Nickel , Andreas Harz , Gunnar Tilch
IPC分类号： B01D3702
CPC分类号： C09B67/0096
摘要： The invention relates to an advantageous process for producing highly concentrated pigment presscakes which comprises concentrating a pigment suspension on a high-pressure filter press with a pressure of at least 16 bar to a pigment content of at least 50% by weight without adding nonionic surfactants which have a cloud point in water.
摘要翻译： 本发明涉及用于生产高浓缩颜料压饼的有利方法，其包括将颜料悬浮液在至少16巴的压力下在高压压滤机上浓缩至颜料含量至少为50重量％，而不添加非离子表面活性剂 在水中有一个浊点。
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