摘要:
The invention is directed to cleaning of micro- and mini-reactors for controlled process management and for avoiding blockages on carrying out chemical reactions and physical processes. The invention is characterized in that the micro- or mini-reactor is cleaned by means of a controlled pressure increase with a subsequent sudden release or with a gas pressure surge in a cyclical manner or using a controller. Wall deposits formed from solid material(s) involved in the chemical synthesis or the physical process are thus almost completely removed such that, after the cleaning procedure, the initial operating pressure can be set in the micro- or mini-reactor. A blockage of the micro- or mini-reactor can thus be avoided and the transferring of said production method to the production scale with micro- or mini-reactors is possible for the first time. The above is particularly true for reactions in which educts in the form of suspensions are used and/or solid products arise, such as in the production of azo dyes, for example.
摘要:
Azo colorants are prepared by conducting the diazotization of aromatic or hetaromatic amines or the azo coupling reaction or the diazotization and the azo coupling reaction in a microreactor.
摘要:
Disclosed is a method for continuously preparing a water-soluble azo dye by coupling a nebulizer with a pipeline. According to the method, the nebulizer is coupled with a pipeline with an interception tower plate, atomized and mixed reaction liquid flow flows through the pipeline with the interception tower plate, and mixing and reacting are further enhanced through turbulent mixing on the tower plate, so that instant separation of reaction heat generated in an atomizing contact reaction from a reactant is achieved, and normal-temperature rapid continuous production of the water-soluble azo dye is achieved. Fog drops which are atomized by using the nebulizer have small particle diameter and large specific surface area, so that a diazo salt and a coupling component are sprayed separately, move face to face and can be fully contacted, and mixing and reacting speeds are increased. The preparation method is simple, and compared with preparation of a dye of the same kind with a batch reactor, in the reparation process of the water-soluble azo dye, a cold source is not required to be added additionally for cooling, thereby reducing energy consumption and improving production quality and efficiency.
摘要:
In C. I. pigment red 57:1 of the present invention, the total content of 3-hydroxy-2-naphthoic acid and a metal salt thereof, which is measured by quantitative analysis using liquid chromatography, is 2,500 ppm or less as converted into the 3-hydroxy-2-naphthoic acid.
摘要:
A mixing apparatus including a plurality of nozzle groups each formed of nozzles for ejecting the same fluid arranged in group, the nozzles being provided with openings for ejecting fluid, to cause the plurality of nozzle groups to separately eject a plurality of fluids to mix the fluids in areas on the extending lines of the nozzles, wherein the openings of the nozzles forming the nozzle groups are arranged along annular loci and the plurality of nozzle groups are arranged coaxially to each other, a plurality of supplying channels for supplying the plurality of fluids to the nozzle groups corresponding to the plurality of nozzle groups are annular in cross section in the direction perpendicular to the direction in which fluid supplied to the supplying channels flows and arranged coaxially to each other.
摘要:
Azo colorants are prepared by conducting the diazotization of aromatic or hetaromatic amines or the azo coupling reaction or the diazotization and the azo coupling reaction in a microreactor.
摘要:
The invention provides a process for preparing uncoated, readily dispersible C.I. Pigment Red 112 by azo coupling in a microreactor, which comprises precipitating the coupling component in an upstream microreactor and coupling the precipitated coupling component in finely divided form to the diazo component in a microreactor.The C.I. Pigment Red 112 of the invention features low dispersion harshness in alkyd resin varnish, and a PCB content of below 25 ppm.
摘要:
A mixing apparatus including a plurality of nozzle groups each formed of nozzles for ejecting the same fluid arranged in group, the nozzles being provided with openings for ejecting fluid, to cause the plurality of nozzle groups to separately eject a plurality of fluids to mix the fluids in areas on the extending lines of the nozzles, wherein the openings of the nozzles forming the nozzle groups are arranged along annular loci and the plurality of nozzle groups are arranged coaxially to each other, a plurality of supplying channels for supplying the plurality of fluids to the nozzle groups corresponding to the plurality of nozzle groups are annular in cross section in the direction perpendicular to the direction in which fluid supplied to the supplying channels flows and arranged coaxially to each other.
摘要:
The invention relates to a method for carrying out chemical and physical methods, in particular for producing organic pigments or the preparations based thereon. The inventive method consists in injecting at least two liquids or suspensions in a vertex chamber, without using carrying gas, with the aid of two end pipes which are not coaxially oriented. Said injection is carried out at a pressure ranging from 1 to 1000 bars and in conformity with a volume flow rate ranging from 5 to 500 l/h, thereby producing the vertex mixing of a liquid phase with a material modification, and continuously extracting said liquid phase from the vertex chamber through a removing hole, the material modification being obtained