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    Production of nickelized shaped articles
    1.
    发明授权
    Production of nickelized shaped articles 失效
    镍化物品的生产

    公开(公告)号：US5445727A

    公开(公告)日：1995-08-29

    申请号：US256374

    申请日：1994-07-25

    申请人： Volker Schwendemann ,  Klaus Glaser ,  Chung-Ji Tschang ,  Bernd Burkhart ,  Alfred Oftring ,  Bernhard Dung

    发明人： Volker Schwendemann ,  Klaus Glaser ,  Chung-Ji Tschang ,  Bernd Burkhart ,  Alfred Oftring ,  Bernhard Dung

    IPC分类号： C25D3/16 ,  C25D3/14 ,  C25D3/18

    CPC分类号： C25D3/14

    摘要： Nickelized shaped articles are produced by electrodeposition of nickel from aqueous acidic baths containing as essential constituents one or more nickel salts, one or more inorganic acids and at least two brighteners by using as brighteners a mixture ofA) from 2 to 98% by weight of one or more cyclic N-allylammonium or N-vinylammonium compounds I ##STR1## where the nitrogen atom is part of a pyridine, quinoline or isoquinoline ring system which may additionally carry one or two C.sub.1 - to C.sub.4 -alkyl substituents or halogen atoms,R.sup.1, R.sup.3 and R.sup.4 are each hydrogen or C.sub.1 - to C.sub.4 -alkyl,R.sup.2 is hydrogen or methyl,m is from 0 to 4,n is from 1 to 4, andX.sup..crclbar. is an n-valent inorganic or organic anion which promotes solubility in water, andB) from 98 to 2% by weight of one or more acetylenically unsaturated compounds IIR.sup.4 --C.tbd.C--R.sup.5 (II) where R.sup.4 and R.sup.5 are identical or different and each is C.sub.1 - to C.sub.4 -alkyl substituted by hydroxyl, sulfo, amino, C.sub.1 - to C.sub.4 -alkylamino or di(C.sub.1 - to C.sub.4 -alkyl)amino, although hydroxyl groups may have been reacted with from 1 to 10 mol of a C.sub.2 - to C.sub.4 -alkylene oxide or a mixture of such alkylene oxides and one of the radicals R.sup.4 and R.sup.5 may also be hydrogen or C.sub.1 - to C.sub.4 -alkyl.

    摘要翻译： PCT No.PCT / EP93 / 00063 Sec。 371日期：1994年7月25日 102（e）日期1994年7月25日PCT提交1993年1月14日PCT公布。 公开号WO93 / 15241 日期：1993年8月5日。通过使用含有酸性浴的含水酸性浴，通过使用作为增白剂的A）的混合物，将含有作为必需组分的一种或多种镍盐，一种或多种无机酸和至少两种增白剂的镍电沉积 2至98重量％的一种或多种环状N-烯丙基铵或N-乙烯基铵化合物I（I）其中氮原子是吡啶，喹啉或异喹啉环体系的一部分，其可另外携带一个或两个C1- 对于C 4 - 烷基取代基或卤素原子，R 1，R 3和R 4各自为氢或C 1〜C 4 - 烷基，R 2为氢或甲基，m为0〜4，n为1〜4，X（ - ） 是促进在水中的溶解度的n价无机或有机阴离子，以及B）98至2重量％的一种或多种炔属不饱和化合物II R4-C 3BOND C-R5（II），其中R4和R5相同或 各自为被羟基，磺基，氨基，C 1〜C 4 - 烷基氨基或二（C1- 对于C 4 - 烷基）氨基，尽管羟基可以与1至10摩尔的C 2 -C 4环氧烷烃或这种烯化氧与其中一个基团R4和R5的混合物也可以是氢或C1 - 至C 4 - 烷基。

    Production of shining shaped articles coated with zinc or a zinc alloy
    2.
    发明授权
    Production of shining shaped articles coated with zinc or a zinc alloy 失效
    生产镀锌或锌合金的发光成型制品

    公开(公告)号：US5421990A

    公开(公告)日：1995-06-06

    申请号：US140178

    申请日：1993-11-09

    申请人： Erwin Hahn ,  Bernhard Dung ,  Bernd Burkhart ,  Chung-Ji Tschang

    发明人： Erwin Hahn ,  Bernhard Dung ,  Bernd Burkhart ,  Chung-Ji Tschang

    IPC分类号： C25D3/22 ,  C25D3/56

    CPC分类号： C25D3/22

    摘要： The production of shining shaped articles coated with zinc or a zinc alloy by electrodeposition of zinc or a zinc alloy from acidic aqueous electrolytic baths which contain as essential components one or more zinc salts and, where appropriate, salts of the other alloy metals, one or more conducting salts, one or more surfactants and one or more brighteners, entails employing as brighteners compounds of the formula I ##STR1## where R.sup.1 is C.sub.1 -C.sub.8 -alkoxy, phenoxy, benzyloxy, amino, C.sub.1 -C.sub.6 -alkylamino or di(C.sub.1 -C.sub.6)alkylamino,R.sup.2 is C.sub.1 -C.sub.4 -alkyl, phenyl, benzyl or the meanings of R.sup.1, andAr is phenyl or naphthyl which can additionally be substituted by one to three C.sub.1 -C.sub.4 -alkyl groups or C.sub.1 -C.sub.4 -alkoxy groups.

    摘要翻译： PCT No.PCT / EP92 / 00983第 371日期：1993年11月9日 102（e）日期1993年11月9日PCT提交1992年5月6日PCT公布。 公开号WO92 / 22683 日期为1992年12月23日。通过从酸性水溶液电解浴中电镀锌或锌合金制成涂有锌或锌合金的闪亮成形制品，其中含有一种或多种锌盐和适当的盐， 其他合金金属，一种或多种导电盐，一种或多种表面活性剂和一种或多种增白剂，需要使用式I的增白剂化合物，其中R 1是C 1 -C 8 - 烷氧基，苯氧基，苄氧基，氨基，C 1 C 1-6 - 烷基氨基或二（C 1 -C 6）烷基氨基，R 2是C 1 -C 4烷基，苯基，苄基或R 1的含义，Ar是苯基或萘基，其可另外被一至三个C 1 -C 4烷基 基团或C 1 -C 4 - 烷氧基。

    Method for producing stable aqueous polymer dispersions based on conjugated alphatic dienes and vinyl aromatic compounds
    8.
    发明申请
    Method for producing stable aqueous polymer dispersions based on conjugated alphatic dienes and vinyl aromatic compounds 审中-公开
    基于共轭二烯和乙烯基芳族化合物制备稳定的聚合物水分散体的方法

    公开(公告)号：US20060148981A1

    公开(公告)日：2006-07-06

    申请号：US10541206

    申请日：2003-12-24

    申请人： Jurgen Schmidt-Thummes ,  Jurgen Hartmann ,  Chung-Ji Tschang

    发明人： Jurgen Schmidt-Thummes ,  Jurgen Hartmann ,  Chung-Ji Tschang

    IPC分类号： C08F2/26

    CPC分类号： C08F236/04 ,  C08F212/04 ,  C08F257/02 ,  C08F2/24

    摘要： The present invention provides a process for preparing a stable aqueous copolymer dispersion by free-radically initiated aqueous emulsion polymerization of a) from 19.9 to 80 parts by weight of conjugated aliphatic dienes [monomers a)], b) from 19.9 to 80 parts by weight of vinylaromatic compounds [monomers b)], c) from 0.1 to 10 parts by weight of ethylenically unsaturated carboxylic acids and/or dicarboxylic acids [monomers c)], d) from 0 to 20 parts by weight of ethylenically unsaturated carbonitriles [monomers d)], and e) from 0 to 20 parts by weight of copolymerizable compounds other than monomers b) [monomers e)], the total amount of ethylenically unsaturated monomers a) to e) being 100 parts by weight, in the presence of water and from 0.1 to 5 parts by weight, based on the total monomer amount, of emulsifiers comprising f) sulfuric monoesters of ethoxylated fatty acid alcohols and/or g) salts of esters and monoesters of alkylpolyoxyethylenesulfosuccinates, from 15 to 85% by weight of the total emulsifiers used being added within the time taken to reach up to 40% of the total conversion of the monomers a) to e), and from 1 to 50% of the carboxylic acid groups deriving from the monomers c) being neutralized by addition of base.

    摘要翻译： 本发明提供了一种通过自由基引发的水乳液聚合制备稳定的含水共聚物分散体的方法，a）从19.9至80重量份的共轭脂族二烯[单体a]]，b）19.9至80重量份 的乙烯基芳族化合物[单体b）]，c）0.1至10重量份的烯属不饱和羧酸和/或二羧酸[单体c]]，d）0至20重量份的烯键式不饱和碳原子[单体d ）]和e）0〜20重量份的可与单体不同的共聚合物b）[单体e]]，烯属不饱和单体a）至e）的总量为100重量份，在水存在下 和基于总单体量的0.1至5重量份的乳化剂，其包含f）乙氧基化脂肪酸醇的硫酸单酯和/或g）烷基聚氧乙基磺基琥珀酸酯和单酯的盐，其为15至85重量％ 使用的总乳化剂的总量在所需时间内加入达到单体a）至e）的总转化率的40％，以及1至50％来源于单体的羧酸基团c）被中和 通过添加基础。