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    Process of making naphthacene from propargyl alcohol
    3.
    发明授权
    Process of making naphthacene from propargyl alcohol 有权
    由炔丙醇制备并四苯的工艺

    公开(公告)号：US07323610B2

    公开(公告)日：2008-01-29

    申请号：US10899821

    申请日：2004-07-27

    申请人： William J. Begley ,  Manju Rajeswaran ,  Natasha Andrievsky

    发明人： William J. Begley ,  Manju Rajeswaran ,  Natasha Andrievsky

    IPC分类号： C07C1/20

    CPC分类号： C07C1/322 ,  C07C2603/44 ,  C07C15/62 ,  C07C15/38

    摘要： A process for synthesizing a naphthacene compound comprises the steps of: (a) reacting a propargyl alcohol compound with a reagent capable of forming a leaving group to form a reaction mixture containing an intermediate; and then (b) heating the intermediate in the presence of a solvent and in the absence of any oxidizing agent and in the absence of any base, to form the naphthacene compound.

    摘要翻译： 合成并四苯化合物的方法包括以下步骤：（a）使炔丙醇化合物与能够形成离去基团的试剂反应形成含有中间体的反应混合物; 然后（b）在溶剂存在下和在不存在任何氧化剂的情况下，在不存在任何碱的情况下加热中间体，以形成并四苯化合物。

    Organic element for low voltage electroluminescent devices
    6.
    发明授权
    Organic element for low voltage electroluminescent devices 有权
    低电压电致发光器件的有机元件

    公开(公告)号：US07767317B2

    公开(公告)日：2010-08-03

    申请号：US11259586

    申请日：2005-10-26

    申请人： William J. Begley ,  Manju Rajeswaran ,  Tukaram K. Hatwar ,  Natasha Andrievsky

    发明人： William J. Begley ,  Manju Rajeswaran ,  Tukaram K. Hatwar ,  Natasha Andrievsky

    IPC分类号： H01L51/54 ,  H01J1/62

    CPC分类号： H01L51/0071 ,  C09K11/06 ,  C09K2211/1007 ,  C09K2211/1011 ,  C09K2211/1014 ,  C09K2211/1055 ,  C09K2211/186 ,  H01L51/0054 ,  H01L51/0055 ,  H01L51/0056 ,  H01L51/0058 ,  H01L51/0059 ,  H01L51/0069 ,  H01L51/0076 ,  H01L51/0079 ,  H01L51/008 ,  H01L51/5012 ,  H01L51/5036 ,  H01L51/5048 ,  H05B33/14 ,  Y10S428/917

    摘要： An OLED device comprises a cathode, a light emitting layer and an anode, in that order, and, having located between the cathode and the light emitting layer, a further layer containing; (a) 10 vol % or more of a carbocyclic fused ring aromatic compound, and (b) a cyclometallated complex represented by Formula (4′) wherein: Z and the dashed arc represent two or three atoms and the bonds necessary to complete a 5- or 6-membered ring with M; each A represents H or a substituent and each B represents an independently selected substituent on the Z atoms, provided that two or more substituents may combine to form a fused ring or a fused ring system; j is 0-3 and k is 1 or 2; M represents a Group IA, IIA, IIIA and IIB element of the Periodic Table; and m and n are independently selected integers selected to provide a neutral charge on the complex; and provided that the complex does not contain the 8-hydroxyquinolate ligand. Such devices exhibit reduce drive voltage while maintaining good luminance.

    摘要翻译： OLED器件依次包括阴极，发光层和阳极，并且位于阴极和发光层之间，还包含含有 （a）10体积％以上的碳环稠环芳香族化合物，（b）由式（4'）表示的环金属络合物，其中：Z和虚线表示2个或3个原子，完成5 - 或6元环与M; 每个A表示H或取代基，并且每个B表示Z原子上独立选择的取代基，条件是两个或多个取代基可以结合形成稠环或稠环体系; j为0-3，k为1或2; M表示周期表的IA，IIA，IIIA和IIB族元素; 并且m和n是独立选择的整数，以在络合物上提供中性电荷; 并且条件是所述复合物不含有8-羟基喹啉配体。 这样的器件在保持良好亮度的同时表现出降低驱动电

    Process of making naphthacene from a propargyl alcohol
    9.
    发明授权
    Process of making naphthacene from a propargyl alcohol 有权
    从炔丙醇制备并四苯的工艺

    公开(公告)号：US07355085B2

    公开(公告)日：2008-04-08

    申请号：US10899919

    申请日：2004-07-27

    申请人： William J. Begley ,  Manju Rajeswaran ,  Natasha Andrievsky

    发明人： William J. Begley ,  Manju Rajeswaran ,  Natasha Andrievsky

    IPC分类号： C07C1/20

    CPC分类号： C07C1/28 ,  C07C1/322 ,  C07C25/22 ,  C07C41/30 ,  C07C43/2055 ,  C07C2603/44 ,  C07C15/38

    摘要： A process for synthesizing a single isomer of a naphthacene compound comprises the steps of: (a) reacting a symmetrically substituted 1,1-diarylpropargyl alcohol compound with a reagent capable of forming a leaving group to form a reaction mixture containing a intermediate; and then (b) heating the intermediate in the presence of a solvent and in the absence of any oxidizing agent to form a single naphthacene compound.

    摘要翻译： 合成并四苯化合物的单一异构体的方法包括以下步骤：（a）使对称取代的1,1-二芳基炔丙醇化合物与能够形成离去基团的试剂反应形成含有中间体的反应混合物; 然后（b）在溶剂存在下和不存在任何氧化剂的情况下加热中间体以形成单一并四苯化合物。